Microwave Reactor:
Monowave
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- Monowave 400 with on-top automation, in an attractive package
- Unattended processing of 24 vials of different sizes
- Specially designed vessels for solvent extraction or bulky samples
- Remote control via VNC
- Environmental footprint reduction
- 21 CFR Part 11-compliant
The Anton Paar Monowave product line is a series of high-performance monomode microwave reactors designed for small- to medium-scale microwave synthesis.
Attain temperatures up to 300 °C and pressures up to 30 bar with advanced all-the-time safety features for high-speed, high-pressure, high-temperature reactions. Improve productivity and product purity across all applications in research and development laboratories with precise heating profiles. Reduce consumable costs and your environmental footprint by using the reusable vials, caps, and septa.
Visit our world of microwave synthesis to find your optimum reaction conditions and to browse through a database of more than 1000 applications which have been successfully performed in Anton Paar reactors.
Key features
Fast and effective: 24 sequential reactions, unattended
The Autosampler MAS 24 allows 24 unattended reactions, in sequence – saving time, and increasing efficiency. High field density produces fast, uniform heating for all kinds of reactions, up to 300 °C. Powerful stirring of up to 1200 rpm assures temperature homogeneity. The powerful 850 W magnetron adjusts its unpulsed microwave power automatically to the sample. This software-driven self-tuning eliminates any guesswork about sample absorption. Achieve high yields and clean reactions with maximum reproducibility.
The key factor in synthesis: Precise, scalable temperature measurement
Current scientific practice is to use reaction temperature as the relevant parameter in microwave reactions. And accurate measurement of the reaction temperature is the key to correct transferal and scale-up of reaction protocols between different reactors. Monowave reactors measure the temperature via an IR temperature sensor – a robust and reliable method for temperature control ensuring absolutely precise temperature measurement. For accurate control of even more demanding reactions, such as an exothermic reactions, or those involving extremely sensitive samples, simultaneous internal temperature measurement with the optional fiber-optic ruby thermometer is available.
Vials for heating any solvent and any reaction mixture
In addition to the standard glass vials, silicon carbide (SiC) vessels are available. They absorb microwave energy efficiently, while shielding the interior from microwave radiation – a method that reveals microwave effects caused by selective absorption, and allows comparison between direct microwave heating and conventional heating of reaction mixtures. All parameters, such as the heating and cooling rate, the form factor of the reaction vessel, and the stirring efficiency are identical, apart from the heating mode. All solvents, from non-absorbing ones such as hexane to excellent absorbers such as ionic liquids, can be heated to achieve equal performance – making Monowave the ideal instrument for solvent comparison across chemical reactions. Finally, even chemicals not suitable for glass vials (fluorination agents or alkaline samples) can be processed in the chemically inert, robust SiC vessels.
Save time, expenditure, and the environment with tool-free and reusable consumables
Choose from reaction vials for any scale between 0.5 mL and 20 mL. For bulky samples and extraction applications, a special wide-neck vessel offers convenience without compromising performance. Establish a hassle-free workflow in your laboratory with tool-free handling, and reduce the cost of ownership and the environmental footprint of your research by using reusable vials, septa, and caps.
See everything: Watch your synthesis and analyze it in real-time
With Monowave 400 and Monowave 450 you can record images and videos with the integrated digital camera. You can follow color changes and precipitation, check the dissolution of substrates, and optimize the stirring efficiency. Monowave 400 R can be combined with Anton Paar’s Cora 5001 Raman spectrometer for in-situ Raman spectroscopy measurements of chemical reactions. Identify intermediates and short-lived transition states, investigate reaction kinetics and optimize reaction conditions with real-time information about the chemical composition of your reaction. The contactless measurement removes any worries about cross-contamination and the need for cleaning in between experiments.
Specifications
| Monowave 400/450 | Monowave 200 | |
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| Max. filling volume | 6 mL for 10 mL vial 20 mL for 30 mL vial 2 mL for 4 mL vial | 6 mL for 10 mL vial 20 mL for 30 mL vial 2 mL for 4 mL vial |
| Max. operation pressure | 30 bar (435 psi) | 20 bar (290 psi) (upgradable) |
| Max. IR temperature | 300 °C | 260 °C (upgradable) |
| Max. fiber-optic temperature | 300 °C | 260 °C (upgradable) |
| Max. power | 850 W | 850 W |
| Vial material | Borosilicate glass, silicon carbide | Borosilicate glass, silicon carbide |
| Cap material | PEEK | PEEK |
| Camera | Integrated | Optional after upgrade |
| Autosampler MAS 24 | Optional | Optional after upgrade |
| Seal material | Teflon-coated silicone | Teflon-coated silicone |
| Typical applications | Method development Optimization Basic academic and industrial research | Method development Optimization Basic academic and industrial research |
Anton Paar Certified Service
- More than 350 manufacturer-certified technical experts worldwide
- Qualified support in your local language
- Protection for your investment throughout its lifecycle
- 3-year warranty
Documents
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Biofuels | Microwave Extraction and Synthesis of Fatty Acid Methyl Esters Application Reports
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Cancer Diagnosis with Persistent Luminescent Nanoparticles Application Reports
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Downscaling of Standard Norms for Microwave-Assisted Extraction Methods Application Reports
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E-Book - Microwave Synthesis Essentials Application Reports
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Extraction and Quantification of Diterpenes from Green Coffee Oil Application Reports
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Extraction | MCPD Esters from Food Application Reports
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Levulinates from Levulinic Acid utilizing Vanadium-incorporated Heteropoly Acid Application Reports
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MAE of PAHs from Dietary Matrices Application Reports
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Microwave-assisted Extraction of Additives from Polymers Application Reports
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Monowave 400 with Camera - Watching Microwave Synthesis Live Application Reports
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Preparation of Palladium Nanocubes in Water Application Reports
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Silicon Carbide Vessel | Applications of Silicon Carbide Vessels Application Reports
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Standard Extraction Methods in Multiwave 5001 or Monowave 450 Application Reports
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Synthesis | Gas Loading | Inert Gas Atmosphere in Microwave Reactions Application Reports
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Synthesis | Solids in Microwave Reactors? Application Reports
Complementary products
If you do not find the item you require, please contact your Anton Paar sales representative.
REACTION VESSEL C30 WIDE NECK ASSEMBLED
Monowave 450 | 400 | 200
Single 30 mL wide neck silicon carbide vessel with wide neck with one Snap Cap Wide Neck and one corresponding PTFE Septum Wide Neck. Operation Volume 6-20 mL. 3 Note: For opening of the C30 Wide Neck vessel the use of the Decapper Wide Neck Vessels (Mat. No. 161692) is required.
Reaction Vial G4
Monowave 450 | 400 | 200
- Vial for Monowave 300
- Designed for volumes between 0.5 mL and 2.0 mL
- For efficient method development with the lowest quantities
Silicon Carbide Vessel
Monowave 450 | 400 | 200
- Accessory for microwave synthesis reactors
- Shortens overall process time
- Heating rates >10 °C/second, even for non-absorbing solvents
- Ideal for fluorinations and other challenging reactions
Ruby Thermometer
Monowave 450 | 400 | 200
- Measures temperature via ruby crystal’s luminescence decay time
- Accurate internal temperature monitoring up to 300 °C
- Precise control with no thermal overshoot, even in extreme conditions
- Calibration-free, Plug and Play operation, no electromagnetic interference
Racks
Monowave 450 | 400 | 200
- Different racks for storing vessels, liners, and vials
- For Multiwave 5000: Rack 12 for HVT vessels, Rack 10 for SVT vessels, Rack 16 for 16 vessels or liners of Rotor 8 and Rotor 16
- For Monowave 200/400/450: 24 x 30 mL vials and 40 x 10 mL vials
IR WINDOW
Monowave 450 | 400 | 200
Mandatory PE sleeve in the microwave cavity to protect the IR sensor in case of vessel breakage.
REACTION VIAL G30 (20 PCS.)
Monowave 450 | 400 | 200
Box containing 20 pcs. 30 mL reaction vials made of borosilicate glass, operation volume 6-20 mL. Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty due to the dependence on the handling by the user.
REACTION VIAL G10 (100 PCS.)
Monowave 450 | 400 | 200
Box containing 100 Pcs 10 mL reaction vials made of borosilicate glass, operation volume 2-6 mL. Note: caps, septa, and stir bars not included Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty due to the dependence on the handling by the user.
SNAP CAPS (20 PCS.)
Monowave 450 | 400 | 200
Package of 20 PEEK-made cap for easy and quick snap-on closure of reaction vials (10 <(>&<)> 30 mL) in combination with the corresponding silicone septa
SILICONE SEPTUM FOR RUBY THERMOMETER
Monowave 450 | 400 | 200
Package of 20 pcs. punched PTFE-coated silicone septum for insertion of the immersion tube when applying the ruby thermometer.
SILICONE SEPTUM (20 PCS.)
Monowave 450 | 400 | 200
Package of 20 pcs. PTFE-coated silicone septa for tight sealing of react vials in combination with snap caps.
IMMERSION TUBE FOR RUBY THERM.(5 pcs)
Monowave 450 | 400 | 200
Package of 5 pcs. immersion tube made of borosilicate glass for applicat of the Ruby Thermometer in reaction vials G4, G10, G30 , and C10 with silicone septum for Ruby Thermometer. Do not use with PTFE Disk d = 22 mm (161731) and PTFE Septum d = 22 mm for Ruby Thermometer (161733)! Do not use with PTFE Septum Wide Neck for Ruby Thermometer (161730)! Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.
STIR BAR PTFE D = 3, L = 10 (10 PCS.)
Monowave 450 | 400 | 200
Package of 10 pcs. cylindrical PTFE coated stir bars for use with reacti vials G10, G30 and MG5.
STIR BAR PTFE D = 2, L = 5 (10 PCS.)
Monowave 450 | 400 | 200
REACTION VIAL G4 (10 PCS.)
Monowave 450 | 400 | 200
Box containing 10 pcs. 4 mL reaction vials made of borosilicate glass. Operation volume: 0.5-2 mL Note: Cannot be used in Monowave 100! Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.
CAVITY INSERT FOR CAMERAOPTION
Monowave 450 | 400 | 200
Cavity insert with glass window for use with the integrated camera. Note: not applicable with Monowave 100!
REACTION VIAL G30 WIDE NECK (10 PCS)
Monowave 450 | 400 | 200
Box containing 10# 30 mL reaction vials with wide neck made of borosilicate glass. Operation volume: 6-20 mL Note: Cannot be used in Monowave 100! Can be used in Monowave 200 only after upgrade by software token! Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.
SNAP CAP WIDE NECK ASSEMBLED (10 PCS)
Monowave 450 | 400 | 200
Package of 10# PEEK made caps (consisting of inner and outer part) for easy snap-on closure of Reaction Vial G30 Wide Neck in combination with the corresponding PTFE septum. For use in Monowave 400 and Monowave 450 only!
PTFE SEPTUM WIDE NECK (50 PCS.) Package of 50 pcs. disposable PTFE septa for tight sealin
Monowave 450 | 400 | 200
Neck reaction vials in combination with Snap Cap G30 Wide Neck assembled. For use in Monowave 400 and Monowave 450 only!
PTFE DISK D = 22 MM (5 PCS) Package of 5 pcs. PTFE disks supporting the tight sealing of
Monowave 450 | 400 | 200
G4, G10, G30, and C10 with corresponding PTFE septa d = 22 mm. For use as an alternative to standard silicone septa in long term reactions or with chemicals reducing the stability of silicone.
PTFE SEPTUM D = 22 MM (50 PCS)
Monowave 450 | 400 | 200
Package of 50 pcs. disposable PTFE septa for tight sealing of reaction v G4, G10, G30, and C10 in combination with PTFE disk. For use as an alternative to standard Silicone Septa in long term reactions or with chemicals reducing the stability of silicone.
PTFE SEPTUM D= 22 MM FOR RUBY THERMOMETER (50 PCS.)
Monowave 450 | 400 | 200
Package of 50 pcs. disposable punched PTFE septa for insertion of the Immersion Tube long for PTFE septa d = 22 mm when applying the Ruby Thermometer with PTFE disk d = 22 mm. For use as an alternative to standard Silicone Septa for Ruby Thermometer in long term reactions or with chemicals reducing the stability of silicone. Do not use with Immersion Tube for Ruby Thermometer! (89048) Do not use with Immersion Tube short for G30 Wide Neck! (161727)
STIR BAR OVAL 15x6 MM (10 PCS)
Monowave 450 | 400 | 200
Package of 10# egg-shaped PTFE coated stir bars for use with reaction vials G30 and G30 Wide Neck.
LONG IMMERSION TUBE FOR PTFE SEPTUM D = 22 mm (5 PCS) Package of 5 pcs. immersion tubes m
Monowave 450 | 400 | 200
for use of Ruby Thermometer with the PTFE disk d = 22mm and PTFE Septum for Ruby§ Thermometer d = 22 mm. Do not use with Silicone Septum for Ruby Thermometer! (88882). Do not use with PTFE septum wideneck Ruby Thermometer! (161730). Glass and quartz parts and complete reaction vessels are not covered by standard warranty.
REACTION VESSEL C10 PACKAGE
Monowave 450 | 400 | 200
Convenient set for experiments with the silicon carbide vessel. Comprising 1 reaction vessel C10 with 1 package (20 pcs) each of snap caps and silicon septa. Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.
SHORT IMMERSION TUBE FOR G30 WIDE NECK (3 PCS.) Package of 3 pcs. immersion tubes made of
Monowave 450 | 400 | 200
in the Ruby thermometer with G30 wide neck reaction vials. For use in Monowave 400 and Monowave 450 only! Do not use with Silicone septum for Ruby thermometer! (88882). Do not use with PTFE septum d=22 mm for Ruby thermometer! (161733). Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.
PTFE SEPTUM WIDE NECK FOR RUBY THERMOMETER (50 PCS) Package of 50 pcs. disposable perfora
Monowave 450 | 400 | 200
insertion of the immersion tube short for G30 Wide neck when applying the Ruby Thermometer with Reaction Vial G30 Wide Neck. For use in Monowave 400 and Monowave 450 only! Do not use with Immersion Tube for Ruby Thermometer! Do not use with Immersion long Tube for PTFE septa d= 22 mm.
ETHERNET CABLE FOR PC CONNECTION CAT5E, RJ45G-RJ45G, SFTP, 2 m, CROSSED
Monowave 450 | 400 | 200
Only for ViscoQC 300. Cable for LIMS Bridge connection to PC for transferring measurement data.
REACTION VESSEL C10
Monowave 450 | 400 | 200
Single 10 mL silicon carbide vessel without any additional consumables. Operation volume 2-6 mL. Glass and quartz parts as well as complete reaction vessels are not covered by standard warranty.
RACK 40
Monowave 450 | 400 | 200
Plastic rack with 40 positions for proper storage of reaction vials G10. (Vessels not included.)
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