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High Vacuum Physisorption Analyzer:
Autosorb

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Model:
  • Accurate high vacuum physisorption analyses of surface area and micropores 
  • Advanced measurement routines made accessible with DoseWizard point selection and PowderProtect
  • Up to three samples, three gases, and three temperatures can be measured simultaneously with independent analysis stations
    Autosorb Contact

    Autosorb instruments are high vacuum physisorption and chemisorption analyzers designed for advanced measurements of BET surface area, active area, and pore size distributions. Independent analysis stations, exclusive TruZone active coolant control, and accessible Kaomi software let you meet your current measurement needs, while factory and field upgradeable options let you adapt to future ones. For your most important gas sorption measurements, the choice is clear: Absolutely Autosorb.

    Key features

    A gas sorption analyzer that’s absolutely accurate

    A gas sorption analyzer that’s absolutely accurate

    • Get highly accurate physisorption measurements from relative pressures below 10-7 for nitrogen 
    • Leverage precise manifold temperature control between 35 °C and 50 °C
    • Rely on TruZone active coolant level control for accurate data – even over lengthy analyses
    • Achieve superior high vacuum performance (38 % better than previous generation instruments) with precision-machined manifolds and high-quality pneumatic valves 
    Independent stations ensure you’re absolutely agile

    Independent stations ensure you’re absolutely agile

    • Analyze up to three different samples with three different analysis gases at three different temperatures simultaneously with independent analysis stations and patented temperature control accessories
    • Perform the most challenging physisorption measurements with the 90-hour Dewar
    • Maximize your throughput with six integrated degassing stations
    • Quickly swap to the 1100 °C furnace for advanced temperature programmed analyses, pulse titrations, or chemisorption isotherms 
    Intuitive software makes every analysis absolutely accessible

    Intuitive software makes every analysis absolutely accessible

    • Enjoy an updated and streamlined Kaomi software, which makes the whole measurement process easier than ever before
    • Optimize measurement definition to suit your needs with DoseWizard’s new standard and advanced modes
    • Keep downtime to a minimum with PowderProtect, which prevents accidental loss of powder in the instrument
    Customization options keep you absolutely adaptable

    Customization options keep you absolutely adaptable

    • With 3 instruments and modular upgrades, the Autosorb adapts to the exact analysis requirements of your porous solids and catalysts
    • As your research changes, the instrument’s physisorption and chemisorption features can be field upgraded to fit new materials and applications
    • Go beyond standard measurements with enhanced chemical resistance, a built-in vapor source, thermal conductivity detector, or even a fully integrated mass spectrometer
    Compliance and quality are absolutely assured

    Compliance and quality are absolutely assured

    • Comply with 20+ ASTM, DIN, and ISO standards for catalyst characterization and the evaluation of porous solids. 
    • Get peace of mind with our 3-year warranty so you can avoid unforeseen costs 

    Technical specifications

    Measurement Specifications

     

     Autosorb 6100Autosorb 6200Autosorb 6300
    Measurement principle
    • Vacuum Volumetric Physisorption
    • Vacuum Volumetric Physisorption
    • Vacuum Volumetric Chemisorption
    • Dynamic Flow Chemisorption (Optional)
    • Vacuum Volumetric Physisorption
    • Vacuum Volumetric Chemisorption
    • Dynamic Flow Chemisorption
    Analysis gas compatibility   
    N2, Ar, Kr, CO2, H2, and other non-corrosive gasesIncludedIncludedIncluded
    CH4, C2H6, C3H8, other alkanes, C6H6, C8H10IncludedDependent on instrument configurationIncluded
    NH3, C5H5N, C3H6O, and other reactive gasesN/ADependent on instrument configurationIncluded
    Physisorption analysis stationsNumber: 1, 2, or 3
    Independence: Up to 3 gases at 3 analysis temperatures can be used concurrently, 
    1 analysis gas and temperature per station
    Chemisorption analysis stationsN/A1
    Independent p0 stationYes (dedicated cell and transducer)
    Pressure
    • Range: 2x10-5 to 1100 Torr (2.6x10-8 to 0.997 p/p0 for N2 77K)
    • Resolution (MP): 2x10-5 Torr (2.6x10-8 p/p0 for N2 77K)
    • Resolution (XR): 1x10-6 Torr (1.3x10-9 p/p0 for N2 77K)
    BET surface area
    • Absolute detection limit: 0.1 m2 (N2 77K)
    • Specific detection limit: 0.01 m2/g (N2 77K)
    • Typical reproducibility: 1 % (measured on BAM P115)
    • Reproducibility limit: 2 % with 2 m2 in the cell
    Pore size
    • Range: 0.35 nm to 500 nm (diameter)
    • Typical reproducibility: 0.5 % (measured on BAM P115)
    Active areaN/A
    • Absolute detection limit: 0.03 m2 (H2 on Platinum 313 K)
    • Specific detection limit: 0.003 m2/g (H2 on Platinum 313K)
    • Typical reproducibility: 2 % (measured on 2% Platinum on Alumina reference sample)
    TruZoneYes (active coolant level control)
    PowderProtectYes (prevents sample elutriation)
    Analysis dewar
    • Duration: 90+ hours with liquid nitrogen
    • Refill during analysis: Yes
    • Volume: 3 L
    Analysis furnaceN/A
    • Maximum temperature: 1,100 °C
    • Maximum Ramp Rate: 50 °C per minute
    • Furnace cooling by built-in fan
    Sample preparation
    • Integrated degassing stations: 6
    • Temperature control: 2 independent heating zones, ambient to 450 °C
    • Dedicated cold trap: Yes
    • Available methods: flow and vacuum, programmable multi-step degassing profiles, test for completion routines, pressure-controlled heating
    Additional capabilities   
    Vapor sourceOptionalOptionalIncluded
    CryoSync control OptionalOptionalOptional
    TCD and loop injectorN/AOptionalIncluded
    Mass spectrometerN/AOptionalOptional

     

    Kaomi software features

     

     Autosorb 6100Autosorb 6200Autosorb 6300
    Instrument connectionControl up to 4 instruments from 1 PC
    DoseWizard
    • 45+ built-in analysis profiles aligned with ASTM, DIN, and ISO
    • Standard profiles with easy measurement selection
    • Advanced profiles with full control of experimental procedures 
    • Dose templates for rapid measurement based on previous analyses
    Physisorption methods
    • Surface area and pore volume: Alpha-s, BET, DR, Gurvich pore volume, Langmuir, t-plot (STSA)
    • Pore size and pore volume distributions: NLDFT, QSDFT, GCMC, Kr(87) thin-film, BJH, DH, DA, HK, SF, MP
    • Other: summary reports, overlays, average particle size, average pore size, fractal dimensions (NK, FHH), heat of adsorption
    Chemisorption methodsN/A
    • Static measurements: extrapolation, bracketing, Langmuir, Temkin, Freundlich, heat of adsorption
    • Dynamic flow measurements: TPx (TPR,TPO,TPD) peak deconvolution, pulse titration analysis, activation energy
    Available languages  Chinese, English, French, German, Japanese, Korean, Portuguese, Spanish

     

    Technical Specifications

     

     Autosorb 6100Autosorb 6200Autosorb 6300
    Dimensions (W x D x H)79.5 cm x 70.1 cm x 107.9 cm (31.3 in x 27.6 in x 42.5 in) dependent on instrument configuration
    Weight136.4 kg (300 lbs) dependent on instrument configuration
    Operating environment
    • Temperature: 15 °C to 35 °C (59 °F to 95 °F)
    • Humidity: 20% RH to 80% RH, non-condensing
    Gas distribution manifold elastomersFKMFKM or EPDM (dependent on instrument configuration)PFE
    Analysis manifold constructionVacuum-brazed manifold block in stainless steel
    Analysis manifold temperature
    • Range: user adjustable 35 °C to 50 °C
    • Stability: ±0.05 °C
    Analysis manifold valves
    • Type: stainless steel, air-operated bellows valve
    • Cycle life: 5,000,000 cycles
    • External leak rate: 5x10-12 Pa m3/sec
    • Seat leak rate: 5x10-12 Pa m3/sec
    Pressure transducer (1550 Torr) 
    -Analysis and degas
    • Number: 3 to 5 (dependent on instrument configuration)
    • Accuracy: ±0.065% full scale* (*This value incorporates precision, linearity, and hysteresis for the entire pressure measurement system)
    • A/D data acquisition: 32 bit
    Pressure transducer (10 Torr)
    – MP or XR
    • Number: 1 to 3 (dependent on instrument configuration)
    • Accuracy: ±0.15 % reading up to 10 Torr
    • Resolution: 0.002 % full scale
    Pressure transducer (1 Torr)
    – MP only
    • Number: 1 to 3 (dependent on instrument configuration)
    • Accuracy: ±0.15 % reading up to 1 Torr
    • Resolution: 0.002 % full scale
    Pressure transducer (0.1 Torr)
    – XR only
    • Number: 1 to 3 (dependent on instrument configuration)
    • Accuracy: ±0.15 % reading up to 0.1 Torr
    • Resolution: 0.001 % full scale
    Pirani vacuum gauge
    – Degas only
    • Number: 1
    • Accuracy:
      5×10-4 to 1x10-3 Torr: ±10 % of reading
      1×10-3 to 100 Torr: ±5 % of reading
    • 100 Torr to atmosphere: ±25 % of reading
    Vacuum system
    • Turbo molecular drag pump and dry diaphragm pump
    • Manufacturer’s specification: 5x10-10 mbar
    • Typical pressure at analysis port: 2.67x10-5 mbar
    Thermal conductivity detector (TCD)N/A
    • Two-filament TCD with rhenium/tungsten filaments (optional)
    • Detection Limit: 0.5 uL (air injected into helium)
    • Two-filament TCD with rhenium/tungsten filaments (standard)
    • Detection Limit: 0.5 uL (air injected into helium)
    Gas ports
    • 7 ports standard (5 analysis, 1 helium, 1 degas/backfill)
    • 7 additional analysis ports optional
    • 7 ports standard (5 analysis, 1 helium, 1 degas/backfill)
    • 7 additional analysis ports optional
    • 1 titration gas port optional
    • 15 ports standard (12 analysis, 1 helium, 1 degas/backfill, 1 titration)
    Gas supply
    • Purity: 99.999 %
    • Input pressure: 8 psig to 10 psig (0.55 bar to 0.69 bar)
    Air
    • Input pressure: 50 psig to 100 psig (3.45 bar to 6.9 bar)
    Electrical
    • Supply: 100 to 240 VAC ±10%, 50 or 60Hz
    • Maximum consumption: 1600W (dependent on instrument configuration)
    PC connectionEthernet
    RoHS3 compliantYes
    CE / UKCA certifiedYes
    Indoor/outdoor useFor indoor use only

    Standards

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    ASTM

    B922 6100, 6200
    C1069 6100, 6200
    C1274 6100, 6200
    D1993 6100
    D3663 6100
    D3908 6100
    D4222 6100
    D4365 6100
    D4641 6100
    D4780 6100
    D4824 6100
    D6556 6100

    DIN

    66134 6100
    66135-1 6100
    66135-2 6100
    66135-3 6100
    66135-4 6100

    ISO

    9277 6100
    15901-2 6100
    15901-3 6100
    18757 6100

    Anton Paar Certified Service

    The Anton Paar quality in service and support:
    • More than 350 manufacturer-certified technical experts worldwide
    • Qualified support in your local language
    • Protection for your investment throughout its lifecycle
    • 3-year warranty
    Learn more

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    P0 COLLAR, AS6X00

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    Part number: 263933

    TYPE A LONG CELL, 9 mm CYL BULB

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    Part number: 257722
    Product details
    Type A long cell with 9 mm stem and cylindrical bulb. Borosilicate glass or equivalent. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 317 mm, cylinder diameter 16 mm, 2.5 cm3 capacity

    P0 CELL, STRAIGHT SM BULB, 323 mm LONG

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    Part number: 239903

    GLASS TUBE, DEGAS COLD TRAP, 325 mm LONG

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    Part number: 237268

    TYPE F CELL, 6 mm MICRO

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    Part number: 193604
    Product details
    Type F micro cell. Borosilicate glass. Nominal Dimensions: 6 mm OD (4 mm ID), cell length 115.5 mm, 0.3 cm3 capacity

    AS6X00, RECIRCULATION DEWAR KIT

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    Part number: 262675
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    Recirculating Dewar and items required to interface a temperature controller bath (not included) with the Autosorb 6X00 series. Includes jacketed Dewar with support base plate to ensure alignment on the dewar lift drive.

    TYPE S CELL, LOOP INJECTOR, QUARTZ

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    Part number: 237269
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    Type S quartz flow cell with 12 mm inlet and 6mm exit. Compatible with the loop injector option on Autosorb 6200/6300 instruments. Quartz for temperatures above 350 C. Nominal Dimensions: Inlet side 12 mm OD (10 mm ID), 250 mm long.

    FLOW DEGASSING KIT, AS6X00

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    Part number: 264190
    Product details
    Accessory kit to allow flow degassing on Autosorb 6X00 instruments. Kit includes a flow rate adjustment line and 6 flow degas adapters, one for each degas port.

    TYPE S ROD, LOOP INJECTOR, QUARTZ

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    Part number: 266121
    Product details
    Non-flared filler rod (cell insert) for the loop injector Type S Cell. Nominal Dimensions: 9 mm diameter, 152 mm long.

    DEWAR FLASK, 3 L

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    Part number: 193659

    TYPE S CELL, THIN FILM

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    Part number: 264532
    Product details
    Specialty large barrel cell for thin films. Borosilicate glass or equivalent. Nominal Dimensions: 12 mm OD (10 mm ID), cell length 307 mm, barrel diameter 24 mm, barrel length 57 mm, 20 cm3 capacity

    DEWAR, 2 L, WITH CLIP AND HANDLE

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    Part number: 235903

    TYPE A CELL, MONOLITH

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    Part number: 264528
    Product details
    Specialty two piece monolith cell. Includes cap and stem. Borosilicate glass or equivalent. Nominal Dimensions: Capillary stem 6 mm OD, cell length 313 mm, chamber diameter 22 mm, chamber depth 38 mm, 14 cm3 capacity

    ASIQ WIDE MOUTH DEWAR ASSEMBLY

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    Part number: 193302

    TYPE A CELL, STOPCOCK

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    Part number: 264529
    Product details
    Specialty two piece stopcock cell. Includes upper section with stopcock, lower section, and 2 spring connectors. Borosilicate glass or equivalent. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 313 mm, bulb diameter 23 mm, 4 cm3 capacity

    LEVEL SENSOR, CLS TYPE, CRYOGEN, OFFSET

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    Part number: 237676
    Product details
    CLS type coolant level sensor for use with liquid argon (87 K) or liquid nitrogen (77 K). Appropriate for use with long cells. Offset geometry compatible with a 3 L Dewar Flask.

    GAS INPUT 1 TO DEGAS CONNECTING LINE FOR AS6X00

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    Part number: 262770
    Product details
    Connection line allowing a gas to be connected to both gas input port 1 and the degas backfill port simultaneously. Compatible with Autosorb 6X00 Instruments.

    HEATING MANTLE, 7 PIN SOCKET, 24 VDC

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    Part number: 226870
    Product details
    Large pocket mantle (4.5 inch internal width) with maximum continuous operating temperature of 450 C (with quartz sample cells). Accomodates up to 3 standard sized cells at one time. Connects to instrument via 7 pin socket connector. Compatible instruments include Autosorb 6X00 and Nova X00 models

    AS6X00 ANALYSIS DEWAR LID, 6 mm CELLS

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    Part number: 237270

    AS6X00 ANALYSIS DEWAR LID, 9 mm CELLS

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    Part number: 237687

    AS6X00 ANALYSIS DEWAR LID, 12 mm CELLS

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    Part number: 237686

    SAFETY COVER, AS6X00

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    Part number: 236813
    Product details
    Replacement safety cover for Autosorb 6x00 Instrument Models

    INPUT LINE, 5 FEET, STAINLESS STEEL MALE

    Compatible with:
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    Part number: 194975

    GAS INPUT LINE, 5 FEET, STAINLESS STEEL

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    Part number: 193192

    CRYOGEN MEASURING STICK

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    Part number: 262788

    SAMPLE EXTRACTION HOOK

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    Part number: 193531
    Product details
    Gancho para extração de amostras

    BALANCE CELL HOLDER TYPE E LONG CELL

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    Part number: 259408

    FITTING PTC 6 mm TUBE X 1/4 NPT

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    Part number: 259818

    PUMP SILENCER G 1/8

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    Part number: 235977
    Product details
    Reduces noise by reducing air velocity at the pump exhaust outlet.
    - Temperature range: -10 to +70 C
    - Material of silencer insert: PE
    - Pneumatic connection: G 1/8

    TUBING POLYURETHANE OD 6 mm

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    Part number: 235901

    TYPE A CELL, STOPCOCK, LOWER

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    Part number: 264531
    Product details
    Replacement lower section for Type A Cell, Stopcock.

    BULKHEAD SPANNER WRENCH

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    Part number: 196453

    TYPE A CELL, STOPCOCK, UPPER

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    Part number: 264530
    Product details
    Replacement upper section for Type A Cell, Stopcock. Includes Stopcock.

    TYPE E LONG CELL, 12 mm, QUARTZ

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    Part number: 193643
    Product details
    Type E quartz flow cell with 12 mm inlet and 6mm exit. Nominal Dimensions: Inlet side 12 mm OD (10 mm ID), 250 mm long.

    TYPE E ROD, FOR 12 mm LONG QUARTZ CELL

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    Part number: 193644
    Product details
    Non-flared filler rod (cell insert) for 12 mm, quartz type E flow cells. Nominal Dimensions: 9 mm diameter, 190 mm long.

    O-RING, EPDM 12 mm, PURPLE, PACK OF 2

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 193831

    VOLUME / VAPOR CELL 13 cm3

    Compatible with:
    Autosorb 6100 | 6200 | 6300
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    Part number: 193657

    FUNNEL, LONG STEM GLASS, 9/12 mm CELLS

    Compatible with:
    Autosorb 6100 | 6200 | 6300
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    Part number: 193663

    TYPE A ROD, FOR 9 mm LONG CELL

    Compatible with:
    Autosorb 6100 | 6200 | 6300
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    Part number: 193927
    Product details
    Flared filler rod (cell insert) for 9 mm, long, type A cells. Nominal Dimensions: 6 mm diameter, 290 mm long

    VACUUM GREASE .25 OUNCE

    Compatible with:
    Autosorb 6100 | 6200 | 6300
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    Part number: 193946

    SAMPLE CELL ADAPTOR, 6 mm

    Compatible with:
    Autosorb 6100
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    Part number: 193362

    O-RING, EPDM 6 mm, PURPLE, PACK OF 2

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 193832

    ChemBET REPLACEMENT FURNACE, 115 V

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 240770

    FURNACE CABLE

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 236567

    FURNACE HEAT SHIELD

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 197677

    O-RING, EPDM 9 mm, PURPLE, PACK OF 2

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 193833

    CALIBRATION SYRINGE, 0.50 mL

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 193942

    SYRINGE 2 INCH SIDE PORT .018X.008

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 197853

    PTC 8 MM TO 1/8" ADAPTER

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 217226
    Product details
    Push-to-connect tubing adapter used in certain Autosorb configuration as an adapter for backing pump exhaust lines

    CHEMSORB FURNACE POWER

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 197477

    O-RING, PFE 12 mm, BLACK

    Compatible with:
    Autosorb 6300
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    Part number: 193836

    THERMOCOUPLE, AS6X00 TCD

    Compatible with:
    Autosorb 6300
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    Part number: 267130

    TITRATION LOOP ADAPTER

    Compatible with:
    Autosorb 6300
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    Part number: 289445

    TYPE B SHORT CELL, 9 mm SM BULB

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 193880
    Product details
    Type B short cell with 9 mm stem and small bulb. Borosilicate Glass. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 151 mm, bulb diameter 16 mm, 1 cm3 capacity.

    DEWAR LID, AS6X00 TCD COLD TRAP

    Compatible with:
    Autosorb 6300
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    Part number: 246760

    O-RING, PFE 6 mm, BLACK

    Compatible with:
    Autosorb 6300
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    Part number: 193837

    GAS INPUT LINE, 5 FEET, STAINLESS STEEL WITH QUICK CONNECT

    Compatible with:
    Autosorb 6300
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    Part number: 193193

    O-RING, PFE 9 mm, BLACK

    Compatible with:
    Autosorb 6300
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    Part number: 193838

    SEPTUM [PACK OF 2]

    Compatible with:
    Autosorb 6200 | 6300
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    Part number: 193668

    NUT & FERRULE, 1/8 INCH STAINLESS STEEL

    Compatible with:
    Autosorb 6300
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    Part number: 193194
    Product details
    Porca e anilha, 1/8 polegada, Inox

    DEWAR, 350 mL

    Compatible with:
    Autosorb 6300
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    Part number: 193629

    CryoSync ACCESSORY, AS6X00

    Compatible with:
    Autosorb 6100 | 6200 | 6300
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    Part number: 237832
    Product details
    Cryogenic temperature control accessory. Includes one Cryosync Cooler, and associated items to run cryogenic analyses on one analysis station. Must be paired with the AS6X00, CryoSync Control Option.
    - Temperature stability better than +/-0.005K
    - Analysis duration greater than 50 hours at 87K
    - Full operating temperature range 82K to 115K

    Cryostat Accessory for autosorb iQ:
    CryoSync 

    Compatible with:
    Autosorb 6100
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    Product details
    • Wide temperature range (82 K to >115 K)
    • Precise temperature control (temp. stability < ±0.005 K S.D.)
    • Perfect for argon isotherm measurements without using liquid argon or for multi-isotherm heat of adsorption experiments
    • Runs for over 50 hours without refilling

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