Low-Temperature Chamber:
TTK 600
- Non-ambient attachment for X-ray diffraction studies from -190 °C to 600 °C
- For investigations on samples in reflection and transmission geometry
- Also for air-sensitive samples and in-operando studies on batteries
- Fits to all common powder diffractometers
The TTK 600 Low-Temperature Chamber is a non-ambient attachment for powder X-ray diffraction studies from -190°C to 600°C. Different sample holders allow investigating samples in reflection and transmission geometry. Samples can be measured in vacuum, air or inert gases. An antechamber option allows safe transfer of air-sensitive samples into the TTK 600.
The TTK 600 fits to all common powder diffractometers and is the instrument of choice for X-ray structure analysis of various sample types at low and medium temperatures.
Key features
Fast and accurate temperature control
- Liquid nitrogen cooling to -190°C or compressed air cooling to -10°C
- Resistance heating for rapid heating up to 600°C
- Pt100 close to the sample for precise temperature measurement
- Flexible liquid nitrogen hoses for movability even at -190°C
- Improved heat transfer from heater to sample holder. Additional convection heating for the capillary sample holder and the transmission sample holder for reduced temperature deviation
Optimized for maximum sample flexibility
- Various types of sample holders:
- Standard sample holder for the investigation of powders in reflection geometry (different depths available)
- Capillary sample holder for the investigation of powders in transmission geometry
- Transmission sample holder for the investigation of foils, pastes and powders in transmission mode
- Zero background holder for transparent samples
- Integrated beam knife to minimize background at low 2θ
- Easy exchange and mounting of samples
Technical specifications
| Operating temperature | -190 °C to 600 °C with liquid nitrogen cooling -10 °C to 600 °C with compressed-air cooling |
|---|---|
| Temperature measurement | Pt 100 |
| Atmosphere | Vacuum (10-2 mbar), air, inert gas |
| Angle of incidence (2Θ) | 0 to 164 ° (standard sample holder) |
| Max. operating pressure | 2 bar above atmospheric pressure |
| Sample holder material | Chromium-plated copper |
| Sample size | 14 x 10 mm |
Anton Paar Certified Service
- More than 350 manufacturer-certified technical experts worldwide
- Qualified support in your local language
- Protection for your investment throughout its lifecycle
- 3-year warranty
Documents
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E-Book - Field Guide to Pharmaceutical Powder Characterization Application Reports
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Ice Formation Mechanisms of Aqueous Sucrose Solutions Application Reports
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Low Temperature Phase Identification in Organic Semiconductor Thin Films Application Reports
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Prohibiting the decomposition reaction of air-sensitive Lithium Hydride (LiH) Application Reports
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Sintering Behavior of Thiol-capped Gold Nanoparticles Investigated with TTK 600 Application Reports
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Temperature Validation for In-Situ X-ray Diffraction Below Ambient Temperatures Application Reports
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Antechamber for TTK 600 Brochures
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Battery Sample Holder for TTK 600 Brochures
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TTK 600 Low Temperature Chamber Brochures
Compatible instruments
Consumables
Consumables
If you do not find the item you require, please contact your Anton Paar sales representative.
To find out if you can purchase online from your location, check the online availability below.
SET OF GRAPHITE FOILS FOR TTK 600
SET OF KAPTON FOILS FOR TTK 600 (5 pcs.)
SET OF O-RINGS FOR TTK600
SPARE PARTS PACKAGE TTK 600
- 1 Pc. 164866 Set of O-Rings
- 1 Pc. 70175 Vacuum grease (20 g)
- 1 Pc. 164865 Set of Kapton foils (5 pcs)
- 1 Pc. 164864 Set of Graphite foils (10 pcs)
SET OF FOILS FOR HEATING ENVIRONMENT FOR STANDARD SAMPLE HOLDER GRAPHITE (5 Pcs.) AND NIC
SET OF FOILS FOR CAPILLARY SAMPLE HOLDER
SET OF FOILS FOR TRANSMISSION SAMPLE HOLDER
NON-AMBIENT GUIDE
STANDARD SAMPLE HOLDER TTK 600 WITH Pt100 (0.8 mm DEPTH) Spare sample holder with cavity
STANDARD SAMPLE HOLDER TTK 600 WITH Pt100 (FLAT)
STANDARD SAMPLE HOLDER TTK 600 WITH Pt100 (0.2 mm DEPTH)
Going beyond, with the HTK 1500 High-Temperature Chamber
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