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驗證錯誤!

帶原位拉曼光譜的微波反應器:
Monowave 400 R

  • Anton Paar Monowave 400 R microwave synthesis reactor (left) and Cora 5001 Raman spectrometer (right) shown together. The Monowave 400 R features a touchscreen interface for reaction control, while the Cora 5001 provides molecular spectroscopy analysis in real-time.
  • Anton Paar Monowave 400 R microwave synthesis reactor (left) and Cora 5001 Raman spectrometer (right) with an open sample compartment. The Monowave 400 R displays reaction monitoring data on its touchscreen, while the Cora 5001 enables real-time molecular spectroscopy analysis.
  • Computer monitor displaying Raman spectroscopy analysis using Anton Paar Spectroscopy Suite software. The screen shows spectral data, measurement acquisition details, and processing options for molecular composition analysis.
  • Close-up view of the reaction vessel inside the Anton Paar Monowave 400 R microwave synthesis reactor. A red laser spot indicates in-situ Raman spectroscopy measurement, providing real-time molecular analysis during chemical reactions.
  • A scientist in a laboratory places a reaction vial into an Anton Paar Monowave 400 microwave synthesis reactor. Another Monowave 400 is on the lab bench, displaying reaction monitoring data. Several sealed reaction vials are arranged in the foreground.
  • A scientist operates the Anton Paar Monowave 400 R microwave synthesis reactor via its touchscreen, while another scientist works in a laboratory fume hood. The Cora 5001 Raman spectrometer is positioned nearby, displaying molecular spectroscopy data on its screen.
  • Anton Paar Monowave 400 R microwave synthesis reactor (left) and Cora 5001 Raman spectrometer (right) shown together. The Monowave 400 R features a touchscreen interface for reaction control, while the Cora 5001 provides molecular spectroscopy analysis in real-time.
  • Anton Paar Monowave 400 R microwave synthesis reactor (left) and Cora 5001 Raman spectrometer (right) with an open sample compartment. The Monowave 400 R displays reaction monitoring data on its touchscreen, while the Cora 5001 enables real-time molecular spectroscopy analysis.
  • Computer monitor displaying Raman spectroscopy analysis using Anton Paar Spectroscopy Suite software. The screen shows spectral data, measurement acquisition details, and processing options for molecular composition analysis.
  • +3
  • 獲得有關加壓反應化學成分的即時資訊
  • 使用精確的時間 - 溫度曲線來深入了解反應行為
  • 無需清潔,不需進行樣品製備,無交叉污染

將 Monowave 400 R 與 Cora 5001 拉曼光譜儀結合使用,可以從以前的黑匣子中接收光譜資訊。安東帕結合了兩種強大的化學合成技術–微波反應器 Monowave 400 R 提供快速的化學反應,而拉曼分析儀 Cora 5001 則透過分子光譜來定義它們的特性。

透過結合精確的溫度曲線與相關反應混合物的化學組成的即時資訊結合起來,就能更全面地了解反應機制和動力學。根據更深入的洞察力優化反應條件,例如參數的影響、不同試劑的作用或對反應理想終點的檢測。

主要功能

在前所未有的反應條件下研究化學反應

Monowave 400 R 提供全範圍的操作參數,溫度支援最高 300°C,壓力最高 30 bar。Cora 5001 拉曼分析儀直接在反應瓶內利用可調整的間隔和暴露時間進行時間序列的測量。微波反應器和拉曼光譜儀透過一個特殊的光纖拉曼探針相連。

Anton Paar Monowave 400 R microwave synthesis reactor (left) and Cora 5001 Raman spectrometer (right) with an open sample compartment. The Monowave 400 R displays reaction monitoring data on its touchscreen, while the Cora 5001 enables real-time molecular spectroscopy analysis.

即時原位反應監測,可更深入地了解反應機制

拉曼光譜法可直接識別官能基和相關反應混合物組成的定量資訊。透過時間解析的測量檢測不可隔離的中間產物或短壽命過渡狀態,以便更深入地了解反應機制。

適用的應用:

  • 反應中間產物的判定
  • 闡明反應機制
  • 反應動力學研究
  • 副產物形成的監測
  • 反應條件的優化
Computer monitor displaying Raman spectroscopy analysis using Anton Paar Spectroscopy Suite software. The screen shows spectral data, measurement acquisition details, and processing options for molecular composition analysis.

就像每次使用非接觸式測量的新探針一樣

拉曼探針採用散射法,因此可以透過硼矽酸鹽玻璃小瓶的壁面進行操作,以直接監測加壓反應的化學成分。您可以研究從 2 mL 到 20 mL 的各種刻度,因為雷射束的焦點可以針對 Monowave 400 R 所提供兩種尺寸的反應容器進行最佳定位。透過非接觸式測量,避免交叉污染,您可以自由選擇反應物,且無需在實驗之間進行清潔工作。

Close-up view of the reaction vessel inside the Anton Paar Monowave 400 R microwave synthesis reactor. A red laser spot indicates in-situ Raman spectroscopy measurement, providing real-time molecular analysis during chemical reactions.

精確的溫度控制,以確保反應過程具有完美的可重複性

使用微波加熱有許多優點:可以直接加熱反應瓶中的反應混合物,而無需加熱周圍環境。與傳統的加熱源不同,可以立即打開和關閉微波加熱,從而完全控制加熱。Monowave 400 R 利用這些優勢,以無與倫比的速度為不限規模的任何溶劑提供高效率加熱。該儀器的軟體控制器不僅可防止溫度過度上衝,還可以透過精確地匹配所需的溫度程式來促進更清潔的轉換。如此可以加速化學反應,使反應溫度遠高於所用溶劑的沸點。

A scientist in a laboratory places a reaction vial into an Anton Paar Monowave 400 microwave synthesis reactor. Another Monowave 400 is on the lab bench, displaying reaction monitoring data. Several sealed reaction vials are arranged in the foreground.

安全可靠的操作

Monowave 400 R 配備有多個聯鎖系統,因此用戶可以免受微波和雷射輻射的傷害。只有關閉 Monowave 400 R 的旋轉蓋,才能啟動兩個設備。 組合設定滿足 laser class 1 的可達到的曝光極限 (AEL)。

A scientist operates the Anton Paar Monowave 400 R microwave synthesis reactor via its touchscreen, while another scientist works in a laboratory fume hood. The Cora 5001 Raman spectrometer is positioned nearby, displaying molecular spectroscopy data on its screen.

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REACTION VESSEL C30 WIDE NECK ASSEMBLED

此價格基於預付款僅供直接在網路購買,恕不提供儀器安裝及操作訓練等服務。 此報價不含國際運費及關稅。 | 不包括包括 0增值稅
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零件編號: 173574
產品詳情
Single 30 mL wide neck silicon carbide vessel with wide neck with one Snap Cap Wide Neck and one corresponding PTFE Septum Wide Neck. Operation Volume 6-20 mL. 3 Note: For opening of the C30 Wide Neck vessel the use of the Decapper Wide Neck Vessels (Mat. No. 161692) is required.

CAVITY COLLAR

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零件編號: 83212

FILTER DISC D14,8

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零件編號: 84294
產品詳情
Small sintered metal filter inserted at the screw opening of the spill bin (83740). Shows fire retardant properties against escaping hot solvent vapors in case of a vial rupture.

CAVITY INSERT

此價格基於預付款僅供直接在網路購買,恕不提供儀器安裝及操作訓練等服務。 此報價不含國際運費及關稅。 | 不包括包括 0增值稅
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零件編號: 88998

RUBY THERMOMETER

此價格基於預付款僅供直接在網路購買,恕不提供儀器安裝及操作訓練等服務。 此報價不含國際運費及關稅。 | 不包括包括 0增值稅
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零件編號: 89047
產品詳情
Immersing fiber optic probe for accurate measurement of the internal reaction temperature, the operation range is 30 to 300 °C. Optional accessory for Monowave 200, Monowave 400, and Monowave 450. Included: 1 pcs. silicone septum for Ruby Thermometer (20 pcs.), 1 pcs. immersion tube for Ruby Thermometer, 1 pcs. holder for Ruby Therm Not included: PTFE Septum Wide Neck, Immersion Tube short for G30 Wide Neck Note: cannot be used with Monowave 100! Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.

MONOWAVE CONSUMABLES SET STANDARD

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零件編號: 93537
產品詳情
Set of consumables, applicable for Monowave 200, Monowave 400, and Monowave 450, containing: Entry Qty. Mat.No. Item 1 1 pcs. 82724 Reaction Vial G10 (100 pcs) 2 1 pcs. 82723 Reaction Vial G30 (20 pcs) 3 1 pcs. 83214 Snap Cap (20 pcs) 4 5 pcs. 88883 Silicone Septum (20 pcs) 5 10 pcs. 89088 Stir bar 10x3 mm (10 pcs) 6 2 pcs. 165242 Stir Bar oval 15x6mm (10 pcs) 7 1 pcs. 89296 Rack 40 8 1 pcs. 23609 Rack 24 Note: not suitable for Monowave 100! Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.

CONSUMABLES SET MONOWAVE 450 Set of consumables, especially for Monowave 450, but also

此價格基於預付款僅供直接在網路購買,恕不提供儀器安裝及操作訓練等服務。 此報價不含國際運費及關稅。 | 不包括包括 0增值稅
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零件編號: 165856
產品詳情
applicable to Monowave 400, containing: Entry Qty. Mat.No. Item 1 2 pcs 161723 Reaction Vial G30 Wide Neck (10 pcs). 2 2 pcs 161724 Snap Cap G30 Wide neck assembled (10 pcs). 3 2 pcs 161728 PTFE Septum Wide Neck (50 pcs.). 4 2 pcs 165242 Stir Bar oval 15x6mm (10 pcs.). 5 1 pc. 23609 Rack 24 6 1 pc. 161692 vial wide neck decapper Note: not suitable for Monowave 100 and Monowave 200 Glass and quartz parts as well as complete reaction vessels are not covered by the standard warranty.

TEST TUBE RACK 50 mL / 24 POSITIONS

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零件編號: 23609
紅寶石溫度計由紅寶石晶體組成,週期性地由閃光信號燈激發。發光的衰減時間取決於溫度,並且與晶體周圍的溫度有關。

紅寶石溫度計

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產品詳情
  • 測量紅寶石晶體發光的溫度依賴性衰減時間
  • 準確的內部溫度監測可達300°C
  • 即使在極端條件下,也能實現精確控制,且無熱過沖
  • 無需校準、即插即用操作,無電磁干擾

更多資訊

REACTION VIAL WIDE NECK DECAPPER

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零件編號: 161692
產品詳情
Optional simple tool for easy decapping of the G30 Wide Neck reaction vials.