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High Vacuum Physisorption Analyzer:
Autosorb

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Model:
  • Full chemisorption and physisorption capabilities in a single instrument package
  • Enhanced chemical resistance allows a wider range of analysis gases and applications
  • Perform a complete catalyst characterization with the included TCD, pulse titration loop, and built-in vapor source
Autosorb Contact

Autosorb instruments are high vacuum physisorption and chemisorption analyzers designed for advanced measurements of BET surface area, active area, and pore size distributions. Independent analysis stations, exclusive TruZone active coolant control, and accessible Kaomi software let you meet your current measurement needs, while factory and field upgradeable options let you adapt to future ones. For your most important gas sorption measurements, the choice is clear: Absolutely Autosorb.

Key features

A gas sorption analyzer that’s absolutely accurate

A gas sorption analyzer that’s absolutely accurate

  • Get highly accurate physisorption measurements from relative pressures below 10-7 for nitrogen 
  • Leverage precise manifold temperature control between 35 °C and 50 °C
  • Rely on TruZone active coolant level control for accurate data – even over lengthy analyses
  • Achieve superior high vacuum performance (38 % better than previous generation instruments) with precision-machined manifolds and high-quality pneumatic valves 
Independent stations ensure you’re absolutely agile

Independent stations ensure you’re absolutely agile

  • Analyze up to three different samples with three different analysis gases at three different temperatures simultaneously with independent analysis stations and patented temperature control accessories
  • Perform the most challenging physisorption measurements with the 90-hour Dewar
  • Maximize your throughput with six integrated degassing stations
  • Quickly swap to the 1100 °C furnace for advanced temperature programmed analyses, pulse titrations, or chemisorption isotherms 
Intuitive software makes every analysis absolutely accessible

Intuitive software makes every analysis absolutely accessible

  • Enjoy an updated and streamlined Kaomi software, which makes the whole measurement process easier than ever before
  • Optimize measurement definition to suit your needs with DoseWizard’s new standard and advanced modes
  • Keep downtime to a minimum with PowderProtect, which prevents accidental loss of powder in the instrument
Customization options keep you absolutely adaptable

Customization options keep you absolutely adaptable

  • With 3 instruments and modular upgrades, the Autosorb adapts to the exact analysis requirements of your porous solids and catalysts
  • As your research changes, the instrument’s physisorption and chemisorption features can be field upgraded to fit new materials and applications
  • Go beyond standard measurements with enhanced chemical resistance, a built-in vapor source, thermal conductivity detector, or even a fully integrated mass spectrometer
Compliance and quality are absolutely assured

Compliance and quality are absolutely assured

  • Comply with 20+ ASTM, DIN, and ISO standards for catalyst characterization and the evaluation of porous solids. 
  • Get peace of mind with our 3-year warranty so you can avoid unforeseen costs 

Technical specifications

Measurement Specifications

 

  Autosorb 6100 Autosorb 6200 Autosorb 6300
Measurement principle
  • Vacuum Volumetric Physisorption
  • Vacuum Volumetric Physisorption
  • Vacuum Volumetric Chemisorption
  • Dynamic Flow Chemisorption (Optional)
  • Vacuum Volumetric Physisorption
  • Vacuum Volumetric Chemisorption
  • Dynamic Flow Chemisorption
Analysis gas compatibility      
N2, Ar, Kr, CO2, H2, and other non-corrosive gases Included Included Included
CH4, C2H6, C3H8, other alkanes, C6H6, C8H10 Included Dependent on instrument configuration Included
NH3, C5H5N, C3H6O, and other reactive gases N/A Dependent on instrument configuration Included
Physisorption analysis stations Number: 1, 2, or 3
Independence: Up to 3 gases at 3 analysis temperatures can be used concurrently, 
1 analysis gas and temperature per station
Chemisorption analysis stations N/A 1
Independent p0 station Yes (dedicated cell and transducer)
Pressure
  • Range: 2x10-5 to 1100 Torr (2.6x10-8 to 0.997 p/p0 for N2 77K)
  • Resolution (MP): 2x10-5 Torr (2.6x10-8 p/p0 for N2 77K)
  • Resolution (XR): 1x10-6 Torr (1.3x10-9 p/p0 for N2 77K)
BET surface area
  • Absolute detection limit: 0.1 m2 (N2 77K)
  • Specific detection limit: 0.01 m2/g (N2 77K)
  • Typical reproducibility: 1 % (measured on BAM P115)
  • Reproducibility limit: 2 % with 2 m2 in the cell
Pore size
  • Range: 0.35 nm to 500 nm (diameter)
  • Typical reproducibility: 0.5 % (measured on BAM P115)
Active area N/A
  • Absolute detection limit: 0.03 m2 (H2 on Platinum 313 K)
  • Specific detection limit: 0.003 m2/g (H2 on Platinum 313K)
  • Typical reproducibility: 2 % (measured on 2% Platinum on Alumina reference sample)
TruZone Yes (active coolant level control)
PowderProtect Yes (prevents sample elutriation)
Analysis dewar
  • Duration: 90+ hours with liquid nitrogen
  • Refill during analysis: Yes
  • Volume: 3 L
Analysis furnace N/A
  • Maximum temperature: 1,100 °C
  • Maximum Ramp Rate: 50 °C per minute
  • Furnace cooling by built-in fan
Sample preparation
  • Integrated degassing stations: 6
  • Temperature control: 2 independent heating zones, ambient to 450 °C
  • Dedicated cold trap: Yes
  • Available methods: flow and vacuum, programmable multi-step degassing profiles, test for completion routines, pressure-controlled heating
Additional capabilities      
Vapor source Optional Optional Included
CryoSync control  Optional Optional Optional
TCD and loop injector N/A Optional Included
Mass spectrometer N/A Optional Optional

 

Kaomi software features

 

  Autosorb 6100 Autosorb 6200 Autosorb 6300
Instrument connection Control up to 4 instruments from 1 PC
DoseWizard
  • 45+ built-in analysis profiles aligned with ASTM, DIN, and ISO
  • Standard profiles with easy measurement selection
  • Advanced profiles with full control of experimental procedures 
  • Dose templates for rapid measurement based on previous analyses
Physisorption methods
  • Surface area and pore volume: Alpha-s, BET, DR, Gurvich pore volume, Langmuir, t-plot (STSA)
  • Pore size and pore volume distributions: NLDFT, QSDFT, GCMC, Kr(87) thin-film, BJH, DH, DA, HK, SF, MP
  • Other: summary reports, overlays, average particle size, average pore size, fractal dimensions (NK, FHH), heat of adsorption
Chemisorption methods N/A
  • Static measurements: extrapolation, bracketing, Langmuir, Temkin, Freundlich, heat of adsorption
  • Dynamic flow measurements: TPx (TPR,TPO,TPD) peak deconvolution, pulse titration analysis, activation energy
Available languages     Chinese, English, French, German, Japanese, Korean, Portuguese, Spanish

 

Technical Specifications

 

  Autosorb 6100 Autosorb 6200 Autosorb 6300
Dimensions (W x D x H) 79.5 cm x 70.1 cm x 107.9 cm (31.3 in x 27.6 in x 42.5 in) dependent on instrument configuration
Weight 136.4 kg (300 lbs) dependent on instrument configuration
Operating environment
  • Temperature: 15 °C to 35 °C (59 °F to 95 °F)
  • Humidity: 20% RH to 80% RH, non-condensing
Gas distribution manifold elastomers FKM FKM or EPDM (dependent on instrument configuration) PFE
Analysis manifold construction Vacuum-brazed manifold block in stainless steel
Analysis manifold temperature
  • Range: user adjustable 35 °C to 50 °C
  • Stability: ±0.05 °C
Analysis manifold valves
  • Type: stainless steel, air-operated bellows valve
  • Cycle life: 5,000,000 cycles
  • External leak rate: 5x10-12 Pa m3/sec
  • Seat leak rate: 5x10-12 Pa m3/sec
Pressure transducer (1550 Torr) 
-Analysis and degas
  • Number: 3 to 5 (dependent on instrument configuration)
  • Accuracy: ±0.1 % of span typical, ±0.15 % of span maximum
  • A/D data acquisition: 32 bit
Pressure transducer (10 Torr)
– MP or XR
  • Number: 1 to 3 (dependent on instrument configuration)
  • Accuracy: ±0.15 % reading up to 10 Torr
  • Resolution: 0.002 % full scale
Pressure transducer (1 Torr)
– MP only
  • Number: 1 to 3 (dependent on instrument configuration)
  • Accuracy: ±0.15 % reading up to 1 Torr
  • Resolution: 0.002 % full scale
Pressure transducer (0.1 Torr)
– XR only
  • Number: 1 to 3 (dependent on instrument configuration)
  • Accuracy: ±0.15 % reading up to 0.1 Torr
  • Resolution: 0.001 % full scale
Pirani vacuum gauge
– Degas only
  • Number: 1
  • Accuracy:
    5×10-4 to 1x10-3 Torr: ±10 % of reading
    1×10-3 to 100 Torr: ±5 % of reading
  • 100 Torr to atmosphere: ±25 % of reading
Vacuum system
  • Turbo molecular drag pump and dry diaphragm pump
  • Manufacturer’s specification: 5x10-10 mbar
  • Typical pressure at analysis port: 2.67x10-5 mbar
Thermal conductivity detector (TCD) N/A
  • Two-filament TCD with rhenium/tungsten filaments (optional)
  • Detection Limit: 0.5 uL (air injected into helium)
  • Two-filament TCD with rhenium/tungsten filaments (standard)
  • Detection Limit: 0.5 uL (air injected into helium)
Gas ports
  • 7 ports standard (5 analysis, 1 helium, 1 degas/backfill)
  • 7 additional analysis ports optional
  • 7 ports standard (5 analysis, 1 helium, 1 degas/backfill)
  • 7 additional analysis ports optional
  • 1 titration gas port optional
  • 15 ports standard (12 analysis, 1 helium, 1 degas/backfill, 1 titration)
Gas supply
  • Purity: 99.999 %
  • Input pressure: 8 psig to 10 psig (0.55 bar to 0.69 bar)
Air
  • Input pressure: 50 psig to 100 psig (3.45 bar to 6.9 bar)
Electrical
  • Supply: 100 to 240 VAC ±10%, 50 or 60Hz
  • Maximum consumption: 1600W (dependent on instrument configuration)
PC connection Ethernet
RoHS3 compliant Yes
CE / UKCA certified Yes
Indoor/outdoor use For indoor use only

Standards

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ASTM

B922 6100, 6200
C1069 6100, 6200
C1274 6100, 6200
D1993 6100
D3663 6100
D3908 6100
D4222 6100
D4365 6100
D4641 6100
D4780 6100
D4824 6100
D6556 6100

DIN

66134 6100
66135-1 6100
66135-2 6100
66135-3 6100
66135-4 6100

ISO

9277 6100
15901-2 6100
15901-3 6100
18757 6100

Anton Paar Certified Service

The Anton Paar quality in service and support:
  • More than 350 manufacturer-certified technical experts worldwide
  • Qualified support in your local language
  • Protection for your investment throughout its lifecycle
  • 3-year warranty
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P0 COLLAR, AS6X00

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Part number: 263933

TYPE A LONG CELL, 9 mm CYL BULB

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Part number: 257722
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Type A long cell with 9 mm stem and cylindrical bulb. Borosilicate glass or equivalent. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 317 mm, cylinder diameter 16 mm, 2.5 cm3 capacity

P0 CELL, STRAIGHT SM BULB, 323 mm LONG

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Part number: 239903

GLASS TUBE, DEGAS COLD TRAP, 325 mm LONG

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Part number: 237268

TYPE F CELL, 6 mm MICRO

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Part number: 193604
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Type F micro cell. Borosilicate glass. Nominal Dimensions: 6 mm OD (4 mm ID), cell length 115.5 mm, 0.3 cm3 capacity

AS6X00, RECIRCULATION DEWAR KIT

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Part number: 262675
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Recirculating Dewar and items required to interface a temperature controller bath (not included) with the Autosorb 6X00 series. Includes jacketed Dewar with support base plate to ensure alignment on the dewar lift drive.

TYPE S CELL, LOOP INJECTOR, QUARTZ

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Part number: 237269
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Type S quartz flow cell with 12 mm inlet and 6mm exit. Compatible with the loop injector option on Autosorb 6200/6300 instruments. Quartz for temperatures above 350 C. Nominal Dimensions: Inlet side 12 mm OD (10 mm ID), 250 mm long.

FLOW DEGASSING KIT, AS6X00

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Part number: 264190
Product details
Accessory kit to allow flow degassing on Autosorb 6X00 instruments. Kit includes a flow rate adjustment line and 6 flow degas adapters, one for each degas port.

TYPE S ROD, LOOP INJECTOR, QUARTZ

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Part number: 266121
Product details
Non-flared filler rod (cell insert) for the loop injector Type S Cell. Nominal Dimensions: 9 mm diameter, 152 mm long.

DEWAR FLASK, 3 L

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Part number: 193659
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Frasco Dewar Fississorção padrão, capacidade 3L. Com alça e tampa

TYPE S CELL, THIN FILM

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Part number: 264532
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Specialty large barrel cell for thin films. Borosilicate glass or equivalent. Nominal Dimensions: 12 mm OD (10 mm ID), cell length 307 mm, barrel diameter 24 mm, barrel length 57 mm, 20 cm3 capacity

DEWAR, 2 L, WITH CLIP AND HANDLE

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Part number: 235903

TYPE A CELL, MONOLITH

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Part number: 264528
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Specialty two piece monolith cell. Includes cap and stem. Borosilicate glass or equivalent. Nominal Dimensions: Capillary stem 6 mm OD, cell length 313 mm, chamber diameter 22 mm, chamber depth 38 mm, 14 cm3 capacity

ASIQ WIDE MOUTH DEWAR ASSEMBLY

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Part number: 193302

TYPE A CELL, STOPCOCK

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Part number: 264529
Product details
Specialty two piece stopcock cell. Includes upper section with stopcock, lower section, and 2 spring connectors. Borosilicate glass or equivalent. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 313 mm, bulb diameter 23 mm, 4 cm3 capacity

LEVEL SENSOR, CLS TYPE, CRYOGEN, OFFSET

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Part number: 237676
Product details
CLS type coolant level sensor for use with liquid argon (87 K) or liquid nitrogen (77 K). Appropriate for use with long cells. Offset geometry compatible with a 3 L Dewar Flask.

GAS INPUT 1 TO DEGAS CONNECTING LINE FOR AS6X00

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Part number: 262770
Product details
Connection line allowing a gas to be connected to both gas input port 1 and the degas backfill port simultaneously. Compatible with Autosorb 6X00 Instruments.

HEATING MANTLE, 7 PIN SOCKET, 24 VDC

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Part number: 226870
Product details
Large pocket mantle (4.5 inch internal width) with maximum continuous operating temperature of 450 C (with quartz sample cells). Accomodates up to 3 standard sized cells at one time. Connects to instrument via 7 pin socket connector. Compatible instruments include Autosorb 6X00 and Nova X00 models

AS6X00 ANALYSIS DEWAR LID, 6 mm CELLS

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Part number: 237270

AS6X00 ANALYSIS DEWAR LID, 9 mm CELLS

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Part number: 237687

AS6X00 ANALYSIS DEWAR LID, 12 mm CELLS

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Part number: 237686

SAFETY COVER, AS6X00

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Part number: 236813
Product details
Replacement safety cover for Autosorb 6x00 Instrument Models

INPUT LINE, 5 FEET, STAINLESS STEEL MALE

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Part number: 194975

GAS INPUT LINE, 5 FEET, STAINLESS STEEL

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Part number: 193192
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Linha de INPUT de gás, 5’ Inox

CRYOGEN MEASURING STICK

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Part number: 262788

SAMPLE EXTRACTION HOOK

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Part number: 193531
Product details
Gancho para extração de amostras

BALANCE CELL HOLDER TYPE E LONG CELL

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Part number: 259408

VACUUM GREASE .25 OUNCE

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Part number: 193946

FITTING PTC 6 mm TUBE X 1/4 NPT

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Part number: 259818

PUMP SILENCER G 1/8

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Part number: 235977
Product details
Reduces noise by reducing air velocity at the pump exhaust outlet.
- Temperature range: -10 to +70 C
- Material of silencer insert: PE
- Pneumatic connection: G 1/8

TYPE A CELL, STOPCOCK, LOWER

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Part number: 264531
Product details
Replacement lower section for Type A Cell, Stopcock.

TUBING POLYURETHANE OD 6 mm

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Part number: 235901

TYPE A CELL, STOPCOCK, UPPER

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Part number: 264530
Product details
Replacement upper section for Type A Cell, Stopcock. Includes Stopcock.

BULKHEAD SPANNER WRENCH

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Part number: 196453

TYPE A ROD, FOR 9 mm LONG CELL

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Part number: 193927
Product details
Flared filler rod (cell insert) for 9 mm, long, type A cells. Nominal Dimensions: 6 mm diameter, 290 mm long

FUNNEL, LONG STEM GLASS, 9/12 mm CELLS

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Part number: 193663

TYPE E ROD, FOR 12 mm LONG QUARTZ CELL

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Part number: 193644
Product details
Non-flared filler rod (cell insert) for 12 mm, quartz type E flow cells. Nominal Dimensions: 9 mm diameter, 190 mm long.

TYPE E LONG CELL, 12 mm, QUARTZ

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Part number: 193643
Product details
Type E quartz flow cell with 12 mm inlet and 6mm exit. Nominal Dimensions: Inlet side 12 mm OD (10 mm ID), 250 mm long.

VOLUME / VAPOR CELL 13 cm3

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Autosorb 6100 | 6200 | 6300
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Part number: 193657

SAMPLE CELL ADAPTOR, 6 mm

Compatible with:
Autosorb 6100
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Part number: 193362

ChemBET REPLACEMENT FURNACE, 115 V

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Autosorb 6200 | 6300
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Part number: 240770

FURNACE CABLE

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Autosorb 6200 | 6300
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Part number: 236567

FURNACE HEAT SHIELD

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Autosorb 6200 | 6300
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Part number: 197677

CALIBRATION SYRINGE, 0.50 mL

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Autosorb 6200 | 6300
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Part number: 193942

SYRINGE 2 INCH SIDE PORT .018X.008

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Autosorb 6200 | 6300
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Part number: 197853

PTC 8 MM TO 1/8" ADAPTER

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Autosorb 6200 | 6300
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Part number: 217226
Product details
Push-to-connect tubing adapter used in certain Autosorb configuration as an adapter for backing pump exhaust lines

CHEMSORB FURNACE POWER

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Autosorb 6200 | 6300
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Part number: 197477

SEPTUM [PACK OF 2]

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Autosorb 6200 | 6300
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Part number: 193668

THERMOCOUPLE, AS6X00 TCD

Compatible with:
Autosorb 6300
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Part number: 267130

O-RING, EPDM 6 mm, PURPLE, PACK OF 2

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Autosorb 6200 | 6300
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Part number: 193832

TITRATION LOOP ADAPTER

Compatible with:
Autosorb 6300
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Part number: 289445

O-RING, EPDM 9 mm, PURPLE, PACK OF 2

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Autosorb 6200 | 6300
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Part number: 193833

DEWAR LID, AS6X00 TCD COLD TRAP

Compatible with:
Autosorb 6300
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Part number: 246760

O-RING, EPDM 12 mm, PURPLE, PACK OF 2

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Autosorb 6200 | 6300
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Part number: 193831

GAS INPUT LINE, 5 FEET, STAINLESS STEEL WITH QUICK CONNECT

Compatible with:
Autosorb 6300
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Part number: 193193

NUT & FERRULE, 1/8 INCH STAINLESS STEEL

Compatible with:
Autosorb 6300
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Part number: 193194
Product details
Porca e anilha, 1/8 polegada, Inox

TYPE B SHORT CELL, 9 mm SM BULB

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Autosorb 6200 | 6300
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Part number: 193880
Product details
Type B short cell with 9 mm stem and small bulb. Borosilicate Glass. Nominal Dimensions: 9 mm OD (7 mm ID), cell length 151 mm, bulb diameter 16 mm, 1 cm3 capacity.

O-RING, PFE 6 mm, BLACK

Compatible with:
Autosorb 6300
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Part number: 193837

O-RING, PFE 9 mm, BLACK

Compatible with:
Autosorb 6300
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Part number: 193838

O-RING, PFE 12 mm, BLACK

Compatible with:
Autosorb 6300
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Part number: 193836

DEWAR, 350 mL

Compatible with:
Autosorb 6300
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Part number: 193629

CryoSync ACCESSORY, AS6X00

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Autosorb 6100 | 6200 | 6300
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Part number: 237832
Product details
Cryogenic temperature control accessory. Includes one Cryosync Cooler, and associated items to run cryogenic analyses on one analysis station. Must be paired with the AS6X00, CryoSync Control Option.
- Temperature stability better than +/-0.005K
- Analysis duration greater than 50 hours at 87K
- Full operating temperature range 82K to 115K

Cryostat Accessory for autosorb iQ:
CryoSync 

Compatible with:
Autosorb 6100
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Product details
  • Wide temperature range (82 K to >115 K)
  • Precise temperature control (temp. stability < ±0.005 K S.D.)
  • Perfect for argon isotherm measurements without using liquid argon or for multi-isotherm heat of adsorption experiments
  • Runs for over 50 hours without refilling

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