Nanomaterials

Nanomateriales

Para una comprensión y optimización más detallada de las propiedades de los nanomateriales, las nanoestructuras de los materiales son de máxima importancia. El conocimiento de las formaciones de las estructuras es inestimable para la elaboración de los materiales técnicos. Anton Paar ofrece una variedad de técnicas para la síntesis y el análisis de los nanomateriales, tal como el patrón de dispersión de rayos X, la reología y más. Busque el instrumento de medición que cumpla con sus necesidades particulares en la lista de instrumentos debajo o póngase en contacto con nosotros para permitirnos ayudarlo a encontrar la mejor solución.

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El accesorio de sensor de presión permite un control exacto de reacción dentro del recipiente de referencia del rotor 16MF100 o el rotor 16HF100. Los datos de presión se transfieren al horno a través de la señal infrarroja. Si es necesario, se puede actualizar el accesorio de sensor de presión a un accesorio de sensor de presión/temperatura.

Accesorio de sensor de presión

Accesorio de sensor de presión/temperatura para un control exacto de reacción dentro del recipiente de referencia del rotor 16MF100 o el rotor 16HF100.

Accesorio del sensor de presión/temperatura

Analizador de microindentación (MHT³)

Analizador electrocinético para análisis de superficies sólidas: SurPASS™ 3

Analizador electrocinético para análisis rutinarios de superficies sólidas: SurPASS™ 3 Eco

Anton Paar Bioindenter™ (UNHT³ Bio)

Instrumento SAXSpace

Análisis rutinarios SAXS/WAXS/BIOSAXS: SAXSpace

Cabezal de medición del DSR (reómetro dinámico de cizalla): DSR 502

Calotest Industrial (CAT²i)

Cámara Cryo & Humidity CHC plus+ es una combinación única de la cámara CHC Cryo & Humidity polifacética y un generador de humedad avanzada (RH) para el análisis de cambios estructurales dependientes de la humedad o temperatura en materiales que usan difracción de rayos X

Cámara Cryo & Humidity: CHC plus⁺

Cámara HPC 900 de alta presión: exclusiva cámara de alta presión y alta temperatura para el análisis in situ de difracción de rayos X de interacciones entre gases y sólidos.

Cámara de alta presión: HPC 900

Cámara de baja temperatura: TTK 600

HTK 1200N: cámara de alta temperatura con un diseño sólido para estudios de difracción de rayos X in situ en diferentes atmósferas de hasta 1200 °C

Cámara de horno de alta temperatura: HTK 1200N

Reactor Chamber: XRK 900

Cámara del reactor: XRK 900

Cámara térmica de tiras de alta temperatura HTK 16N | HTK 2000N

Densímetro: DMA™4500 M

Densímetro: DMA™ 4100 M

Densímetro: DMA™ 5000 M

El rotor 16HF100 de digestión ácida con 16 recipientes de presión alta está diseñado para una alta capacidad de rendimiento de las muestras y un manejo eficiente.

Digestión por microondas: Rotor 16HF100

El rotor 16MF100 de digestión ácida con 16 recipientes de presión está diseñado para una alta capacidad de rendimiento de las muestras y un manejo eficiente.

Digestión por microondas: Rotor 16MF100

Dispositivo de prueba de nano-rayado: NST³

Etapa de tensión TS 600: mesa de ajuste de altura para muestras para estudios de difracción de rayos X in situ de fenómenos de estrés/cepas en fibras, láminas y capas delgadas

Dispositivo de tracción: TS 600

Equipo de micro rayado (MST³)

Equipo de nanoindentación: NHT³

Equipo de ultra nanoindentación: UNHT³

Equipo micro-combi (MCT³)

Espectrómetro portátil Raman: Cora 100

Etapa caliente con cúpula para goniómetros de cuatro círculos DHS 1100 con cúpula de grafito para estudios de rayox X de alta temperatura de muestras policristalinas y capas delgadas de 25 °C a 1100 °C

Etapa caliente con cúpula para goniómetros de cuatro círculos: DHS 1100

Etapa de alineación controlable por PC

Etapa de refrigeración con cúpula para goniómetros de cuatro círculos: DCS 500

El rotor 8EVAP es un accesorio innovador para la evaporación por microondas con el sistema modular de preparación de muestras para microondas de Multiwave PRO. Simplifica y acelera en gran medida la evaporación asistida por microondas de los ácidos y la concentración de soluciones de muestras acuosas en 8 recipientes al mismo tiempo.

Evaporación asistida por microondas: Rotor 8EVAP

Cámara de alta temperatura HTK 1200N para estudios XRD de refracción y transmisión combinadas a altas temperaturas de hasta 1200 °C.

Extensión capilar: HTK 1200N

El rotor 16SOLV HF100 amplía las posibilidades de Multiwave PRO para la digestión asistida por microondas y la extracción de muestras inorgánicas y orgánicas. Además, se mejora con facilidad para aplicaciones de digestión ácida mediante el cambio de tapas roscadas.

Extracción asistida por microondas: Rotor 16SOLV HF100

El rotor 168OLV MF100 amplía las posibilidades de Multiwave PRO para la digestión y extracción de muestras inorgánicas y orgánicas asistidas por microondas y se mejora con facilidad para aplicaciones de digestión ácida mediante el cambio de tapas roscadas.

Extracción asistida por microondas: Rotor 16SOLV MF100

Haz para laboratorio SAXS/WAXS/GISAXS: SAXSpoint 2.0

HTR Compact: Reómetro - inyector automático para el mayor rendimiento de muestras

HTR: Automatización Reométrica para un rendimiento de muestras alto y manejo de muestras complejas

HTX: Medición de viscosidad, densidad, concentración de líquidos, altamente automatizado y ampliable

Litesizer™ 100

Litesizer™ 500

Abbemat Performance y Performance Plus

Línea Abbemat Performance y Performance Plus

Abbemat Heavy Duty

línea Heavy Duty de Abbemat

Medidor de densidad y velocidad del sonido DSA 5000 M

Probador de rayado Revetest® (RST³)

Refractómetro de múltiple longitud de onda Abbemat WR/MW

Refractómetro con longitudes de onda múltiples Abbemat MW

Reómetro: MCR 72 y MCR 92

Reómetro: MCR 102, MCR 302, MCR 502

El rotor 1DRY es el accesorio ideal para el manejo eficiente de muestras con anterioridad a la digestión. El secado asistido por microondas requiere un cuarto del tiempo necesario si utiliza métodos convencionales, sin carbonización ni contaminación de las muestras.

Secado asistido por microondas: Rotor 1DRY

Vista desde arriba de la sonda en T montada con rotor 8N de Multiwave PRO.

Sensor de temperatura

Sistemas de reómetro y horno FRS 1600 y FRS 1800

Software para el análisis de partículas: Kalliope™

Síntesis Asistida por Microondas: Monowave 400/200

En función de una nueva y revolucionaria técnica, el reactor de mesa Masterwave BTR completamente nuevo transfiere por primera vez síntesis por microondas al kilolab. La productividad en su laboratorio mejora considerablemente hasta lograr cantidades de kilogramos por día. El agitador de paleta magnético del reactor de mesa proporciona programas de agitación independientes para el contenido individual. Dada su técnica de medición de temperatura con sensor en aumento, Masterwave BTR cuenta con la precisión de alta temperatura necesaria para la transferencia de método directo desde cualquier dispositivo asistido por microondas más pequeño.

Síntesis de Kilogramos asistida por microondas en el laboratorio: Masterwave BTR

Temperature Tribometer

Tribómetro de alta temperatura (THT)

High Temperature Vacuum Tribometer

Tribómetro de vacío (VTHT / VTRB)

Tribómetro tipo pin-on-disk (perno en disco): TRB³

Ultra nanoindentación a alta temperatura UNHT³ HTV

Viscosímetro de caída de bola Lovis 2000 M/ME

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Anton Paar Aplicaciones

Better Sample Preparation of Polymers - Microwave-induced Oxygen Combustion (MIC)

Better Sample Preparation of Polymers - Microwave-induced Oxygen Combustion (MIC)

If you have any problems with digesting plastic & polymer samples for elemental analysis due to inhomogeneity or high residual carbon content think about the unique microwave-induced oxygen combustion from Anton Paar.

Improve Digestion Quality and Save Money – Microwave Digestion rules out Open Digestion

Improve Digestion Quality and Save Money – Microwave Digestion rules out Open Digestion

Reliable elemental analysis results need robust sample preparation to destroy sample matrices or to separate matrix from analytes. The sample preparation step is by far the most error-prone and critical step of the analytical procedure.

Mesoporous thin films - Investigating the structure of multi-layered films by GISAXS

Mesoporous thin films - Investigating the structure of multi-layered films by GISAXS

Single- and double-layered mesoporous thin films have been analyzed by GISAXS for their structural properties using the SAXSpoint system.

Characterization of the scratch resistance of ceramic tiles

Characterization of the scratch resistance of ceramic tiles

High temperature tribological behavior of advanced hard coatings for cutting tools

High temperature tribological behavior of advanced hard coatings for cutting tools

High temperature tribological behavior of advanced hard coatings for cutting tools

The influence of Surface Roughness on Instrumented Indentation Testing (IIT)

The influence of Surface Roughness on Instrumented Indentation Testing (IIT)

In-Situ observation of the scratch/indentation true contact area to provide analysis without being model-dependent

In-Situ observation of the scratch/indentation true contact area to provide analysis without being model-dependent

Nanoindentation and Nanoscratch of Oxide Coatings on Thin Film Polymer Substrates

Nanoindentation and Nanoscratch of Oxide Coatings on Thin Film Polymer Substrates

Nanotribological properties of Diamond like carbon thin flexible films on ACM rubber

Nanotribological properties of Diamond like carbon thin flexible films on ACM rubber

Physical characterization of coated surfaces - Part II : Scratch Test

Physical characterization of coated surfaces - Part II : Scratch Test

Review of Indenter Materials for High Temperature Nanoindentation

Review of Indenter Materials for High Temperature Nanoindentation

Spherical Nanoindentation of Polyacrylamide Hydrogels using the Bioindenter (BHT)

Spherical Nanoindentation of Polyacrylamide Hydrogels using the Bioindenter (BHT)

The Ultra Nanoindentation Tester: New generation of thermal drift free indentation

The Ultra Nanoindentation Tester: New generation of thermal drift free indentation

Gold nanoparticles: Size matters, and so does stability

Gold nanoparticles: Size matters, and so does stability

Gold nanoparticles are now used in many fields, from medicine to electronics, but each application has specific particle-size and stability requirements. Gold nanoparticles can be easily monitored with the Litesizer™ 500.

Applications of nanoindentation in biology and medicine

Applications of nanoindentation in biology and medicine

Nanoindentation for biological materials

Nanomaterials | Platinum-doped TiO2 Nanofibers and Nanowires

Nanomaterials | Platinum-doped TiO2 Nanofibers and Nanowires

Herein is summarized an easy large scale synthesis of TiO2 nanotubes which were doped with platinum and characterized towards their photocatalytic activity.

Identifying three different particle sizes in one sample with DLS

Identifying three different particle sizes in one sample with DLS

Particle suspensions often contain more than one size of particle. However, many particle analyzers cannot resolve particle mixtures, instead they detect an average of all sizes. The Litesizer™ 500 can detect three sizes in one sample.

Nanoparticles for Ceramics: Size, Stability & pH

Nanoparticles for Ceramics: Size, Stability & pH

In nanoparticle suspensions that will be used in ceramics, particle size and stability are of vital importance. Suspension stability is essential to ensure that the particles to stay in suspension, and maintain constant particle size.

Temperature-dependent GISAXS studies on thin films

Temperature-dependent GISAXS studies on thin films

The temperature-induced decomposition of a thin film structure has been studied using the SAXSpoint system with the new temperature-controlled GISAXS stage.

An insight into the Structure of Copolymer Surfactants

An insight into the Structure of Copolymer Surfactants

The structure of inhomogeneous (core-shell) nanoparticles was studied with the SAXSpoint system. The internal structure of Pluronic P123 micelles in water was determined by calculating the radial electron density profile.

Collagen - A Validation Sample for SAXS Systems

Collagen - A Validation Sample for SAXS Systems

The performance of the SAXSpoint 2.0 system is evaluated by measurements of tendon collagen. SAXSpoint 2.0 produces data with excellent resolution in the entire angular range and delivers true 2D SWAXS images.

Tuning of Solid Surface Properties by Self-Assembled Monolayers

Tuning of Solid Surface Properties by Self-Assembled Monolayers

The zeta potential measurement assists in tailoring the properties of technical and biomedical surfaces using self-assembled monolayers.

Nanomaterials | Microwave Synthesis Meets X-ray Diffraction

Nanomaterials | Microwave Synthesis Meets X-ray Diffraction

Herein a kinetic study is presented employing a high-energy X-ray synchotron beamline together with a customized microwave reactor.

SAXSpoint with MetalJet Source

SAXSpoint with MetalJet Source

SAXSpoint now integrates the high-brightness MetalJet X-ray source enabling ultra-fast SAXS measurements in the laboratory.

_Synthesis | Nanomaterials | TiO2 Thin Films

_Synthesis | Nanomaterials | TiO2 Thin Films

The fabrication of nano-sized films is an important research topic, as it allows diverse applications, e.g. for semiconductor devices, optoelectronics, energy storage, medicine, etc.

In-situ GISAXS heating experiments on self-assembled Gold nanoparticles

In-situ GISAXS heating experiments on self-assembled Gold nanoparticles

Thermal morphology changes of self-assembled Gold nanoparticles have been studied using the SAXSpoint system with the temperature controlled GISAXS stage.

Size and shape of gold nanoparticles in toluene via SAXS

Size and shape of gold nanoparticles in toluene via SAXS

A solution of colloidal gold nanoparticles was characterized for size and shape by the SAXSpace system.

Evaluating GISAXS data with SAXSanalysis using the BornAgain export

Evaluating GISAXS data with SAXSanalysis using the BornAgain export

A detailed GISAXS structure analysis of a monolayer of gold nanoparticles with SAXSanalysis and BornAgain.

Studying the Internal Structure of Carbon Nanotubes with SAXS

Studying the Internal Structure of Carbon Nanotubes with SAXS

A polymer/multi-walled carbon nanotubes composite was measured with the SAXSpace system. The internal structure of the nanotubes was determined by calculating the electron density profile of the nanotube’s cross-section.

Protein Shape Determination by Small Angle X-Ray Scattering

Protein Shape Determination by Small Angle X-Ray Scattering

The 3-dimensional shape of Glucose Isomerase in solution was studied with the SAXSpace system. The solution structure of this protein was compared with the crystal structure obtained by X-ray crystallography.

Protein Mass Determination using Small Angle X-Ray Scattering

Protein Mass Determination using Small Angle X-Ray Scattering

The molecular weight of Glucose Isomerase was determined with the SAXSpace small-angle X-ray scattering system. The results are in good agreement with theoretically calculated values from X-ray crystallography data.

Desmearing of Line-smeared Scattering Curves

Desmearing of Line-smeared Scattering Curves

Small Angle X-Ray Scattering instruments use two different beam geometries - point collimation and line collimation. Using a line shaped beam dramatically reduces the measurement time while maintaining the same data quality.

Quantum dots - Size determination by SAXS

Quantum dots - Size determination by SAXS

A dispersion of nanosized CdSe quantum dots was analyzed with the SAXSpace system. The particle size, which is a very crucial parameter for the properties of quantum dots, was determined within a very short time.

Fast SAXS Measurements of a Diluted Protein Solution

Fast SAXS Measurements of a Diluted Protein Solution

A 1% Lysozyme solution was measured with the SAXSpace system. Structural information can be obtained already after 1 minute due to the highly intense line-collimation mode and the compact design of the SAXSpace system.

Structural Characterization of a Mesoporous Material

Structural Characterization of a Mesoporous Material

A mesoporous material was studied with the SAXSpace system. Important structural parameters like pore size, degree of polydispersity, total volume fraction of the pores and arrangement of the pores were obtained.

Small Angle X-Ray Scattering with Microcrystalline Materials

Small Angle X-Ray Scattering with Microcrystalline Materials

SAXS is routinely used for the characterization of liquid crystalline phases. If the crystalline domains are large and the sample is very viscous the scattering is not averaged over all orientations. The RotorCell enables measuring such samples.

Quality control of pharmaceutical excipients during storage and processing

Quality control of pharmaceutical excipients during storage and processing

The structure of pharmaceutical excipients as a function of storage time and temperature was analyzed by small- and wide-angle X-ray scattering using the SAXSpace system.

Fast Structure Analysis of Pharmaceutical Excipients by SWAXS for Product Quality Control

Fast Structure Analysis of Pharmaceutical Excipients by SWAXS for Product Quality Control

The nanostructure of pharmaceutical excipients used as taste masking agents was rapidly determined for quick quality control with the SAXSpace system.

Coir fibers - SWAXS studies of structural changes induced by tensile stress

Coir fibers - SWAXS studies of structural changes induced by tensile stress

Microfibril angle in coir fibers during tensile straining was studied using the SAXSpace system operated in point collimation mode in combination with the integrated TS 600 tensile stage.

Structure Determination of Interacting Sample Systems

Structure Determination of Interacting Sample Systems

Evaluation of interacting (charged or concentrated) particles requires the knowledge of “form and structure factor”. The unique GIFT software allows to study samples in their original state and to determine the nanostructure of the particles.

Studying the Internal Structure of Lamellar Systems

Studying the Internal Structure of Lamellar Systems

The SAXSpace system was used to characterize nano-structured lamellae present in a surfactant sample. The internal structure (core-shell) of the lamellae could be precisely determined.

An Insight into the Structure of Surfactants

An Insight into the Structure of Surfactants

The structure of inhomogeneous (core-shell) nanoparticles was studied with the SAXSpace system. The internal structure of Sodium Dodecyl Sulfate micelles in water was determined by calculating the radial electron density profile.

Size and Size Distribution of Gold Nanoparticles by SAXS

Size and Size Distribution of Gold Nanoparticles by SAXS

Gold nanoparticle dispersions were measured with the SAXSpace system. SAXS proved to be a well-suited method for determining the size distribution of a binary mixture of two dispersions with very similar particle size.