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Analyzátory mikroporovité fyzické sorpce a chemisorpce:
autosorb iQ

Mikroporézní fyzisorpční/chemisorpční analyzátory

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Tyto vysoce citlivé analyzátory sorpce plynu používají patentovanou technologii malých chlazených zón pro detailní analýzu distribuce velikosti mikropórů až tří vzorků najednou. Realizují ta nejnáročnější měření zeolitů, aktivního uhlí a MOF v rámci výzkumu nových materiálů v průmyslových a ekologických aplikacích, jako jsou skladování plynu či superkondenzátory. Jejich integrované vnitřní vývěvy a specializované stanice pro přípravu vzorků minimalizují prostorové nároky. Jsou k dispozici v různých konfiguracích jako chemisorpční jednotky, které stále disponují i kompletní schopností měření fyzisorpce, pro ucelenou charakterizaci katalyzátoru způsobem „all-in-one“.

Technical specifications

Snímače tlaku
XR stanice 0,1 torr + 10 torr + 1000 torr
MP stanice 1 torr + 10 torr + 1000 torr
AG stanice 1000 torr
Přesnost tlaku
0,1 torr, 1 torr <±0,15 % z odečtu
10 torr <±0,12 % z odečtu
1000 torr <±0,11 % z celého rozsahu
Vestavěný vakuový systém
Vysokovakuová konstrukce Těsnění „kov na kov“ v kritických zónách měření
Vakuový systém (XR/MP) Turbomolekulární vývěva a suché membránové čerpadlo
Nejvyšší dosažitelné vakuum (XR/MP) 5 x 10⁻¹⁰ mbar (5 x 10⁻⁸ Pa) (3,75 x 10⁻¹⁰ mm Hg)
Vakuový systém (AG) Dvoustupňové rotační olejové čerpadlo s předsazeným záchytem kondenzátu
Nejvyšší dosažitelné vakuum (AG) <2,5 x 10⁻³ mm Hg (<3,3 x 10⁻³ mbar)
Fyzisorpční schopnosti
Analytické stanice 1, 2 či 3
Měřené parametry Distribuce velikosti pórů, objem pórů, plocha povrchu
Adsorbáty N₂, Ar, Kr, CO₂, O₂, H₂, CH₄, atd.
Chemisorpční schopnosti
Analytické stanice 1
Měřené parametry Aktivní (kovová) oblast, disperze, velikost krystalitů
Chemisorbované množství Kombinované, reverzibilní (slabé), nevratné (silné)
Chemisorpční monovrstva Extrapolace, Langmuir, disociační Langmuir, Freundlich, Temkin
Parametry katalyzátoru Aktivní (kovová) oblast, disperze, velikost krystalitů
Chemisorpční entalpie Clausius-Clapeyron
Průměr kapiláry cely 6 mm, 12 mm
Chemisorpční pec
Typ Keramická trubková pec s bezpečnostním tepelným štítem
Maximální teplota 1100 °C
Přesnost teploty 0,1 % rozsahu
Teplotní stabilita ±1 °C
Rychlost navyšování 1 °C až 50 °C za minutu
Maximální teplota 1100 °C
Chlazení pece Vestavěný ventilátor
Pec / uzávěr pece / separace Automatický
Adsorbáty N₂, Ar, Kr, CO₂, O₂, H₂, NH₃, atd.

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Consumables & Accessories

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Cell-Seal, 12mm, Buna

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Part number: 222959

Cell-Seal, 9mm, Buna

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Part number: 222935

COLD TRAP TUBE

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Part number: 193628

DEWAR, 350 mL

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Part number: 193629

Dowel Pin, 12 mm

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Part number: 197827

Dowel Pin, 6 mm

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Part number: 197598

Dowel Pin, 9 mm

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Part number: 194983

Level Sensor, Hybrid type, 77 K, long

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Part number: 195455

Level Sensor, Hybrid type, 87 K, long

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Part number: 197483

Mantle, Lg, Male Inlet, 2 Mini J

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Part number: 193466

Non-elutriating Plug 12mm, Metal, Buna

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Part number: 222961

Non-elutriating Plug 9mm, Metal, Buna

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Part number: 222937

Non-elutriating Plug, 6 mm

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Part number: 193257

Non-elutriating Plug, 9 mm

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Part number: 193256

O-Ring, Buna 010, Black

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Part number: 193783

O-Ring, Buna 015, Black, Pack of 2

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Part number: 193786

O-Ring, EPDM 12 mm, Purple, Pack of 2

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Part number: 193831

O-Ring, EPDM 6 mm, Purple, Pack of 2

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Part number: 193832

O-Ring, EPDM 9 mm, Purple, Pack of 2

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Part number: 193833

O-Ring, PFE 12 mm, Black

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Part number: 193836

O-Ring, PFE 6 mm, Black

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Part number: 193837

O-Ring, PFE 9 mm, Black

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Part number: 193838

O-Ring, Viton 010, Brown, Pack of 2

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Part number: 193808

O-Ring, Viton 12 mm, Brown, Pack of 2

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Part number: 193817

O-Ring, Viton 6 mm, Brown, Pack of 2

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Part number: 193820

O-Ring, Viton 9 mm, Brown, Pack of 2

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Part number: 193821

Quartz Wool, pack of 2.5 g

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Part number: 193227

Sample Cell Cap, FOR 6/9/12 mm Stems

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Part number: 193680

Septum [Pack of 2]

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Part number: 193668

Stem Cleaner, 6mm X 18" (Pack of 18)

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Part number: 193684

Surface Area Reference Material, 2003

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Part number: 193439

Surface Area Reference Material, 2005

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Part number: 193441

Surface Area Reference Material, 2009

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Part number: 193443

Surface Area Reference Material, 2012

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Part number: 193445

Type C macro cell, cap

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Part number: 193624

Vacuum Grease .25 Ounce

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Part number: 193946

Vacuum Hose Assembly, 5' (1.5 m)

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Part number: 221014

Vacuum Pump Oil, Pfeiffer, 1 L

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Part number: 193678

VCR Gasket, 1/4 inch, Ag

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Part number: 196507

ASIQ P0 CELL

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Part number: 193928

FOAM SAMPLE CELL HOLDER FOR BALANCE

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Part number: 194981

Funnel, 6 mm Opening, 6/9/12 mm Cell

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Part number: 193369

Funnel, Long Stem Glass, 9/12 mm Cells

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Part number: 193663

Kryostatické příslušenství pro autosorb iQ:
CryoSync

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P0 Cell, Bent SM Bulb, 306 mm Long

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Part number: 193851

Sample Cell Adapter, 12 mm

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Part number: 193364

Sample Cell Adapter, 6 mm

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Part number: 193362

Sample Cell Adapter, 9 mm

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Part number: 193363

Type A long cell, 12 mm LG bulb

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Part number: 193910

Type A long cell, 12 mm LG bulb, dimple

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Part number: 193911

Type A long cell, 12 mm NO bulb

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Part number: 193909

Type A long cell, 6 mm LG bulb

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Part number: 193913

Type A long cell, 6 mm LG bulb, dimple

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Part number: 193914

Type A long cell, 6 mm LG bulb, quartz

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Part number: 193915

Type A long cell, 6 mm SM bulb, dimple

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Part number: 193917

Type A long cell, 6 mm SM bulb, quartz

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Part number: 197846

Type A long cell, 6 mm SM bulb70179000

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Part number: 193916

Type A long cell, 9 mm LG bulb

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Part number: 193918

Type A long cell, 9 mm LG bulb, dimple

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Part number: 193919

Type A long cell, 9 mm LG bulb, quartz

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Part number: 193921

Type A long cell, 9 mm NO bulb

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Part number: 193922

Type A long cell, 9 mm NO Bulb, quartz

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Part number: 193924

Type A rod, for 12 mm long cell

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Part number: 193925

Type A rod, for 6 mm long cell

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Part number: 193926

Type A rod, for 9 mm long cell

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Part number: 193927

Type B rod, for 9 mm short cell

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Part number: 193903

Type B short cell, 9 mm SM bulb

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Part number: 193880

Type C long cell, thin film

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Part number: 193660

Type C macro cell, stem

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Part number: 193625

Type C rod, for 12 mm long cell

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Part number: 193873

Type D cell, 6 mm Cylindrical Bulb

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Part number: 197843

Type D cell, 9 mm Cylindrical Bulb

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Part number: 197844

Type E long cell, 12 mm, quartz

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Part number: 193643

Type S rod, for cryocooler short cell

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Part number: 193907

Volume / Vapor Cell 13 cm3

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Part number: 193657