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Microwave reactor:
Monowave

Model:
  • High-speed, closed-vessel microwave chemistry
  • Temperatures of up to 260 °C and pressures of up to 20 bar
  • Tool-free reaction vials for any scale between 0.5 mL and 20 mL
  • Software upgrades for extended operational limits, supplementary features, tools, and accessories 
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The Anton Paar Monowave product line is a series of high-performance monomode microwave reactors designed for small- to medium-scale microwave synthesis.

Attain temperatures up to 300 °C and pressures up to 30 bar with advanced all-the-time safety features for high-speed, high-pressure, high-temperature reactions. Improve productivity and product purity across all applications in research and development laboratories with precise heating profiles. Reduce consumable costs and your environmental footprint by using the reusable vials, caps, and septa.

Visit our world of microwave synthesis to find your optimum reaction conditions and to browse through a database of more than 1000 applications which have been successfully performed in Anton Paar reactors.

Key features

Fast and effective: 24 sequential reactions, unattended

Fast and effective: 24 sequential reactions, unattended

The Autosampler MAS 24 allows 24 unattended reactions, in sequence – saving time, and increasing efficiency. High field density produces fast, uniform heating for all kinds of reactions, up to 300 °C. Powerful stirring of up to 1200 rpm assures temperature homogeneity. The powerful 850 W magnetron adjusts its unpulsed microwave power automatically to the sample. This software-driven self-tuning eliminates any guesswork about sample absorption. Achieve high yields and clean reactions with maximum reproducibility.

The key factor in synthesis: Precise, scalable temperature measurement

The key factor in synthesis: Precise, scalable temperature measurement

Current scientific practice is to use reaction temperature as the relevant parameter in microwave reactions. And accurate measurement of the reaction temperature is the key to correct transferal and scale-up of reaction protocols between different reactors. Monowave reactors measure the temperature via an IR temperature sensor – a robust and reliable method for temperature control ensuring absolutely precise temperature measurement. For accurate control of even more demanding reactions, such as an exothermic reactions, or those involving extremely sensitive samples, simultaneous internal temperature measurement with the optional fiber-optic ruby thermometer is available.

Vials for heating any solvent and any reaction mixture

Vials for heating any solvent and any reaction mixture

In addition to the standard glass vials, silicon carbide (SiC) vessels are available. They absorb microwave energy efficiently, while shielding the interior from microwave radiation – a method that reveals microwave effects caused by selective absorption, and allows comparison between direct microwave heating and conventional heating of reaction mixtures. All parameters, such as the heating and cooling rate, the form factor of the reaction vessel, and the stirring efficiency are identical, apart from the heating mode. All solvents, from non-absorbing ones such as hexane to excellent absorbers such as ionic liquids, can be heated to achieve equal performance – making Monowave the ideal instrument for solvent comparison across chemical reactions. Finally, even chemicals not suitable for glass vials (fluorination agents or alkaline samples) can be processed in the chemically inert, robust SiC vessels.

Save time, expenditure, and the environment with tool-free and reusable consumables

Save time, expenditure, and the environment with tool-free and reusable consumables

Choose from reaction vials for any scale between 0.5 mL and 20 mL. For bulky samples and extraction applications, a special wide-neck vessel offers convenience without compromising performance. Establish a hassle-free workflow in your laboratory with tool-free handling, and reduce the cost of ownership and the environmental footprint of your research by using reusable vials, septa, and caps.

See everything: Watch your synthesis and analyze it in real-time

See everything: Watch your synthesis and analyze it in real-time

With Monowave 400 and Monowave 450 you can record images and videos with the integrated digital camera. You can follow color changes and precipitation, check the dissolution of substrates, and optimize the stirring efficiency. Monowave 400 R can be combined with Anton Paar’s Cora 5001 Raman spectrometer for in-situ Raman spectroscopy measurements of chemical reactions. Identify intermediates and short-lived transition states, investigate reaction kinetics and optimize reaction conditions with real-time information about the chemical composition of your reaction. The contactless measurement removes any worries about cross-contamination and the need for cleaning in between experiments.

Technical specifications

 Monowave 400/450Monowave 200
Max. filling volume 6 mL for 10 mL vial
20 mL for 30 mL vial
2 mL for 4 mL vial
6 mL for 10 mL vial
20 mL for 30 mL vial
2 mL for 4 mL vial
Max. operation pressure 30 bar (435 psi) 20 bar (290 psi)
(upgradable)
Max. IR temperature 300 °C 260 °C (upgradable)
Max. fiber-optic temperature 300 °C 260 °C (upgradable)
Max. power 850 W 850 W
Vial material Borosilicate glass, silicon carbide Borosilicate glass, silicon carbide
Cap material PEEK PEEK
Camera Integrated Optional after upgrade
Autosampler MAS24 Optional Optional after upgrade
Seal material Teflon-coated silicone Teflon-coated silicone
Typical applications Method development Optimization
Basic academic and industrial research
Method development
Optimization
Basic academic and industrial research

Anton Paar Certified Service

The Anton Paar quality in service and support:
  • More than 350 manufacturer-certified technical experts worldwide
  • Qualified support in your local language
  • Protection for your investment throughout its lifecycle
  • 3-year warranty
Learn more

Documents

Consumables & Accessories

Consumables & Accessories

Accessories

Accessories

Not all items are purchasable online in specific countries.

To find out if you can purchase online from your location, check the online availability below.

Online price only | excl.incl. 0VAT

IR WINDOW

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 80893
Product details
Mandatory PE sleeve in the microwave cavity to protect the IR sensor in case of vessel breakage.

REACTION VIAL G30 (20 PCS.)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 82723
Product details
Box containing 20 pcs. 30 mL reaction vials made of borosilicate glass, operation volume 6-20 mL. Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty due to the dependence on the handling by the user.

REACTION VIAL G10 (100 PCS.)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 82724
Product details
Box containing 100 Pcs 10 mL reaction vials made of borosilicate glass, operation volume 2-6 mL. Note: caps, septa, and stir bars not included Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty due to the dependence on the handling by the user.

SNAP CAPS (20 PCS.)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 83214
Product details
Package of 20 PEEK-made cap for easy and quick snap-on closure of reaction vials (10 <(>&<)> 30 mL) in combination with the corresponding silicone septa

SILICONE SEPTUM FOR RUBY THERMOMETER

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 88882
Product details
Package of 20 pcs. punched PTFE-coated silicone septum for insertion of the immersion tube when applying the ruby thermometer.

SILICONE SEPTUM (20 PCS.)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 88883
Product details
Package of 20 pcs. PTFE-coated silicone septa for tight sealing of react vials in combination with snap caps.

IMMERSION TUBE FOR RUBY THERM.(5 pcs)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 89048
Product details
Package of 5 pcs. immersion tube made of borosilicate glass for applicat of the Ruby Thermometer in reaction vials G4, G10, G30 , and C10 with silicone septum for Ruby Thermometer. Do not use with PTFE Disk d = 22 mm (161731) and PTFE Septum d = 22 mm for Ruby Thermometer (161733)! Do not use with PTFE Septum Wide Neck for Ruby Thermometer (161730)! Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.

STIR BAR PTFE D = 3, L = 10 (10 PCS.)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 89088
Product details
Package of 10 pcs. cylindrical PTFE coated stir bars for use with reacti vials G10, G30 and MG5.

STIR BAR PTFE D = 2, L = 5 (10 PCS.)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 99134

REACTION VIAL G4 (10 PCS.)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 99135
Product details
Box containing 10 pcs. 4 mL reaction vials made of borosilicate glass. Operation volume: 0.5-2 mL Note: Cannot be used in Monowave 100! Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.

CAVITY INSERT FOR CAMERAOPTION

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 105332
Product details
Cavity insert with glass window for use with the integrated camera. Note: not applicable with Monowave 100!

REACTION VIAL G30 WIDE NECK (10 PCS)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161723
Product details
Box containing 10# 30 mL reaction vials with wide neck made of borosilicate glass. Operation volume: 6-20 mL Note: Cannot be used in Monowave 100! Can be used in Monowave 200 only after upgrade by software token! Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.

SNAP CAP WIDE NECK ASSEMBLED (10 PCS)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161724
Product details
Package of 10# PEEK made caps (consisting of inner and outer part) for easy snap-on closure of Reaction Vial G30 Wide Neck in combination with the corresponding PTFE septum. For use in Monowave 400 and Monowave 450 only!

PTFE SEPTUM WIDE NECK (50 PCS.) Package of 50 pcs. disposable PTFE septa for tight sealin

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161728
Product details
Neck reaction vials in combination with Snap Cap G30 Wide Neck assembled. For use in Monowave 400 and Monowave 450 only!

PTFE DISK D = 22 MM (5 PCS) Package of 5 pcs. PTFE disks supporting the tight sealing of

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161731
Product details
G4, G10, G30, and C10 with corresponding PTFE septa d = 22 mm. For use as an alternative to standard silicone septa in long term reactions or with chemicals reducing the stability of silicone.

PTFE SEPTUM D = 22 MM (50 PCS)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161732
Product details
Package of 50 pcs. disposable PTFE septa for tight sealing of reaction v G4, G10, G30, and C10 in combination with PTFE disk. For use as an alternative to standard Silicone Septa in long term reactions or with chemicals reducing the stability of silicone.

PTFE SEPTUM D= 22 MM FOR RUBY THERMOMETER (50 PCS.)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161733
Product details
Package of 50 pcs. disposable punched PTFE septa for insertion of the Immersion Tube long for PTFE septa d = 22 mm when applying the Ruby Thermometer with PTFE disk d = 22 mm. For use as an alternative to standard Silicone Septa for Ruby Thermometer in long term reactions or with chemicals reducing the stability of silicone. Do not use with Immersion Tube for Ruby Thermometer! (89048) Do not use with Immersion Tube short for G30 Wide Neck! (161727)

STIR BAR OVAL 15x6 MM (10 PCS)

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 165242
Product details
Package of 10# egg-shaped PTFE coated stir bars for use with reaction vials G30 and G30 Wide Neck.

LONG IMMERSION TUBE FOR PTFE SEPTUM D = 22 mm (5 PCS) Package of 5 pcs. immersion tubes m

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161734
Product details
for use of Ruby Thermometer with the PTFE disk d = 22mm and PTFE Septum for Ruby§ Thermometer d = 22 mm. Do not use with Silicone Septum for Ruby Thermometer! (88882). Do not use with PTFE septum wideneck Ruby Thermometer! (161730). Glass and quartz parts and complete reaction vessels are not covered by standard warranty.

REACTION VESSEL C10 PACKAGE

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 93487
Product details
Convenient set for experiments with the silicon carbide vessel. Comprising 1 reaction vessel C10 with 1 package (20 pcs) each of snap caps and silicon septa. Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.

SHORT IMMERSION TUBE FOR G30 WIDE NECK (3 PCS.) Package of 3 pcs. immersion tubes made of

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161727
Product details
in the Ruby thermometer with G30 wide neck reaction vials. For use in Monowave 400 and Monowave 450 only! Do not use with Silicone septum for Ruby thermometer! (88882). Do not use with PTFE septum d=22 mm for Ruby thermometer! (161733). Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.

PTFE SEPTUM WIDE NECK FOR RUBY THERMOMETER (50 PCS) Package of 50 pcs. disposable perfora

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 161730
Product details
insertion of the immersion tube short for G30 Wide neck when applying the Ruby Thermometer with Reaction Vial G30 Wide Neck. For use in Monowave 400 and Monowave 450 only! Do not use with Immersion Tube for Ruby Thermometer! Do not use with Immersion long Tube for PTFE septa d= 22 mm.

ETHERNET CABLE FOR PC CONNECTION CAT5E, RJ45G-RJ45G, SFTP, 2 m, CROSSED

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 18597
Product details

Only for ViscoQC 300. Cable for LIMS Bridge connection to PC for transferring measurement data.

REACTION VESSEL C10

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 93486
Product details
Single 10 mL silicon carbide vessel without any additional consumables. Operation volume 2-6 mL. Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.

RACK 40

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 89296
Product details
Plastic rack with 40 positions for proper storage of reaction vials G10. (Vessels not included.)
This vial type was introduced to allow beneficial application of volumes below 2 mL in Monowave 300. As with all other vial types, the G4 vial tolerates conditions up to 300 °C and 30 bar and therefore enables efficient method development with the lowest quantities. Even stirring is possible to ensure agitation of the reaction mixture.

Reaction Vial G4

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Product details
  • Vial for Monowave 300
  • Designed for volumes between 0.5 mL and 2.0 mL
  • For efficient method development with the lowest quantities

 

More info

Silicon carbide (SiC) is a chemically inert material with high heat conductivity which strongly absorbs microwave energy. Employing SiC as a vessel material makes microwave chemistry even more attractive since it will not only shorten your overall process time, but enables access to reactions which cannot be performed in standard glass vials (e.g. fluorinations).

Silicon Carbide Vessel

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Product details
  • Accessory for microwave synthesis reactors
  • Shortens overall process time
  • Heating rates >10 °C/second, even for non-absorbing solvents
  • Ideal for fluorinations and other challenging reactions

More info

The ruby thermometer consists of a ruby crystal which is periodically excited by blinking light. The decay time of the luminescence is temperature-dependent and correlates with the temperature around the crystal.

Ruby Thermometer

Compatible with:
Monowave 450 | 400 | 200
More info
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Different racks are available for the adequate storage of the various vessel types and liners of Multiwave PRO as well both vial sizes of Monowave 300. For vessels applicable in the multimode reactors Anton Paar supplies Rack 16, a polyethylene foam block for 16 vessels or liners of Rotor 8 and Rotor 16.

Racks

Compatible with:
Monowave 450 | 400 | 200
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Product details
  • Different racks for storing vessels, liners, and vials
  • For Multiwave 5000: Rack 12 for HVT vessels, Rack 10 for SVT vessels, Rack 16 for 16 vessels or liners of Rotor 8 and Rotor 16
  • For Monowave 200/400/450: 24 x 30 mL vials and 40 x 10 mL vials

More info