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  4. Gain insights into synthesis processes and material properties with live Raman analysis

Gain insights into synthesis processes and material properties with live Raman analysis

기본 교육

Combining microwave synthesis and measurement of physical properties with Live Raman Spectroscopy opens up a wealth of information that has not been accessible before. This is particularly the case for in-situ measurements during chemical reactions.

We will demonstrate the capabilities of Live Raman analysis during microwave synthesis on the example of a Suzuki Cross-Coupling reaction. Raman monitoring during the reaction cycle provides valuable insights into the reaction kinetics, formation and consumption of intermediates as well as reaction end-points. Collecting information throughout the entire reaction cycle allows a much more targeted reaction optimization compared to analysis steps after synthesis. This way, iterations can be reduced and better yields can be achieved within a fraction of the time.

Chemical reactions can result in changes in the mechanical properties. In epoxy curing, for example, we show the changes in macroscopic visco-elastic behavior show in the rheology data. The chemical reaction on the molecular level can be made visible in the Raman signal and follow a different path over time. Both combined shed light onto the underlying mechanisms and kinetics of the curing process, which influence the material properties and help in their optimization.

Dr. Nils Bertram, Dr. Mandy Jahns (English)

장소: Gurugram, India, Anton Paar India's Application Lab Gurugram
참가자 수: 35
주최자: Anton Paar India
비용: Free of cost
등록 완료: 2022. 12. 6.

연락 담당자 및 등록:
Mr. Gomathi Nallasivan
전화: 9004002079
gomathi.nallasivan[at]anton-paar.com