Nanomaterials

ナノ材料

ナノ材料の特性をより深く理解し調整する上で、材料のナノ構造は極めて大きな意味を持つ要素です。用途に合った工業材料の製造には、構造の成り立ちを理解することが非常に重要になります。アントンパール社は、X線散乱や粘弾性測定など、ナノ材料の合成及び分析のための様々な測定ソリューションを提供しています。下記の装置リストでは、お客様固有の様々なニーズに応える測定装置をご紹介しています。また、当社に直接お問い合わせいただければ、最適なソリューションを見つけるお手伝いをいたします。

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Anton Paar 製品

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4軸ゴニオメータ用のドーム型冷却ステージ: DCS 500

DHS 1100は、グラファイト製ドームを備えた4軸ゴニオメーター用のドーム型加熱ステージです。25~1100 °Cまでの多結晶サンプルや薄膜のX線回折に使用されます。

4軸ゴニオメータ用のドーム型加熱ステージ:DHS 1100

マルチウェーブ屈折計Abbemat WR/MW

Abbemat MW多波長屈折計

Anton Paarバイオインデンタ(UNHT³ Bio)

HTR: 高サンプルスループット及び複雑なサンプル処理を実現するレオメータ自動化

HTRコンパクト: 高サンプルスループットを実現するレオメータオートサンプラー

HTX: 液体の粘度、密度、濃度の測定、高度に自動化かつ拡張可能

Litesizer™ 100

Litesizer™ 500

PC制御可能な調整ステージ

SAXS/WAXS/GISAXSラボ用ビームライン: SAXSpoint 2.0

インダストリアルタイプカロテスト(CAT²i)

ウルトラナノインデンテーションテスタ: UNHT³

高温チャンバHTK 1200Nは、1200 °Cまでの高温で、反射法と透過法を組み合わせたXRD測定に使用されます。

キャピラリーエクステンション:HTK 1200N

革新的な新技術に基づく全く新しいMasterwave BTRベンチトップ・リアクターにより、キロ単位規模でのマイクロ波合成が初めて実現しました。研究室での生産性を大幅に(1日当たりの処理量をキログラム規模にまで)拡大できます。ベンチトップ・リアクターの磁気駆動式スターラーにより、対象それぞれに適した方法で撹拌が可能です。差し込み式センサーを使用した温度測定技術を採用したMasterwave BTRは、任意の小容量タイプのマイクロ波装置からメソッドを直接移行するのに必要な温度精度を備えています。

キロ単位規模のマイクロ波合成:Masterwave BTR

ナノインデンテーションテスタ: NHT³

ナノスクラッチテスタ: NST³

ピンオンディスクトライボメータ: TRB³

マイクロインデンテーションテスタ(MHT³)

マイクロコンビテスタ(MCT³)

マイクロスクラッチテスタ(MST³)

マイクロ波でサンプルを濃縮するローター8EVAPは、モジュール型のマイクロ波サンプル前処理システム、Multiwave PRO用の革新的なアクセサリーです。8つの容器で同時に処理できるため、マイクロ波加熱を利用した酸とサンプル水溶液の濃縮作業を大幅に簡略化し、時間を短縮します。

マイクロ波による気化: ローター8EVAP

16の耐高圧容器を備えた酸分解ローター16HF100は、高速サンプルスループットと効率的な処理の実現を目指して設計された製品です。

マイクロ波前処理装置: ローター16HF100

16の耐圧容器を備えた酸分解ローター16MF100は、高速サンプルスループットと効率的な処理の実現を目指して設計された製品です。

マイクロ波前処理装置:ローター16MF100

ローター1DRYは、分解前サンプルの効率的な処理に最適なアクセサリーです。マイクロ波加熱による乾燥は、従来の方法と比較して所要時間が4分の1と短く、サンプルの炭化や汚染もありません。

マイクロ波加熱による乾燥: ローター1DRY

マイクロ波合成Monowave 400/200

ローター16SOLV HF100はマイクロ波加熱による有機及び無機サンプルの分解・抽出に対応し、Multiwave PROの可能性を広げます。スクリューキャップを交換すれば、簡単に酸分解用にアップグレードできます。

マイクロ波抽出: ローター16SOLV HF100

ローター16SOLV MF100はマイクロ波加熱による有機及び無機サンプルの分解・抽出に対応し、Multiwave PROの可能性を広げます。スクリューキャップを交換すれば、簡単に酸分解用にアップグレードできます。

マイクロ波抽出: ローター16SOLV MF100

レオメータ: MCR 102、MCR 302、MCR 502

レオメータ:MCR 72 / MCR 92

レベテスト®スクラッチテスタ(RST³)

低温チャンバー:TTK 600

低温・高湿チャンバCHC plus+は、汎用のCHC低温・高湿チャンバに高度な湿度(RH)発生器を組み合わせた独自の製品です。X線回折を使用して、湿度または温度に依存する材料の構造変化を分析できます。

低温・高湿チャンバー:CHC plus⁺

動的粘弾性レオメータ測定ヘッド: DSR 502

Reactor Chamber: XRK 900

反応チャンバー:XRK 900

固体表面分析用ゼータ電位測定装置: SurPASS™ 3

密度・比重・濃度計: DMA 4100 M

密度・比重・濃度計: DMA 4500 M

密度・比重・濃度計: DMA 5000 M

密度・音速計: DSA 5000 M

Abbematスタンダード

屈折計: Abbematシンプルライン及びスタンダードライン

Abbemat Heavy Duty

屈折計: Abbematプロフェッショナルライン

引張ステージTS 600 - 繊維やホイル、薄膜の応力/歪み現象のIn-Situ X線回折に使用するサンプルステージです。

引張応力ステージ:TS 600

携帯型ラマン分光計: Cora 100

SAXspace装置

日常的なSAXS/WAXS/BIOSAXS分析: SAXSpace

日常的な固体表面分析向けのルーチン分析用固体表面ゼータ電位測定装置: SurPASS™ 3 Eco

Multiwave PROのローター8Nに温度プローブを取り付けた場合の上面図。

温度プローブ

High Temperature Vacuum Tribometer

真空トライボメータ(VTHT/VTRB)

粒子分析用ソフトウェア: Kalliope™

落球式粘度計Lovis 2000 M/ME

超高温加熱炉レオメータシステムFRS 1600及びFRS 1800

高圧チャンバHPC 900は、気体-固体間の相互作用を分析するIn-Situ X線回折のための高温・高圧チャンバです。

高圧チャンバー:HPC 900

高温ウルトラナノインデンテーション(UNHT³ HTV)

HKT 1200N - 堅牢な設計の高温チャンバで、1200 °Cまでの様々な雰囲気下でのIn-Situ X線回折に使用されます。

高温オーブンチャンバー:HTK 1200N

高温ストリップヒーターチャンバー:HTK 16N | HTK 2000N

Temperature Tribometer

高温トライボメータ(THT)

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Anton Paar 用途

Better Sample Preparation of Polymers - Microwave-induced Oxygen Combustion (MIC)

Better Sample Preparation of Polymers - Microwave-induced Oxygen Combustion (MIC)

If you have any problems with digesting plastic & polymer samples for elemental analysis due to inhomogeneity or high residual carbon content think about the unique microwave-induced oxygen combustion from Anton Paar.

Improve Digestion Quality and Save Money – Microwave Digestion rules out Open Digestion

Improve Digestion Quality and Save Money – Microwave Digestion rules out Open Digestion

Reliable elemental analysis results need robust sample preparation to destroy sample matrices or to separate matrix from analytes. The sample preparation step is by far the most error-prone and critical step of the analytical procedure.

Mesoporous thin films - Investigating the structure of multi-layered films by GISAXS

Mesoporous thin films - Investigating the structure of multi-layered films by GISAXS

Single- and double-layered mesoporous thin films have been analyzed by GISAXS for their structural properties using the SAXSpoint system.

Characterization of the scratch resistance of ceramic tiles

Characterization of the scratch resistance of ceramic tiles

High temperature tribological behavior of advanced hard coatings for cutting tools

High temperature tribological behavior of advanced hard coatings for cutting tools

High temperature tribological behavior of advanced hard coatings for cutting tools

The influence of Surface Roughness on Instrumented Indentation Testing (IIT)

The influence of Surface Roughness on Instrumented Indentation Testing (IIT)

In-Situ observation of the scratch/indentation true contact area to provide analysis without being model-dependent

In-Situ observation of the scratch/indentation true contact area to provide analysis without being model-dependent

Nanoindentation and Nanoscratch of Oxide Coatings on Thin Film Polymer Substrates

Nanoindentation and Nanoscratch of Oxide Coatings on Thin Film Polymer Substrates

Nanotribological properties of Diamond like carbon thin flexible films on ACM rubber

Nanotribological properties of Diamond like carbon thin flexible films on ACM rubber

Physical characterization of coated surfaces - Part II : Scratch Test

Physical characterization of coated surfaces - Part II : Scratch Test

Review of Indenter Materials for High Temperature Nanoindentation

Review of Indenter Materials for High Temperature Nanoindentation

Spherical Nanoindentation of Polyacrylamide Hydrogels using the Bioindenter (BHT)

Spherical Nanoindentation of Polyacrylamide Hydrogels using the Bioindenter (BHT)

The Ultra Nanoindentation Tester: New generation of thermal drift free indentation

The Ultra Nanoindentation Tester: New generation of thermal drift free indentation

Gold nanoparticles: Size matters, and so does stability

Gold nanoparticles: Size matters, and so does stability

Gold nanoparticles are now used in many fields, from medicine to electronics, but each application has specific particle-size and stability requirements. Gold nanoparticles can be easily monitored with the Litesizer™ 500.

Applications of nanoindentation in biology and medicine

Applications of nanoindentation in biology and medicine

Nanoindentation for biological materials

Nanomaterials | Platinum-doped TiO2 Nanofibers and Nanowires

Nanomaterials | Platinum-doped TiO2 Nanofibers and Nanowires

Herein is summarized an easy large scale synthesis of TiO2 nanotubes which were doped with platinum and characterized towards their photocatalytic activity.

Identifying three different particle sizes in one sample with DLS

Identifying three different particle sizes in one sample with DLS

Particle suspensions often contain more than one size of particle. However, many particle analyzers cannot resolve particle mixtures, instead they detect an average of all sizes. The Litesizer™ 500 can detect three sizes in one sample.

Nanoparticles for Ceramics: Size, Stability & pH

Nanoparticles for Ceramics: Size, Stability & pH

In nanoparticle suspensions that will be used in ceramics, particle size and stability are of vital importance. Suspension stability is essential to ensure that the particles to stay in suspension, and maintain constant particle size.

Temperature-dependent GISAXS studies on thin films

Temperature-dependent GISAXS studies on thin films

The temperature-induced decomposition of a thin film structure has been studied using the SAXSpoint system with the new temperature-controlled GISAXS stage.

An insight into the Structure of Copolymer Surfactants

An insight into the Structure of Copolymer Surfactants

The structure of inhomogeneous (core-shell) nanoparticles was studied with the SAXSpoint system. The internal structure of Pluronic P123 micelles in water was determined by calculating the radial electron density profile.

Collagen - A Validation Sample for SAXS Systems

Collagen - A Validation Sample for SAXS Systems

The performance of the SAXSpoint 2.0 system is evaluated by measurements of tendon collagen. SAXSpoint 2.0 produces data with excellent resolution in the entire angular range and delivers true 2D SWAXS images.

Tuning of Solid Surface Properties by Self-Assembled Monolayers

Tuning of Solid Surface Properties by Self-Assembled Monolayers

The zeta potential measurement assists in tailoring the properties of technical and biomedical surfaces using self-assembled monolayers.

Nanomaterials | Microwave Synthesis Meets X-ray Diffraction

Nanomaterials | Microwave Synthesis Meets X-ray Diffraction

Herein a kinetic study is presented employing a high-energy X-ray synchotron beamline together with a customized microwave reactor.

SAXSpoint with MetalJet Source

SAXSpoint with MetalJet Source

SAXSpoint now integrates the high-brightness MetalJet X-ray source enabling ultra-fast SAXS measurements in the laboratory.

_Synthesis | Nanomaterials | TiO2 Thin Films

_Synthesis | Nanomaterials | TiO2 Thin Films

The fabrication of nano-sized films is an important research topic, as it allows diverse applications, e.g. for semiconductor devices, optoelectronics, energy storage, medicine, etc.

In-situ GISAXS heating experiments on self-assembled Gold nanoparticles

In-situ GISAXS heating experiments on self-assembled Gold nanoparticles

Thermal morphology changes of self-assembled Gold nanoparticles have been studied using the SAXSpoint system with the temperature controlled GISAXS stage.

Size and shape of gold nanoparticles in toluene via SAXS

Size and shape of gold nanoparticles in toluene via SAXS

A solution of colloidal gold nanoparticles was characterized for size and shape by the SAXSpace system.

Evaluating GISAXS data with SAXSanalysis using the BornAgain export

Evaluating GISAXS data with SAXSanalysis using the BornAgain export

A detailed GISAXS structure analysis of a monolayer of gold nanoparticles with SAXSanalysis and BornAgain.

Studying the Internal Structure of Carbon Nanotubes with SAXS

Studying the Internal Structure of Carbon Nanotubes with SAXS

A polymer/multi-walled carbon nanotubes composite was measured with the SAXSpace system. The internal structure of the nanotubes was determined by calculating the electron density profile of the nanotube’s cross-section.

Protein Shape Determination by Small Angle X-Ray Scattering

Protein Shape Determination by Small Angle X-Ray Scattering

The 3-dimensional shape of Glucose Isomerase in solution was studied with the SAXSpace system. The solution structure of this protein was compared with the crystal structure obtained by X-ray crystallography.

Protein Mass Determination using Small Angle X-Ray Scattering

Protein Mass Determination using Small Angle X-Ray Scattering

The molecular weight of Glucose Isomerase was determined with the SAXSpace small-angle X-ray scattering system. The results are in good agreement with theoretically calculated values from X-ray crystallography data.

Quantum dots - Size determination by SAXS

Quantum dots - Size determination by SAXS

A dispersion of nanosized CdSe quantum dots was analyzed with the SAXSpace system. The particle size, which is a very crucial parameter for the properties of quantum dots, was determined within a very short time.

Structural Characterization of a Mesoporous Material

Structural Characterization of a Mesoporous Material

A mesoporous material was studied with the SAXSpace system. Important structural parameters like pore size, degree of polydispersity, total volume fraction of the pores and arrangement of the pores were obtained.

Small Angle X-Ray Scattering with Microcrystalline Materials

Small Angle X-Ray Scattering with Microcrystalline Materials

SAXS is routinely used for the characterization of liquid crystalline phases. If the crystalline domains are large and the sample is very viscous the scattering is not averaged over all orientations. The RotorCell enables measuring such samples.

Quality control of pharmaceutical excipients during storage and processing

Quality control of pharmaceutical excipients during storage and processing

The structure of pharmaceutical excipients as a function of storage time and temperature was analyzed by small- and wide-angle X-ray scattering using the SAXSpace system.

Fast Structure Analysis of Pharmaceutical Excipients by SWAXS for Product Quality Control

Fast Structure Analysis of Pharmaceutical Excipients by SWAXS for Product Quality Control

The nanostructure of pharmaceutical excipients used as taste masking agents was rapidly determined for quick quality control with the SAXSpace system.

Coir fibers - SWAXS studies of structural changes induced by tensile stress

Coir fibers - SWAXS studies of structural changes induced by tensile stress

Microfibril angle in coir fibers during tensile straining was studied using the SAXSpace system operated in point collimation mode in combination with the integrated TS 600 tensile stage.

Structure Determination of Interacting Sample Systems

Structure Determination of Interacting Sample Systems

Evaluation of interacting (charged or concentrated) particles requires the knowledge of “form and structure factor”. The unique GIFT software allows to study samples in their original state and to determine the nanostructure of the particles.

Studying the Internal Structure of Lamellar Systems

Studying the Internal Structure of Lamellar Systems

The SAXSpace system was used to characterize nano-structured lamellae present in a surfactant sample. The internal structure (core-shell) of the lamellae could be precisely determined.

An Insight into the Structure of Surfactants

An Insight into the Structure of Surfactants

The structure of inhomogeneous (core-shell) nanoparticles was studied with the SAXSpace system. The internal structure of Sodium Dodecyl Sulfate micelles in water was determined by calculating the radial electron density profile.

Size and Size Distribution of Gold Nanoparticles by SAXS

Size and Size Distribution of Gold Nanoparticles by SAXS

Gold nanoparticle dispersions were measured with the SAXSpace system. SAXS proved to be a well-suited method for determining the size distribution of a binary mixture of two dispersions with very similar particle size.