反応チャンバー:
XRK 900
XRK 900はX線回折用に設計された唯一の市販反応チャンバーで、900 ℃、10 barまでの固体及び固体 -気体反応の測定に使用されます。堅牢で高性能なXRK 900は、他社製品の追従を許さない優れたIn-Situ X線回析研究用機器です。
技術仕様
動作温度 | 25~900 °C |
---|---|
温度測定 | NiCr/NiAl熱電対 |
雰囲気 | 真空(1 mbar)、空気、不活性ガス、反応ガス |
ハウジング最大温度 | 150 °C |
入射角 | 0~+165° 2Θ |
最大圧力 | 1 mbar~10 bar |
サンプルホルダーの材質 | ステンレス鋼またはガラスセラミック |
サンプル直径 | 最大14 mm |
測定システム | 反射 |
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SIEVE FOR SAMPLE HOLDER OPEN MACOR
Macor plate with Ø 0.5 mm holes for gas flow through the sample.

SAMPLE HOLDER CLOSED MADE OF GLASS CERAMICS (MACOR)
Closed sample holder made of Macor (glass ceramics) Gas flow through the sample and extraction of gas through the sample holder is not possible.

SIEVE 0.2 mm MACOR FOR XRK SAMPLE HOLDER OPEN
Macor plate with Ø 0.2 mm holes for gas flow through the sample.

SAMPLE HOLDER CLOSED MADE OF STAINLESS STEEL
Closed stainless steel sample holder. Gas flow through the sample and extraction of gas through the sample holder is not possible. Maximum operating temperature 600 °C.

SAMPLE HOLDER OPEN STEEL WITH SIEVE
Stainless steel sample holder where the sample is placed on a sieve plate. Gas can flow through the sample and can be extracted at the bottom of the sample holder. Not feasible for vacuum operation of XRK 900. Maximum operating temperature 600 °C.

SAMPLE HOLDER OPEN MACOR WITH SIEVE
Sample holder made of Macor (glass ceramics) where the sample is placed on a sieve plate (69963). Gas can flow through the sample and can be extracted at the bottom of the sample holder. Not feasible for vacuum operation of XRK 900

SPARE PARTS PACKAGE XRK 900
Consists of:
- 2 Pcs. 17162 Set of Kapton foils (XRK with BE foil)
- 1 Pc. 13463 Pressure hose silicone (6.5 m)
- 1 Pc. 70175 Vacuum grease (20 g)
- 1 Pc. 10213 Set of O-Rings

Si (510) ZERO BACKGROUND INSERT XRK
Si(510) plate of 0.5 mm thickness without X-ray scattering for X-ray transparent samples. Maximum temperature in oxidizing atmospheres: 500 °C Maximum temperature in non-reactive atmospheres: 900 °C.