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High Vacuum Physisorption Analyzer:
Autosorb 6100

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  • Accurate high-vacuum analyses of surface area and micropores
  • Advanced measurement routines made accessible with DoseWizard point selection and PowderProtect
  • Up to three samples, three gases, and three temperatures can be measured simultaneously with independent analysis stations
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Autosorb 6100 Contact

The Autosorb 6100 is a high vacuum physisorption analyzer that’s been re-engineered for the most challenging measurements of surface area, pore size, and pore volume. Independent analysis stations, exclusive TruZone active coolant control, and accessible Kaomi for Autosorb software let you meet your current measurement needs, while factory and field upgradeable options let you adapt to future ones. For your most important physisorption measurements, the choice is clear: Absolutely Autosorb.

Key features

A physisorption analyzer that’s absolutely accurate

A physisorption analyzer that’s absolutely accurate

  • Get highly accurate physisorption measurements from relative pressures below 10-7 for nitrogen
  • Leverage precise manifold temperature control between 35 °C and 50 °C
  • Rely on TruZone active coolant level control for accurate data – even over lengthy analyses
  • Achieve superior high-vacuum performance (38 % better than previous generation instruments) with precision-machined manifolds and high-quality pneumatic valves
Independent stations ensure you’re absolutely agile

Independent stations ensure you’re absolutely agile

  • Analyze up to three different samples with three different analysis gases at three different temperatures simultaneously with independent analysis stations and patented temperature control accessories
  • Perform the most challenging micropore measurements with the physisorption analyzer’s 90-hour Dewar
  • Maximize your throughput with six integrated degassing stations
  • Degas two sets of samples at different temperatures up to 450 °C
Intuitive software makes physisorption absolutely accessible

Intuitive software makes physisorption absolutely accessible

  • Enjoy an updated and streamlined Kaomi software, which makes the whole measurement process easier than ever before
  • Optimize measurement definition to suit your needs with DoseWizard’s new standard and advanced modes
  • Keep downtime to a minimum with PowderProtect, which prevents accidental loss of powder in the instrument
Customization options keep you absolutely adaptable

Customization options keep you absolutely adaptable

  • Select the number of stations (one, two, or three) to match your throughput needs
  • Upgrade the number of stations and transducer sets as your needs change
  • Control up to three of our patented CryoSync accessories with a CryoSync control option so you can perform three measurements at three different temperatures simultaneously – no need for any external software
  • Benefit from a built-in vapor generator and recirculating Dewar now or in the future to enable precise measurements of water and organic vapor sorption
Compliance and quality are absolutely assured

Compliance and quality are absolutely assured

  • Comply with 15 ASTM, DIN, and ISO standards for surface area, pore size, and pore volume measurements
  • Get peace of mind with our 3-year warranty so you can avoid unforeseen costs

Technical specifications

Measurement principle: Vacuum volumetric
Analysis gases: N2, Ar, Kr, CO2, CH4, H2, and other non-corrosive gases
Analysis stations:
  • Number: 1, 2, or 3
  • Independence: Up to 3 gases at three analysis temperatures can be used concurrently, 1 analysis gas and temperature per station
Independent p0 station: Yes (dedicated cell and transducer)
Pressure: 
  • Range: 2x10-5 to 1100 Torr | 2.6x10-8 to 0.997 p/p0 for N2 77K
  • Resolution (MP): 2x10-5 Torr | 2.6x10-8 p/p0 for N2 77K
  • Resolution (XR): 1x10-6 Torr | 1.3x10-9 p/p0 for N2 77K
Surface area:
  • Absolute detection limit: 0.1 m2 (N2 77K)
  • Specific detection limit: 0.01 m2/g (N2 77K)
  • Typical reproducibility: 1 %* 
  • Reproducibility limit: 2 % with 2 m2 in the cell
Pore size:
  • Range: 0.35 nm to 500 nm (diameter)
  • Typical reproducibility: 0.5 %*
TruZone: Yes (active coolant level control) 
PowderProtect: Yes (prevents sample elutriation)
Analysis Dewar:
  • Duration: 90+ hours with liquid nitrogen
  • Refill during analysis: Yes
  • Volume: 3 L
Sample preparation:
  • Integrated degassing stations: 6 
  • Temperature control: 2 independent heating zones, ambient to 450 °C 
  • Dedicated cold trap: Yes
  • Available methods: flow and vacuum, programmable multistep degassing profiles
Vapor option: Yes (water, isopropanol, benzene, hexane, cyclohexane, xylene, and other non-corrosive vapors)
Cryosync control option: Yes (automated control of temperature between 82 K and 115 K) 
Dimensions (W x H x D): 70.5 x 69.9 x 107.9 cm | 27.8 x 26.5 x 42.5 in
Weight: 128.4 kg | 283.1 lb
Operating environment:
  • Temperature: 15 °C to 35 °C | 59 °F to 95 °F
  • Humidity: 20% RH to 80% RH, non-condensing
Wetted parts:
  • 303 SS
  • 304 SS
  • 316 SS
  • Ni/Cr/Si/Fe/C/P
  • PCTFE
  • NW2201
  • Inconel and incoloy nickel alloys
  • FKM
  • Silicon
  • SiO2
  • Si3N4
  • Gold
  • Copper
  • Aluminum
  • EPDM
  • Nylon
  • Borosilicate glass
  • Fused silica glass
Analysis manifold construction: Vacuum-brazed manifold block in stainless steel
Analysis manifold temperature:
  • Range: User adjustable 35 °C to 50 °C 
  • Stability: ± 0.05 °C
Analysis manifold valves:
  • Type: Stainless steel, air-operated bellows valve 
  • Cycle life: 5,000,000 cycles
  • External leak rate: 5x10-12 Pa m3 / sec
  • Seat leak rate: 5x10-12 Pa m3 / sec
Pressure transducer (1550 Torr):
  • Number: 3 to 5 (dependent on instrument configuration)
  • Accuracy: ± 0.1 % of span typical, ± 0.15 % of span maximum
  • A/D data acquisition: 32 bit
Pressure transducer (10 Torr):
- MP or XR
  • Number: 1 to 3 (dependent on instrument configuration)
  • Accuracy: ± 0.12 % reading up to 1 Torr 
                     ± 0.1 % reading from 1 to 10 Torr
  • Resolution: 0.002 % full scale
Pressure transducer (1 Torr):
- MP only
  • Number: 1 to 3 (dependent on instrument configuration)
  • Accuracy: ± 0.12 % reading up to 1 Torr
  • Resolution: 0.02 % full scale 
Pressure transducer (0.1 Torr):
- XR only
  • Number: 1 to 3 (dependent on instrument configuration)
  • Accuracy: ± 0.15 % reading up to 0.1 Torr
  • Resolution: 0.001 % full scale 
Pirani vacuum gage:
- Degas only
  • Number: 1 
  • Accuracy: 
    5×10-4 to 1x10-3 Torr: ±10% of reading
    1×10-3 to 100 Torr: ± 5% of reading
    100 Torr to atmosphere: ± 25% of reading 
Vacuum system:
  • Turbo molecular drag pump and dry diaphragm pump 
  • Manufacturer’s specification: 5x10-10 mbar
  • Typical pressure at analysis port: 2.67 x 10-5 mbar
Gas:
  • Ports: 7 (5 analysis, 1 helium, 1 degas/backfill) 
  • Purity: 99.999 %
  • Input pressure: 8 psig to 10 psig | 0.55 bar to 0.69 bar
Air: Input pressure: 50 psig to 100 psig (3.45 bar to 6.9 bar)
Electrical:
  • Supply: AC 100 to 240 V AC, 50 / 60 Hz 
  • Maximum consumption: 1810 VA (dependent on instrument configuration)
PC connection: Ethernet
RoHS3 compliant: Yes
CE / UKCA certified Yes
Altitude: Up to 3,000 m
Indoor/outdoor use: For indoor use only

Standards

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ASTM

B922
C1069
C1274
D1993
D3663
D4222
D4365
D4641
D4780
D6556

DIN

66134
66135-1
66135-2
66135-3
66135-4

ISO

9277
15901-2
15901-3
18757

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The Anton Paar quality in service and support:
  • More than 350 manufacturer-certified technical experts worldwide
  • Qualified support in your local language
  • Protection for your investment throughout its lifecycle
  • 3-year warranty
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SAMPLE CELL ADAPTOR, 6 mm

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Part number: 193362

Cryostat accessory for autosorb iQ:
CryoSync 

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Product details
  • Wide temperature range (82 K to >115 K)
  • Precise temperature control (temp. stability < ±0.005 K S.D.)
  • Perfect for argon isotherm measurements without using liquid argon or for multi-isotherm heat of adsorption experiments
  • Runs for over 50 hours without refilling

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