Pulse titration (Part 1): sample-independent optimization Autosorb 6X00 Series
This application report focuses on optimizing parameters to reach the highest accuracy when running pulse titration experiments on the Autosorb series.
This application report is the first in a series about pulse titration experiments. It provides a brief description of the system, with theoretical insights into components such as the injection loop valve and the thermal conductivity detector. It focuses on the instrumentation and how experimental parameters (such as carrier gas flow rate, active gas concentration, injection loop size, cell temperature, and thermal conductivity detector (TCD) filament current), which were systematically varied, influence the pulse titration experiment independently of a sample.
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