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Low-Temperature Chamber:
TTK 600
- Non-ambient attachment for X-ray diffraction studies from -190 °C to 600 °C
- For investigations on samples in reflection and transmission geometry
- Also for air-sensitive samples and in-operando studies on batteries
- Fits to all common powder diffractometers
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The TTK 600 Low-Temperature Chamber is a non-ambient attachment for powder X-ray diffraction studies from -190°C to 600°C. Different sample holders allow investigating samples in reflection and transmission geometry. Samples can be measured in vacuum, air or inert gases. An antechamber option allows safe transfer of air-sensitive samples into the TTK 600.
The TTK 600 fits to all common powder diffractometers and is the instrument of choice for X-ray structure analysis of various sample types at low and medium temperatures.
Key features
Fast and accurate temperature control
- Liquid nitrogen cooling to -190°C or compressed air cooling to -10°C
- Resistance heating for rapid heating up to 600°C
- Pt100 close to the sample for precise temperature measurement
- Flexible liquid nitrogen hoses for movability even at -190°C
- Improved heat transfer from heater to sample holder. Additional convection heating for the capillary sample holder and the transmission sample holder for reduced temperature deviation
Optimized for maximum sample flexibility
- Various types of sample holders:
- Standard sample holder for the investigation of powders in reflection geometry (different depths available)
- Capillary sample holder for the investigation of powders in transmission geometry
- Transmission sample holder for the investigation of foils, pastes and powders in transmission mode
- Zero background holder for transparent samples
- Integrated beam knife to minimize background at low 2θ
- Easy exchange and mounting of samples
Technical specifications
| Operating temperature | -190 °C to 600 °C with liquid nitrogen cooling -10 °C to 600 °C with compressed-air cooling |
|---|---|
| Temperature measurement | Pt 100 |
| Atmosphere | Vacuum (10-2 mbar), air, inert gas |
| Angle of incidence (2Θ) | 0 to 164 ° (standard sample holder) |
| Max. operating pressure | 2 bar above atmospheric pressure |
| Sample holder material | Chromium-plated copper |
| Sample size | 14 x 10 mm |
Anton Paar Certified Service
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Documents
Your choice:
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Ice Formation Mechanisms of Aqueous Sucrose Solutions Application Reports
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Low Temperature Phase Identification in Organic Semiconductor Thin Films Application Reports
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Prohibiting the decomposition reaction of air-sensitive Lithium Hydride (LiH) Application Reports
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Sintering Behavior of Thiol-capped Gold Nanoparticles Investigated with TTK 600 Application Reports
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Temperature Validation for In-Situ X-ray Diffraction Below Ambient Temperatures Application Reports
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eBook - The Field Guide to Pharmaceutical Powder Characterization Application Reports
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Antechamber for TTK 600 Brochures
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Battery Sample Holder for TTK 600 Brochures
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TTK 600 Low Temperature Chamber Brochures
Compatible instruments
Consumables
Consumables
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SET OF GRAPHITE FOILS FOR TTK 600
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Part number: 164864
Product details
Set of 10 pcs of graphite foils for heat transfer between heater and sample holder of TTK 600.
SET OF KAPTON FOILS FOR TTK 600 (5 pcs.)
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Part number: 164865
Product details
5 pcs of Kapton window foils (50 μm) for TTK 600.
SET OF O-RINGS FOR TTK600
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Part number: 164866
SPARE PARTS PACKAGE TTK 600
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Part number: 165748
Product details
Consists of:
- 1 Pc. 164866 Set of O-Rings
- 1 Pc. 70175 Vacuum grease (20 g)
- 1 Pc. 164865 Set of Kapton foils (5 pcs)
- 1 Pc. 164864 Set of Graphite foils (10 pcs)
- 1 Pc. 164866 Set of O-Rings
- 1 Pc. 70175 Vacuum grease (20 g)
- 1 Pc. 164865 Set of Kapton foils (5 pcs)
- 1 Pc. 164864 Set of Graphite foils (10 pcs)
SET OF FOILS FOR HEATING ENVIRONMENT FOR STANDARD SAMPLE HOLDER GRAPHITE (5 Pcs.) AND NIC
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Part number: 171083
SET OF FOILS FOR CAPILLARY SAMPLE HOLDER
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Part number: 171084
Product details
The set contains each 3 pcs. of Kapton, Nickel and Graphite foils for the use in combination with the capillary sample holder.
SET OF FOILS FOR TRANSMISSION SAMPLE HOLDER
Delivery time:
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Part number: 171085
Product details
The set contains each 10 pcs. of Kapton and Graphite foils and 2 pcs. of Nickel foils for the use in combination with the transmission sample holder.
NON-AMBIENT GUIDE
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Part number: 223464
Product details
The XRD-Guide gives an overview from instrumentation, analysis, and data interpretation to applications. It gives an introduction to non-ambient X-ray diffraction (NA-XRD) and aims to give a global overview on the main instrumentation and applications. The XRD-Guide is intended to help people new to the field of NA-XRD analysis.
STANDARD SAMPLE HOLDER TTK 600 WITH Pt100 (0.8 mm DEPTH) Spare sample holder with cavity
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Part number: 159930
STANDARD SAMPLE HOLDER TTK 600 WITH Pt100 (FLAT)
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Part number: 162263
Product details
Spare sample holder with integrated Pt100 RTD without cavity.
STANDARD SAMPLE HOLDER TTK 600 WITH Pt100 (0.2 mm DEPTH)
Delivery time:
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Part number: 162262
Product details
Spare sample holder with a cavity of 0.2 mm depth and integrated Pt100 RTD.
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