| | Autosorb 6100 | Autosorb 6200 | Autosorb 6300 |
| Measurement Specisfitations |
| Measurement principle | Vacuum volumetric | Vacuum volumetric | Vacuum volumetric dynamic flow |
| Adsorption gases | Standard
N2, Ar, Kr, CO2, CO, H2, CH4, C2H6, C3H8 | Extended range
N2, Ar, Kr, CO2, CO, H2, CH4, C2H6, C3H8, NH3 |
| Adsorption vapors | N/A | H2O, C6H6, C5H5N, C3H6O, C2H5OH, CH3OH, C3H7OH |
| Physisorption analysis stations | Number: 1, 2, or 3
Independent analysis stations: Up to three gases at three analysis temperatures can be used concurrently (one analysis gas and temperature per station)
Independent p0 station (dedicated cell and transducer) |
| Chemisorption analysis stations | N/A | 1 |
| Maximum pressure | 1,100 Torr (0.997 p/p0 for N2 77 K) |
| Pressure resolution | 2 × 10-5 Torr (2.6 × 10-8 p/p0 for N2 77 K) | 1 × 10-6 Torr (1.3 × 10-9 p/p0 for N2 77 K) |
| BET surface area | - Absolute detection limit: 0.1 m² (N2 77 K)
- Specific detection limit: 0.01 m²/g (N2 77 K)
- Typical reproducibility: 1 % (measured on BAM P115)
- Reproducibility limit: 2 % with 2 m² in the cell |
| Pore size | - Range: 0.35 nm to 500 nm (diameter)
- Typical reproducibility: 0.5 % (measured on BAM P115) |
| Active area | N/A | - Absolute detection limit: 0.03 m² (H₂ on platinum 313 K)
- Specific detection limit: 0.003 m²/g (H₂ on platinum 313 K)
- Typical reproducibility: 2 % (measured on 2 % platinum on alumina reference sample) |
| TruZone | Yes (active coolant level control) |
| PowderProtect | Yes (prevents sample elutriation) |
| Analysis dewar | - Duration: 90+ hours with liquid nitrogen
- Refill during analysis: Yes
- Volume: 3 L |
| Analysis furnace | N/A | - Maximum temperature: 1,100 °C
- Maximum ramp rate: 50 °C per minute
- Furnace cooling by built-in fan |
| Sample preparation | - Six integrated degassing stations with dedicated cold trap
- Temperature control: two independent heating zones, ambient to 450 °C
- Available methods: flow and vacuum, programmable multi-step degassing profiles, test for completion routines, pressure-controlled heating |
| CryoSync control | N/A | Yes | Yes |
| Mass spectrometer | N/A | N/A | Yes |
| Software Specifications |
| Kaomi for Autosorb software | - Control up to four instruments from one PC
- Eight languages: Chinese, English, French, German, Japanese, Korean, Portuguese, Spanish
- DoseWizard: 45+ built-in analysis profiles (ASTM, USP, DIN, ISO) |
| Technical Specifications |
| Dimensions (W x D x H) | 79.5 cm × 70.1 cm × 107.9 cm (31.3 in × 27.6 in × 42.5 in) depending on instrument configuration |
| Weight | 136.4 kg (300 lbs) depending on instrument configuration |
| Operating environment | - Temperature: 15 °C to 35 °C (59 °F to 95 °F)
- Humidity: 20 % RH to 80 % RH, non-condensing
- Indoor use only
- Altitude up to 3,000 m |
| Analysis manifold construction | Vacuum-brazed manifold block in stainless steel |
| Analysis manifold temperature | User-adjustable 35 °C to 50 °C (stability: ±0.05 °C) |
| Pressure transducer (1,550 Torr) | - Number: 3 to 5 (depending on instrument configuration)
- Accuracy: ±0.1 % of span (typical), ±0.15 % of span (maximum)
- A/D data acquisition: 32 bit |
| Pressure transducer (10 Torr) | - Number: 1 to 3 (depending on instrument configuration)
- Accuracy: ±0.15 % reading up to 10 Torr
- Resolution: 0.002 % of full scale |
| Pressure transducer (1 Torr) | - Number: 1 to 3 (depending on instrument configuration)
- Accuracy: ±0.15 % reading up to 1 Torr
- Resolution: 0.002 % of full scale | N/A | N/A |
| Pressure transducer (0.1 Torr) | N/A | - Number: 1 to 3 (depending on instrument configuration)
- Accuracy: ±0.15 % reading up to 0.1 Torr
- Resolution: 0.001 % of full scale |
| Pirani vacuum gauge | - Number: 1
- Accuracy:
- 5 × 10⁻⁴ Torr to 1 × 10⁻³ Torr: ±10 % of reading
- 1 × 10⁻³ Torr to 100 Torr: ±5 % of reading
- 100 Torr to atmosphere: ±25 % of reading |
| Vacuum system | - Turbo-molecular drag pump and dry-diaphragm pump
- Manufacturer’s specification: 5 mbar × 10⁻¹⁰ mbar to 2.67 mbar × 10⁻⁵ mbar
- Typical pressure at analysis port: 2.67 mbar × 10⁻⁵ mbar |
| Thermal conductivity detector (TCD) | N/A | N/A | - Two-filament TCD with rhenium/tungsten filaments
- Detection Limit: 0.5 µL (air injected into helium) |
| Input ports | - 7
(five analysis (FKM), one helium, one degas/backfill) | - 8
(four analysis (FKM), one analysis (PFE), one vapor, one helium, one degas/backfill) | - 16 ports
(11 analysis (FKM), one analysis (PFE), one vapor, one helium, one degas/backfill, one titration) |
| Gas supply | - Purity: 99.999 %
- Input pressure: 8 psig to 10 psig (0.55 bar to 0.69 bar) |
| Air | - Input pressure: 50 psig to 100 psig (3.45 bar to 6.9 bar) |
| Electrical | - Supply: AC 100 to 240 V AC, 50 / 60 Hz
- Maximum consumption: 1,810 VA (depending on instrument configuration) |
| PC connection | Ethernet |
| RoHS3 compliant | Yes |
| CE / UKCA certified | Yes |
