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Microwave Digestion Platform:
Multiwave 5000

  • media
  • +8
  • 360°
  • A single microwave digestion platform for all your needs
  • >500 pre-installed programs, guiding features, and a 'clever' door
  • Up to 64 samples in a single run; tool-free vessel handling; 2x faster vessel opening/closing
  • 10,1" high-resolution, durable touchscreen display

40 years’ sample preparation expertise driving the most ambitious, user-friendly microwave digestion system ever built: Digestion of a broad array of samples (varying in difficulty or volume), acid leaching, solvent extraction, evaporation, microwave-induced O₂ combustion, sample drying and synthesis. A comprehensive, interactive method library. A customizable, intuitive user interface, and modern sensor technology, together with Anton Paar’s easy-to-handle compact rotors. 500 pre-installed programs. A very ‘clever’ door. Multiwave 5000. The lab chemist’s dream.

Benefits

  • More than 500 programs
  • Full-text database search
  • Add your own methods if needed

Challenge

Sometimes, it can be difficult to predict which conditions are required for full digestion, or how a sample will react – especially when dealing with unknown or frequently changing samples.

Solution

With a database of more than 500 methods, Multiwave 5000 eases your workload. Use sample tags to search for your application and Multiwave 5000 will provide you with the program – and even recommend a recipe – directly on the instrument, without any paperwork. 

Benefit

A pre-installed method library of >500 programs gives you access to the most comprehensive application knowledge base on the market. No need to spend hours of valuable lab time developing the right method.

SmartScreen
SmartScreen
  • Shortcuts to often-used programs and features
  • Start your experiment right from the SmartScreen

Challenge

Conventional user interfaces make you go through pages and pages of menus and lists each time you’re in front of the instrument. 

Solution

SmartScreen lets you configure the home screen according to your needs: define shortcuts to often-used programs, menu links, or experiment data.

Benefit

Save time, nerves and money by configuring the Multiwave 5000 home screen, so the instrument behaves like it’s truly yours.

Video manuals
Video manuals
  • Extensive video library with in-depth explanations

Challenge

You’re not an expert in analytical chemistry but you have to perform acid digestion procedures in your lab. You need an instrument that is easy to operate.

Solution

Questions? Simply watch the video manual directly on the screen. 

Benefit

We guide you through the whole process step-by-step.

Hands-free door opener
Hands-free door opener
  • A 'clever' door indeed

Challenge

You’re standing in front of the instrument with a fully loaded rotor, and the door is closed.

Solution

With the unique hands-free door opener, all you need to do is push gently against the door. You can do it with your elbow – no need to set the vessels or rotor aside.

Benefit

It's the simple things: Multiwave 5000 takes convenience to the next level.

All kinds of samples
All kinds of samples
  • SmartVent technology: Safe overpressure release – for higher sample amounts, higher temperatures and various samples in one run
  • Ingenious sensor technology for the best reaction control

Challenge

Some samples are challenging, they have changing compositions, or their reactivity is unknown. 

Solution

Multiwave 5000 and its various rotors are designed for any challenge. Premium operation parameters and a supreme reaction control – with the seal of Austrian quality – allow for complete digestion of even the most demanding samples. 

Benefit

Our rotors, especially those with SmartVent technology, are designed for a broad range of samples – from routine ones like food, feed, or environmental samples, to demanding ones like ceramics, oil, polymers, and petroleum. 

Future-proof
Future-proof
  • Acid digestion and leaching
  • Solvent extraction and synthesis
  • Special solutions: Microwave-induced O2 combustion etc.

Challenge

Some samples require special treatment beyond microwave acid digestion.

Solution

Multiwave 5000 goes beyond digestion: perform other sample preparation techniques or even synthesis. Microwave heating technology makes all these methods faster, safer, cleaner, and more cost-efficient than classic, conventionally-heated alternatives. 

Benefit

Multiwave 5000 is a future-proof instrument. With the broadest portfolio available, you can extend your setup – rotors from previous models can be carried over.

SmartVent technology
SmartVent technology
  • Digestion of a large variety of samples
  • Up to 50 % higher sample quantities
  • Samples with varying reactivity in a single run

Challenge

Final digestion temperature and sample weight are often limited by the pressure built up during the digestion reaction.

Solution

The use of SmartVent technology is a reliable way to deal with overpressure. 

Benefit

Thanks to the controlled release of reaction gases, maximum digestion temperatures are attained independent of the applied sample amounts.

Intelligent vessels
Intelligent vessels
  • SmartVent technology for reliable release of overpressure
  • Cooling fins and guided airflow enable fast cooling
  • Varying vessel volumes; compact, easy-to-handle vessel design

Challenge

Long liners, lots of vessel components, difficult cleaning and unsafe operation of conventional vessels are downsides in the lab. 

Solution

The practical design of the SmartVent vessels – available in different volumes – facilitates all steps of operation: from sample weighing and reagent addition to closing, opening, and cleaning.

Benefit

Fast, safe, tool-free operation providing new levels of performance and convenience for the sample preparation lab.  

Tool-free vessel handling
Tool-free vessel handling
  • Tool-free assembly
  • HVT and SVT: Only three vessel parts
  • Optimized surface and compact design for less adsorption and easier cleaning

Challenge

Setup, but also alignment and cleaning of vessel parts, can be tedious. Tools get lost in the lab and additional handling steps can mean setting up an experiment takes longer than the experiment itself.

Solution

Opening and sealing Multiwave 5000's rotors, vessels, and sensors is quick and simple – just use your hands.

Benefit

Unique tool-free handling makes closing and opening vessels twice as fast. 

Super-high throughput
Super-high throughput
  • Rotor 41HVT56: highest throughput for routine samples
  • Rotor 20SVT50: high-performance rotor with the highest throughput on the market
  • Up to 64 samples in disposable glass vials

Challenge

Super-high throughput and fast turnover times are often requirements in elemental analysis. 

Solution

Anton Paar’s rotors are robust, lightweight, and accommodate more samples on a smaller footprint.

Benefit

The practical design of our vessel impacts all operation steps: from sample weighing and reagent addition, to closing, opening, and cleaning. Digest up to 64 samples in a single run.

Safety features
Safety features
  • Each instrument is tested individually
  • Active and passive safety features
  • ETL and GS certificates

Challenge

Safety is non-negotiable, especially at elevated temperatures and pressures. 

Solution

Multiwave 5000 comes with active and passive safety features: self-checks, software interlocks, and a resealing safety door. This way, users and equipment are protected.

Benefit

Each instrument is tested individually, but beyond that, Multiwave 5000 is the only sample preparation microwave platform with ETL and GS “approved safety” certificates from independent testing institutes.

Sensor technology
Sensor technology
  • SmartTemp: Contactless internal temp. measurement (SVT/HVT)
  • SmartVent detection for registration of venting events

Challenge

Correct temperature and pressure control are the key to reliable results. Conventional sensors require extensive efforts to set up, employ only one control strategy, or react slowly due to infrequent vessel control or temperature measurement solely in a reference vessel. 

Solution

Comprehensive reaction control is guaranteed thanks to temperature and pressure control for each position, including various control strategies for the simultaneous digestion of different sample types. Our newest additions: SmartTemp temperature sensor and SmartVent detection (for identification of venting events).

Benefit

Reaction control is easier and safer than ever before: The new SmartTemp sensor combines the fast temperature feedback of an internal temperature probe with the convenience of an infrared sensor. 

Connectivity
Connectivity
  • Visualization of the instrument's status
  • Connect your Multiwave 5000 to the technology of your choice

Challenge

Work interruptions can be annoying and time-consuming. Especially if you have to change rooms to check if everything is running smoothly, or if the experiment has finished.

Solution

The color and mode of SmartLight reflect whether an experiment is in progress, finished, or on standby. SmartLink connects Multiwave 5000 to your PC, notebook, tablet, or mobile phone, so you can monitor and operate experiments remotely.

Benefit

No need to dash over from your desk to check if the run is finished – just cast a glance from afar. Automated notifications keep you informed, whether you’re in the lab or on the go.

Technical specifications

The main acid digestion rotors of Multiwave 5000:*

 

  Rotor 24HVT Rotor 41HVT Rotor 20SVT Rotor 8 NXF/NXQ Rotor 64MG5
Number of vessels 24 41 20 8 64
Volume 50 mL/80 mL 56 mL 50 mL 100 mL/80 mL 5 mL
Material PTFE-TFM PTFE-TFM PTFE-TFM PTFE-TFM / Quartz Glass
HF resistance Yes Yes Yes Yes (NXF) No
Temperature control Internal T in all positions / SmartTemp SmartTemp T in all positions IR in 16 positions
Pressure control SmartVent technology / SmartVent detection p in all vessels PTFE seal
Applications Routine samples: Biological and environmental samples, EPA procedures, food, cosmetic and pharmaceutical samples Harder to digest samples: including polymers, ceramics, petroleum products, and alloys Most difficult samples Micro samples up to 20 mg

*Multiwave 5000 can be used with the digestion rotors (Rotor 16MF100 and 16HF100) of Multiwave PRO as well

Standards

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ASTM

D4309
D5258
D5513
D5765
D6010
D7210
D7876
D7879

Chinese Pharmacopoeia (ChP)

2321

EN

13346
13656
13657
13804
13805
13806
14083
14084
14332
14385
14627
14902
15297
15411
15763
15764
15765

EN ISO

15587-1
15587-2

EPA

3015
3051
3052
3546

GA

T1662

GB

5009
T24533
T26125
T 36592
T 36593
T 38287

HJ

491
678
680
702
703
765
766
781
803
832
921
922

ICH

Q3D Guideline

JIS

K0050

Japanese Pharmacopoeia (JP)

General Tests, Processes and Apparatus 2.63

Pharmacopoeia Europe (Ph. Eur.)

5.20

U.S. Pharmacopoeia (USP)

232 - Elemental impurities - limits introduction
233 - Elemental impurities - procedures

Anton Paar Certified Service

The Anton Paar quality in service and support:
  • More than 350 manufacturer-certified technical experts worldwide
  • Qualified support in your local language
  • Protection for your investment throughout its lifecycle
  • 3-year warranty
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Accessories

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VESSEL JACKET M100 PEEK

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Supporting jacket for Pressure Vessels MF100 and SOLV100, made of fibre-reinforced PEEK.

SCREW CAP SOLV

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PRESSURE VESSEL SOLV HF100

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Complete reaction vessel for solvent extraction applications. The 100 mL liner is made of PTFE-TFM and supported by the Vessel Jacket H100 Ceramics. A screw cap with a PTFE-TFM seal SOLV closes the vessel. Volume of vessel: 100 mL Working pressure: 18 bar (260 psi) Opening pressure: 22 bar (320 psi) Max. temperature: 240 °C

DISPOSABLE INSERT HVT80 (100 PCS)

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Borosilicate glass-vial for HVT80 vessels

PRESSURE VESSEL SVT50

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Complete pressure vessel SVT50 providing SmartVent technology for the controlled release of overpressure. SmartVent technology allows to digest samples with different or unknown reaction behavior and higher sample amounts in one run. Easy to assemble vessels out of three parts without the need for any additional tools. SVT50 vessels are made out of PTFE-TFM and are ideal for the digestion of various samples, including food, environmental and pharmaceutical applications but also more demanding samples such as ceramics, alloys, polymers, cosmetics, geological materials, petrochemicals, chemicals, and samples from refractories.

SEAL FOR PRESSURE VESSEL SVT

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SCREW CAP SVT (ASSEMBLED)

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ROTOR LID FOAM 20SVT (5 PCS)

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Replacement rotor lid foam for rotor SVT

STIR BAR PTFE

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D = 6 mm, L = 20 mm

DRIVE BEARING

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DRIVE STAR

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PRESSURE VESSEL HF100

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Complete reaction vessel for reactions at medium pressure and temperature, with a self-sealing lip type seal, a PTFE-TFM liner and a ceramic pressure jacket. Volume of vessel: 100 mL Working pressure: 40 bar (580 psi) Opening pressure: 70 bar (1000 psi) Max. temperature: 240 °C

SEAL FOR VESSEL HOLDER

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SEAL FORMING DEVICE FOR 8 CAPS

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Safe and clean storage for XF/XQ seals and Screw Cap M&H. Provides proper, timesaving closing, and longer service life.

CENTRE RING

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SYRINGE FILTER

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D = 25 mm, PP/PTFE, 0.2 µm

SAFETY DISK SOLV

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SCREW PEEK M3X6

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SEAL HUSK S

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RACK 16

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Made of polyethylene foam for keeping all vessels and liners of Rotor 8 and 16 in place or transporting them safely.

HEATING ELEMENT D = 10, H = 18

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Standard cylindrical heating element (d=10 mm, h=18 mm), made of sintered silicon carbide (SiC) for use in XQ80 and MF/HF/ XF100 vessels.

SEAL SOLV C

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IR CAP

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MULTIWAVE 3000 FOAM PACKAGE

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PRESSURE VESSEL HVT80

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HVT80 vessel providing SMART VENT technology. SMART VENT technology enables the digestion of high sample amounts and of samples with different or unknown reaction behaviour in one run. The vessel made of PTFE-TFM (80 mL) is optimized for a broad range of samples including agricultural samples, food, waste water, sludge, soil, sediment and standard test methods as EPA 3015A, 3051A, 3052 oder EN ISO 15587.

CAP NXF (ASSEMBLED)

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Complete cap for Pressure Vessel NXF100 for Rotor 8N. Comes with: 102865 SEAL HOLDER NX 1 pcs. 104286 SEAL NXF 1 pcs. 10359 SAFETY DISK X 1 pcs. 10358 SAFETY DISK HOLDER X 1 pcs. 2722 SYRINGE CONNECTOR 1 pcs. 104284 VENTING SCREW N 1 pcs.

PRESSURE VESSEL HVT 56

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Complete pressure vessel HVT56 providing SMART VENT technology. The vessel made of PTFE-TFM (56 mL) is optimized for the digestion and acid leaching of all kinds of samples including biological, environmental, agricultural, cosmetic and pharmaceutical samples. The 176269 Vessel Body HVT56 is sealed with the 104454 Seal for Pressure Vessel HVT and closed by the 104453 Screw Cap HVT (Assembled).

RACK 10SVT

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DISPOSABLE INSERT HVT50/56 (100 PCS.)

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Borosilicate glass-vial for HVT50 and HVT56 vessels

QUARTZ INSERT SVT50

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Reusable quartz vial for SVT50 vessels

ROTOR LID FOAM 24HVT (5 PCS)

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Replacement rotor lid foam for Rotor 24HVT.

Microwave Digestion Rotor:
Rotor 12HVT50 

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  • A rotor for the microwave reaction platform Multiwave 5000
  • Acid digestion of up to 12 samples in one run
  • SmartVent technology handles higher temperatures, heavier sample weights, and samples with different reaction behaviors in one run
  • Ideal for routine samples (e.g., environmental, agricultural, food)

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WIFI/BLUETOOTH DONGLE

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Part number: 194727

Closing Station HVT

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  • Ideal for high-throughput laboratories
  • Reproducible closing of all HVT vessels
  • Easy, self-explanatory operation

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Disposable Glass Vials for Vessels with SmartVent Technology

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Accessory for HVT Rotors:
24EVAP 

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Microwave Digestion Rotor:
20SVT50 

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  • Rotor for Multiwave 5000
  • Ideal for the digestion of demanding samples
  • Highest sample throughput (20 samples in a run)
  • SmartTemp temperature measurement for optimum reaction control
  • Only three parts allows tool-free, easy handling of the vessel

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Rotor Stand

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For the evaporation of reagents and aqueous solutions using Rotor 8EVAP a scrubber accessory is required. It consists of a set of washing bottles with highly efficient gas diffusers, a chemically resistant vacuum pump and a lead-through connecting the outlet of Rotor 8EVAP to the washing bottles. This lead-through can be installed in every Multiwave PRO.

Scrubber Accessory

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Microwave-induced oxygen combustion is an innovative method for sample preparation for all kinds of combustible solids such as wood, paper, coal, food or polymers.

Oxygen Combustion Set

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  • Accessory for Rotor 8NXQ
  • Suitable for all combustible solids
  • Modern alternative to steel combustion bombs
  • Parallel combustion of up to 8 samples
  • No electrical components or ignition wires

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Magnetic Stirrer Device

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  • Accessory for microwave reaction systems
  • Stirring improves leaching and extraction processes
  • Supports acid digestion of floating samples
  • Different speeds selectable
  • Retrofittable

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Safety Module SOLV

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  • Accessory for microwave reaction systems
  • Ensures safe solvent extraction and microwave-assisted synthesis
  • Fail-safe design for maximum safety
  • Can be retrofitted to existing setups

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The seal forming device enables the proper pre-forming and safe storage of seals and screw caps of Rotor 8 and 16. One unit has a capacity for 8 caps/seals of different kinds. Storage in this device prolongs the lifetime of the lip-type seals.

Seal Forming Device

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Hydrolysis Set

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  • Protein hydrolysis accessory for microwave reaction systems
  • Protein hydrolysis of milligrams to grams
  • Samples processed in less than one hour
  • For up to 60 samples in one run
  • Inert gas can be applied

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The cylindrically shaped passive heating elements are made of sintered silicon carbide (SiC). Due to its high microwave absorbance and excellent heat capacity, SiC can be used to efficiently heat low-absorbing solvents (toluene, dioxane, THF…) in a microwave environment.

Passive Heating Elements

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  • Accessory for microwave reaction systems
  • Made of sintered silicon carbide (SiC) to provide high microwave absorbance and excellent heat capacity
  • Purchase once and reuse again and again
  • Chemically inert and easy to clean

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Different racks are available for the adequate storage of the various vessel types and liners of Multiwave PRO as well both vial sizes of Monowave 300. For vessels applicable in the multimode reactors Anton Paar supplies Rack 16, a polyethylene foam block for 16 vessels or liners of Rotor 8 and Rotor 16.

Racks

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  • Different racks for storing vessels, liners, and vials
  • For Multiwave 5000: Rack 12 for HVT vessels, Rack 10 for SVT vessels, Rack 16 for 16 vessels or liners of Rotor 8 and Rotor 16
  • For Monowave 200/400/450: 24 x 30 mL vials and 40 x 10 mL vials

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Pressure/temperature sensor accessory for precise reaction control within the reference vessel of Rotor 16MF100 and/or Rotor 16HF100.

p/T Sensor Accessory

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  • Accessory for Rotor 16MF100 or Rotor 16HF100
  • Precise reaction control within a reference vessel
  • Simultaneous pressure and temperature measurement up to 86 bar (1250 psi) and 280 °C

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The pressure sensor accessory allows for precise reaction control within the reference vessel of Rotor 16MF100 or Rotor 16HF100. The pressure data is transferred to the oven via infrared signal. If required, the pressure sensor accessory can be upgraded to a pressure/temperature sensor accessory.

Pressure Sensor Accessory

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