Optimizing and troubleshooting TPX experiments: calcium oxalate case study
This report presents a successful temperature programmed experiment (TPX) as a reference with a variety of controlled “failed” experiments to showcase the most common reasons for failure.
Determining whether a flow chemisorption experiment is a success begins with identifying the expected features of a successful experiment. A successful temperature programmed decomposition (TPD) is presented in this application report, as well as several “failed” experiments, to contrast reasons for success with the most common reasons for failure. The observations made about this TPD experiment are also relevant to other TPXs, such as temperature programmed reduction (TPR) and temperature programmed oxidation (TPO).
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