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High vacuum physisorption/chemisorption analyzers:
autosorb iQ

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Model:
  • Workhorse high vacuum physisorption analyzer
  • For measurement of BET surface areas, micropores, and mesopores
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autosorb iQ Contact

Driven by decades of experience in gas sorption, the autosorb iQ series performs the most challenging measurements of non-porous, mesoporous, and microporous materials with accuracy and precision. Capable of determining specific surface areas below 0.01 m2/g, active areas, pore volumes, and pore size distributions down to 0.35 nm of porous solids in compliance with more than 20 ASTM, DIN, and ISO standard test methods, the autosorb iQ is your gateway to intelligent particle analysis.

Key features

Active coolant level control for sensitivity, accuracy and reproducibility

Active coolant level control for sensitivity, accuracy and reproducibility

Coolant level control is critical for physisorption analyzers to obtain accurate and reproducible results when dealing with evaporative coolants like liquid nitrogen. Rather than relying on passive wicking systems or empirical corrections, the autosorb iQ series combines a 90+ hour analysis Dewar, a coolant-level sensor, and a responsive elevator in an advanced active coolant level control system that ensures highly sensitive and accurate measurements regardless of analysis time.

Integrated and highly precise sample preparation

Integrated and highly precise sample preparation

Precisely prepared samples are the foundation of accurate analysis data. Four built-in degassing stations with access to analysis-quality levels of vacuum through a dedicated cold trap ensure that even the most difficult microporous samples are properly prepared for analysis. User-flexible programming of test protocols, including a pressure rise limit and test for completion methods, minimize elutriation and steaming damage to susceptible samples.

Peer-reviewed data reduction methods

Peer-reviewed data reduction methods

The software includes a comprehensive and peer-reviewed DFT method library. These proprietary data reduction methods developed in conjunction with academic partners, like our unique Quenched Solid Density Functional Theory (QSDFT) methods, deliver reliable and accurate pore size distributions.

Analysis flexibility and adaptability

Analysis flexibility and adaptability

autosorb iQ instruments have been designed to be the most flexible, versatile, and customizable physisorption and chemisorption analyzers on the market. You can upgrade to 2 or 3 analysis stations for up to 2 or 3 times the physisorption throughput. Each additional analysis station comes with its own dedicated transducer set, allowing maximum flexibility in analysis conditions without compromising speed or performance. Capabilities can be further expanded to include a built-in vapor source, additional gas inputs, and much more. 

Technical specifications

autosorb iQ series
Physisorption analysis stations 1, 2, or 3
Chemisorption analysis stations (-C models) 1
Construction
  • Metal-to-metal seals in critical measurement zones
  • Choice of EPDM, Viton, PFE elastomers
Adsorbates N2, Ar, Kr, CO2, O2, H2, etc.
Analysis dewar 3 L, 90+ hours (liquid nitrogen)
Cryogen level control Active sensor/elevator
Saturation pressure measurement Dedicated cell with dedicated transducer
Chemisorption furnace (-C models)
  • Maximum temperature: 1100 °C
  • Ramp rates: 1 °C to 50 °C per minute
  • Furnace cooling by built-in fan
Dosing modes Target p/p0 with:
  • MaxiDose (automatically adapts to individual sample’s sorption characteristics)
  • VectorDose (fixed volumes in multiple ranges) DoseWizard (uses prior analysis as template)
Void volume modes
  • Automatically measure and re-measure during analysis
  • Re-use value already measured
  • Helium-free method
1/0.1 torr transducer accuracy (MP/XR) <0.15 % of reading*
Vacuum system (MP/XR)
  • Turbomolecular drag pump and dry backing pump
  • Ultimate vacuum: 5 x 10-10 mbar*
p/p0 Range (XR using nitrogen/argon) 10-8 to 0.999
Minimum surface area 0.01 m2/g**
Minimum pore size 0.35 nm**
Degassing
  • Four dedicated and built-in degassing ports
  • Operate simultaneously with analysis up to 450 °C with quartz mantles/glassware
  • Vacuum level monitored with Pirani
Physical and utilities

Width: 699 mm (28 inches)
Height: 1035 mm (41 inches)
Depth: 705 mm (28 inches)
Weight: 148 kg (325 pounds)
Electrical: 100 VAC to 240 VAC, 50/60 Hz, single phase
Controller: PC with Windows 7 or newer. 64-bit compatible software

*Manufacturers' specification
**Dependent on analysis gas and temperature

Standards

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ASTM

B922
C1069
C1274
D1993
D3663
D3908
D4222
D4365
D4641
D4780
D4824
D6556

DIN

66134
66135-1
66135-2
66135-3
66135-4

ISO

9277
15901-2
15901-3
18757

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  • More than 350 manufacturer-certified technical experts worldwide
  • Qualified support in your local language
  • Protection for your investment throughout its lifecycle
  • 3-year warranty
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Consumables & Accessories

Consumables & Accessories

Accessories

Accessories

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O-RING, VITON 116, BROWN, PACK OF 2

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Part number: 193816

O-RING, EPDM 010, PURPLE, PACK OF 2

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Part number: 193826

TYPE B ROD, FOR 9 mm LONG DIMPLE LG CELL

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Part number: 193900
Product details
Non-flared filler rod (cell insert) for 9 mm, long, large bulb dimpled, type B cells. For use with non-elutriating cell kit. Nominal Dimensions: 6 mm diameter, 239 mm long.

Vacuum Pump Oil, Edwards, 1 L

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Part number: 196521

NON-ELUTRIATING PLUG, 12MM, METAL, BUNA

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Part number: 222961
Product details
Non-elutriating plug for use with 12mm OD (10mm ID) sample cells. Metal body incorporates 20micron metal frit filter.

CELL-SEAL, 12MM, BUNA

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Part number: 222959
Product details
Valved insert for 12mm OD (10mm ID) cells. Allows transfer of sensitive samples from degasser to analysis station without risk of exposing sample to atmosphere. Automatically opens when inserted into bulkhead fitting. Includes actuator (opener). Metal body incoporates 20micron metal frit filter.

NON-ELUTRIATING PLUG, 9MM, METAL, BUNA

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Part number: 222937
Product details
Non-elutriating plug for use with 9mm OD (7mm ID) sample cells. Metal body incorporates 20micron metal frit filter.

CELL-SEAL, 9MM, BUNA

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Part number: 222935
Product details
Valved insert for 9mm OD (7mm ID) cells. Allows transfer of sensitive samples from degasser to analysis station without risk of exposing sample to atmosphere. Automatically opens when inserted into bulkhead fitting. Includes actuator (opener). Metal body incorporates 20micron metal frit filter.

NON-ELUTRIATING PLUG, 9 mm

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Part number: 193256
Product details
Replacement non-elutriating plug for use with 9 mm OD (7 mm ID) sample cells.

NON-ELUTRIATING PLUG, 6 mm

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Part number: 193257
Product details
Replacement non-elutriating plug for use with 6 mm OD (4 mm ID) sample cells.

SAMPLE CELL ADAPTOR, 6 mm

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Part number: 193362

VACUUM HOSE ASSEMBLY, 5' (1.5 M)

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Part number: 221014
Product details
For connecting to an external vacuum pump. Includes 5 foot (1.5 meter) length of 3/4 inch (1.9 cm) diameter reinforced vacuum hose, 16KF flanges, centering rings and clamps.

SAMPLE CELL ADAPTOR, 9 mm

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Part number: 193363

SAMPLE CELL ADAPTOR, 12 mm

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Part number: 193364

Sample Funnel For 6/9/12 mm 6mm Opening

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Part number: 193369
Product details
lt.Zg. E87M00001/A Material: POM-H RS SCHWARZ

SURFACE AREA REFERENCE MATERIAL, 2003

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Part number: 193439
Product details
Surface area reference material catalog number 2003 for gas sorption instruments. Aluminum oxide powder with 0.5 m2/g nominal BET surface area using nitrogen or krypton.

TYPE A LONG CELL, 6 mm SM BULB, QUARTZ

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Part number: 197846
Product details
Type A long cell with 6 mm stem and small bulb. Quartz for temperatures above 350 C. Nominal Dimensions: 6 mm OD (4 mm ID), cell length 317 mm, bulb diameter 11 mm, 1 cm3 capacity.

TYPE D CELL, 9 mm CYLINDRICAL BULB

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Part number: 197844
Product details
Type D long cell with 9 mm stem and cylindrical bulb. Borosilicate glass Nominal Dimensions: 9 mm OD (7 mm ID), cell length 267 mm, bulb diameter 16 mm, 2.5 cm3 capacity.

SURFACE AREA REFERENCE MATERIAL, 2005

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Part number: 193441
Product details
Surface area reference material catalog number 2005 for gas sorption instruments. Aluminum oxide pellets with 105 m2/g nominal BET surface area using nitrogen.

TYPE D CELL, 6 mm CYLINDRICAL BULB

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Part number: 197843
Product details
Type D long cell with 6 mm stem and cylindrical bulb. Borosilicate glass Nominal Dimensions: 6 mm OD (4 mm ID), cell length 267 mm, bulb diameter 16 mm, 2.5 cm3 capacity.

SURFACE AREA REFERENCE MATERIAL, 2009

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Part number: 193443
Product details
Surface area reference material catalog number 2009 for gas sorption instruments. Silica-Alumina powder with 30 m2/g nominal BET surface area using nitrogen.

SURFACE AREA REFERENCE MATERIAL, 2012

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Part number: 193445
Product details
Surface area reference material catalog number 2012 for gas sorption instruments. 0.5 nm zeolite powder with 750 m2/g nominal BET surface area using nitrogen.

DOWEL PIN, 12 mm

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Part number: 197827

DOWEL PIN, 6 mm

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Part number: 197598

LEVEL SENSOR, HYBRID TYPE, 87 K, LONG

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Part number: 197483
Product details
Hybrid type coolant level sensor for use with liquid argon (87 K). Appropriate for use with long cells.

VCR GASKET, 1/4 INCH, AG

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Part number: 196507
Product details
316 SS VCR Face Seal Fitting. 1/4 inch Silver-plated gasket non-retainer assembly (per unit)

TYPE C MACRO CELL, CAP

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Part number: 193624
Product details
Type C macro cell cap. Must be used with Type C macro cell stem

LEVEL SENSOR, HYBRID TYPE, 77 K, LONG

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Part number: 195455
Product details
Hybrid type coolant level sensor for use with liquid nitrogen (77 K). Appropriate for use with long cells.

COLD TRAP TUBE

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Part number: 193628

DEWAR, 350 mL

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Part number: 193629

DOWEL PIN, 9 mm

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Part number: 194983

FOAM SAMPLE CELL HOLDER FOR BALANCE

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Part number: 194981

VOLUME / VAPOR CELL 13 cm3

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Part number: 193657

TYPE C LONG CELL, THIN FILM

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Part number: 193660

FUNNEL, LONG STEM GLASS, 9/12 mm CELLS

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Part number: 193663

VACUUM GREASE .25 OUNCE

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Part number: 193946

ASIQ P0 CELL

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Part number: 193928

SEPTUM [PACK OF 2]

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Part number: 193668

TYPE A ROD, FOR 12 mm LONG CELL

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Part number: 193925
Product details
Flared filler rod (cell insert) for 12 mm, long, type A cells. Nominal Dimensions: 9 mm diameter, 285 mm long.

VACUUM PUMP OIL, PFEIFFER, 1 L

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Part number: 193678

TYPE A LONG CELL, 9 mm NO BULB, QUARTZ

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Part number: 193924
Product details
Type A long cell with 9 mm stem and no bulb. Quartz for temperatures above 350 C. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 312.5 mm, 1 cm3 capacity.

SAMPLE CELL CAP, FOR 6/9/12 mm STEMS

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Part number: 193680

TYPE A LONG CELL, 9 mm LG BULB, QUARTZ

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Part number: 193921
Product details
Type A long cell with 9 mm stem and large bulb. Quartz for temperatures above 350 C. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 312.5 mm, bulb diameter 23 mm, 4 cm3 capacity.

TYPE A LONG CELL, 9 mm LG BULB, DIMPLE

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Part number: 193919
Product details
Type A long cell with 9 mm stem, large bulb, and dimple. For use with non-elutriating kits. Borosilicate Glass. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 312.5 mm, bulb diameter 23 mm, 4 cm3 capacity.

STEM CLEANER, 18 INCH [PACK OF 18]

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Part number: 193684

TYPE A LONG CELL, 6 mm SM BULB, DIMPLE

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Part number: 193917
Product details
Type A long cell with 6 mm stem, small bulb, and dimple. For use with non-elutriating kits. Borosilicate Glass. Nominal Dimensions: 6 mm OD (4 mm ID), cell length 317 mm, bulb diameter 11 mm, 1 cm3 capacity.

TYPE A LONG CELL, 6 mm SM BULB

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Part number: 193916
Product details
Type A long cell with 6mm stem and small bulb. Borosilicate Glass. Nominal Dimensions: 6 mm OD (4 mm ID), cell length 317 mm, bulb diameter 11 mm, 1 cm3 capacity.

TYPE A LONG CELL, 6 mm LG BULB, QUARTZ

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Part number: 193915
Product details
Type A long cell with 6 mm stem and large bulb. Quartz for temperatures above 350 C. Nominal Dimensions: 6 mm OD (4 mm ID), cell length 317 mm, bulb diameter 23 mm, 4 cm3 capacity.

O-RING, BUNA 010, BLACK, PACK OF 2

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Part number: 193783

TYPE A LONG CELL, 6 mm LG BULB, DIMPLE

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Part number: 193914
Product details
Type A long cell with 6mm stem, large bulb, and dimple. For use with non-elutriating kits. Borosilicate Glass. Nominal Dimensions: 6 mm OD (4 mm ID), cell length 317 mm, bulb diameter 23 mm, 4 cm3 capacity.

O-RING, BUNA 015, BLACK, PACK OF 2

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Part number: 193786

TYPE A LONG CELL, 12 mm LG BULB, DIMPLE

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Part number: 193911
Product details
Type A long cell with 12 mm stem, large bulb, and dimple. For use with non-elutriating kits. Borosilicate Glass. Nominal Dimensions: 12 mm OD (10 mm ID), cell length 308 mm, bulb diameter 23 mm, 4 cm3 capacity.

TYPE A LONG CELL, 12 mm LG BULB

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Part number: 193910
Product details
Type A long cell with 12 mm stem and large bulb. Borosilicate Glass. Nominal Dimensions: 12 mm OD (10 mm ID), cell length 308 mm, bulb diameter 23 mm, 4 cm3 capacity.

TYPE A LONG CELL, 12 mm NO BULB

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Part number: 193909
Product details
Type A long cell with 12 mm stem and no bulb. Borosilicate Glass. Nominal Dimensions: 12 mm OD (10 mm ID), cell length 308 mm, 1.8 cm3 capacity.

TYPE S ROD, FOR CRYOCOOLER SHORT CELL

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Part number: 193907
Product details
Flared filler rod (cell insert) for 9 mm, short, type S cells. Nominal Dimensions: 6 mm diameter, 130 mm long.

O-RING, VITON 010, BROWN, PACK OF 2

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Part number: 193808

TYPE B ROD, FOR 9 mm SHORT CELL

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Part number: 193903
Product details
Flared filler rod (cell insert) for 9 mm, short, type B cells. Nominal Dimensions: 6 mm diameter, 132 mm long.

O-RING, VITON 12 mm, BROWN, PACK OF 2

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Part number: 193817

O-RING, VITON 6 mm, BROWN, PACK OF 2

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Part number: 193820

O-RING, VITON 9 mm, BROWN, PACK OF 2

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Part number: 193821

O-RING, EPDM 12 mm, PURPLE, PACK OF 2

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Part number: 193831

TYPE C ROD, FOR 12 mm LONG CELL

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Part number: 193873
Product details
Flared filler rod (cell insert) for 12 mm, long, type C cells. Nominal Dimensions: 9 mm diameter, 231 mm long.

O-RING, EPDM 6 mm, PURPLE, PACK OF 2

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Part number: 193832

O-RING, EPDM 9 mm, PURPLE, PACK OF 2

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Part number: 193833

O-RING, PFE 12 mm, BLACK

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Part number: 193836

O-RING, PFE 6 mm, BLACK

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Part number: 193837

P0 CELL, BENT SM BULB, 306 mm LONG

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Part number: 193851

O-RING, PFE 9 mm, BLACK

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Part number: 193838

QUARTZ WOOL, PACK OF 2.5 g

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Part number: 193227

TYPE E LONG CELL, 12 mm, QUARTZ

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Part number: 193643
Product details
Type E quartz flow cell with 12 mm inlet and 6mm exit. Nominal Dimensions: Inlet side 12 mm OD (10 mm ID), 250 mm long.

TYPE B SHORT CELL, 9 mm SM BULB

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Part number: 193880
Product details
Type B short cell with 9 mm stem and small bulb. Borosilicate Glass. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 151 mm, bulb diameter 16 mm, 1 cm3 capacity.

TYPE A LONG CELL, 6 mm LG BULB

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Part number: 193913
Product details
Type A long cell with 6 mm stem and large bulb. Borosilicate Glass. Nominal Dimensions: 6 mm OD (4 mm ID), cell length 317 mm, bulb diameter 23 mm, 4 cm3 capacity.

TYPE A LONG CELL, 9 mm LG BULB

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Part number: 193918
Product details
Type A long cell with 9 mm stem and large bulb. Borosilicate Glass. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 312.5 mm, bulb diameter 23 mm, 4 cm3 capacity.

TYPE A LONG CELL, 9 mm NO BULB

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Part number: 193922
Product details
Type A long cell with 9 mm stem and no bulb. Borosilicate Glass. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 312.5 mm, 1 cm3 capacity.

TYPE A ROD, FOR 6 mm LONG CELL

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Part number: 193926
Product details
Flared filler rod (cell insert) for 6 mm, long, type A cells. Nominal Dimensions: 3 mm diameter, 295 mm long

TYPE A ROD, FOR 9 mm LONG CELL

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Part number: 193927
Product details
Flared filler rod (cell insert) for 9 mm, long, type A cells. Nominal Dimensions: 6 mm diameter, 290 mm long

Cryostat accessory for autosorb iQ:
CryoSync 

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Product details
  • Wide temperature range (82 K to >115 K)
  • Precise temperature control (temp. stability < ±0.005 K S.D.)
  • Perfect for argon isotherm measurements without using liquid argon or for multi-isotherm heat of adsorption experiments
  • Runs for over 50 hours without refilling

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TYPE C MACRO CELL, STEM

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Part number: 193625
Product details
Type C Macro cell stem. Must be used with Type C macro cell cap