Microwave Digestion: Rotor 16HF100

The acid digestion rotor 16HF100 with 16 high pressure vessels is designed for high sample throughput and efficient handling. The reaction temperature is controlled by means of two sensors: an immersing temperature probe (optional) inside a reference vessel and an IR sensor underneath the oven cavity, which measures each microwave digestion vessel through ports in the rotor base.

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Key Features

No loss of volatile analytes
No risk of contamination
No handling of hot and pressurized vessels or rotors

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Documents

Digestion in Multiwave PRO using HF Complexation of Fluorides Application Reports en
EPA Methods 3015A, 3051A and 3052 | Sample Preparation in Multiwave PRO Application Reports en

Accessories

The all-purpose calibration unit enables checks and calibrations of all types of temperature sensors used in Multiwave PRO and Multiwave ECO. Calibration of the temperature sensors using the calibration unit maintains the accuracy of the temperature measurement in order to comply with GLP and to extend the lifetime of the reaction vessels.

Calibration Unit

Consumable Sets

The gas loading accessory set is a special tool for purging and charging the pressure vessel with gases. It is a helpful tool for performing reactions under inert gas atmosphere or utilizing gaseous reagents. This accessory is suitable for several applications such as microwave oxygen combustion, synthesis, protein hydrolysis and pressure filtration.

Gas Loading Accessory Set

Protein hydrolysis in the liquid or gas phase is a well-established procedure for sample preparation and structure analysis. Microwave protocols reduce the overall process time to less than one hour, compared to several hours of heating with classical thermal methods.

Hydrolysis Set

The Multiwave PRO microwave reaction system serves two groups: professionals in trace analysis and synthetic chemistry.

Magnetic Stirrer Device

Pressure/temperature sensor accessory for precise reaction control within the reference vessel of Rotor 16MF100 and/or Rotor 16HF100.

p/T Sensor Accessory

The cylindrically shaped passive heating elements are made of sintered silicon carbide (SiC). Due to its high microwave absorbance and excellent heat capacity, SiC can be used to efficiently heat low-absorbing solvents (toluene, dioxane, THF…) in a microwave environment.

Passive Heating Elements

The pressure sensor accessory allows for precise reaction control within the reference vessel of Rotor 16MF100 or Rotor 16HF100. The pressure data is transferred to the oven via infrared signal. If required, the pressure sensor accessory can be upgraded to a pressure/temperature sensor accessory.

Pressure Sensor Accessory

Different racks are available for the adequate storage of the various vessel types and liners of Multiwave PRO as well both vial sizes of Monowave 300. For vessels applicable in the multimode reactors Anton Paar supplies Rack 16, a polyethylene foam block for 16 vessels or liners of Rotor 8 and Rotor 16.

Racks

Anton Paar provides a Rotor Stand for the easy loading and unloading of reaction vessels into and out of any rotor used for Multiwave PRO or Multiwave ECO. Once a rotor is placed onto the Rotor Stand, the rotor is in a stable position and can be turned easily without the bottom plate of the rotor being scratched or worn out.

Rotor Stand

The Multiwave PRO microwave reaction system serves two groups: professionals in trace analysis and synthetic chemistry.

Safety Module SOLV

The seal forming device enables the proper pre-forming and safe storage of seals and screw caps of Rotor 8 and 16. One unit has a capacity for 8 caps/seals of different kinds. Storage in this device prolongs the lifetime of the lip-type seals.

Seal Forming Device