Nanomaterials

Nanomateriali

Per una comprensione approfondita e una messa a punto ottimale delle proprietà dei nanomateriali sono di fondamentale importanza le nanostrutture dei materiali. La conoscenza del processo di formazione di queste strutture è essenziale per personalizzare i materiali tecnici. Anton Paar offre un'ampia gamma di tecniche per la sintesi e l'analisi di nanomateriali, quali lo scattering di raggi X, la reologia e altre. Cercate lo strumento di misura che meglio risponde alle vostre esigenze nella lista riportata sotto oppure contattateci direttamente.

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Abbemat Heavy Duty

Abbemat Heavy Duty Line

Sensore accessorio di pressione/temperatura per un controllo accurato della reazione all'interno del recipiente di riferimento del rotore 16MF100 e/o del rotore 16HF100.

Accessorio sensore p/T

Il sensore accessorio di pressione consente un controllo accurato della reazione all'interno del recipiente di riferimento del rotore 16MF100 o del rotore 16HF100. I dati della pressione vengono trasferiti al forno tramite un segnale a infrarossi. Se necessario, il sensore accessorio della pressione può essere trasformato in un sensore accessorio di pressione/temperatura.

Accessorio sensore pressione

Analizzatore elettrocinetico per analisi di routine su superfici solide: SurPASS™ 3 Eco

Analizzatore elettrocinetico per analisi superfici solide: SurPASS™ 3

Beamline di laboratorio SAXS/WAXS/GISAXS: SAXSpoint 2.0

Bioindentatore (UNHT³ Bio) Anton Paar

Camera a bassa temperatura: TTK 600

Camera ad alta pressione HPC 900 - Camera ad alta pressione e ad alta temperatura per studi di diffrazione di raggi X in loco sulle interazioni tra gas e solidi

Camera ad alta pressione: HPC 900

Reactor Chamber: XRK 900

Camera per reattore: XRK 900

La camera umida criogenica CHC plus+ è un'esclusiva combinazione della camera umida criogenica multifunzione CHC e di un generatore avanzato di umidità (RH) per l'analisi tramite diffrazione di raggi X di modifiche strutturali di materiali dipendenti dall'umidità e/o dalla temperatura

Camera umida criogenica CHC plus⁺

Camere con filamento riscaldante ad alta temperatura: HTK 16N | HTK 2000N

Densimetro e misuratore velocità del suono: DSA 5000 M

Densimetro: DMA™ 4100 M

Densimetro: DMA™ 4500 M

Densimetro: DMA™ 5000 M

Il rotore per digestione acida 16MF100 con 16 recipienti a pressione è progettato per un'elevata produttività e una manipolazione efficiente.

Digestione a microonde: Rotor 16MF100

Il rotore per digestione acida 16HF100 con 16 recipienti ad alta pressione è progettato per un'elevata produttività e una manipolazione efficiente.

Digestione a microonde: Rotore 16HF100

Dispositivo di trazione TS 600 - Dispositivo per studi in loco con diffrazione di raggi X di fenomeni di stress/sollecitazioni in fibre, lamine e film sottili

Dispositivo di trazione: TS 600

Il rotore 1DRY è l'accessorio ideale per una manipolazione efficiente dei campioni prima della digestione. L'essiccamento assistito da microonde richiede un quarto del tempo impiegato dai metodi tradizionali e non provoca carbonizzazione o contaminazione dei campioni.

Essiccamento assistito da microonde: Rotore 1DRY

Il rotore 16SOLV HF100 espande le possibilità del Multiwave PRO in termini di digestione ed estrazione assistite da microonde di campioni organici e inorganici e può essere facilmente modificato per applicazioni di digestione acida cambiando i tappi a vite.

Estrazione a microonde: Rotore 16SOLV HF100

Il rotore 16SOLV MF100 espande le possibilità del Multiwave PRO in termini di digestione ed estrazione assistite da microonde di campioni organici e inorganici e può essere facilmente modificato per applicazioni di digestione acida cambiando i tappi a vite.

Estrazione a microonde: Rotore 16SOLV MF100

Il rotore 8EVAP è un accessorio innovativo per l'evaporazione a microonde con il sistema modulare di preparazione dei campioni a microonde Multiwave PRO. Semplifica e accelera notevolmente l'evaporazione assistita da microonde di acidi e concentrazioni di soluzioni di campioni acquosi in 8 recipienti contemporaneamente.

Evaporazione a microonde: Rotore 8EVAP

HTK 1200N - Camera ad alta temperatura con design robusto per studi di diffrazione di raggi X in loco in atmosfere diverse fino a 1200 °C

Forno a camera ad alta temperatura HTK 1200N

HTR Compact: reometro campionatore automatico per un'elevata produttività di campionamento

HTR: reometro automatizzato per la massima produttività e la gestione complessa di campioni

HTX: misura della viscosità, densità, concentrazione di liquidi, elevata automazione ed espansibilità

Industrial Calotest (CAT²i)

Abbemat Performance e Performance Plus

Linea Abbemat Performance e Performance Plus

Litesizer™ 100

Litesizer™ 500

Micro Combi Tester (MCT³)

Micro Indentation Tester (MHT³)

Micro Scratch Tester (MST³)

Nano Scratch Tester: NST³

Nanoindentation tester: NHT³

Nanoindentazione ad alta temperatura (UNHT³ HTV)

Reometri: MCR 102, MCR 302, MCR 502

Reometri: MCR 72 e MCR 92

Abbemat WR/MW, rifrattometro a lunghezze d'onda multiple

Rifrattometro multilunghezza d'onda Abbemat MW

Camera ad alta temperatura HTK 1200N per studi XRD combinati di riflessione e trasmissione ad alte temperature fino a 1200 °C

Riscaldatore capillare per HTK 1200N

SAXSpace instrument

Routine analisi SAXS/WAXS/BIOSAXS: SAXSpace

Scratch Tester Revetest® (RST³)

Basato su una nuova tecnica rivoluzionaria, il nuovissimo reattore da banco Masterwave BTR consente per la prima volta di trasferire la sintesi a microonde su scala Kilolab. La produttività del laboratorio viene così notevolmente incrementata fino a diversi chilogrammi al giorno. L'agitatore a pala del reattore da banco, azionato magneticamente, fornisce regimi di agitazione indipendenti per singolo contenuto. Grazie alla particolare tecnologia di misura della temperatura, Masterwave BTR offre l'accuratezza di temperatura richiesta per il trasferimento diretto da qualsiasi dispositivo a microonde più piccolo.

Sintesi a microonde nel Kilolab: Masterwave BTR

Sintesi a microonde: Monowave 400/200

Sistemi combinati di reometro a fornace FRS 1600 e FRS 1800

Software per l'analisi delle particelle: Kalliope™

Spettrometro Raman portatile: Cora 100

Stadio allineamento controllabile da PC

Supporto caldo a cupola per goniometri a quattro cerchi DHS 1100 con cupola in grafite per studi a raggi X ad alte temperature di campioni policristallini e film sottili da 25 a 1100 °C

Stadio caldo a cupola per goniometri a quattro cerchi: DHS 1100

Stadio di raffreddamento a cupola per goniometri a quattro cerchi: DCS 500

Vista dall'alto del sensore della temperatura T-probe montato sul rotore 8N del Multiwave PRO.

T-probe

Testa di misura per reometro a taglio dinamico: DSR 502

Temperature Tribometer

Tribometro per alte temperature (THT)

High Temperature Vacuum Tribometer

Tribometro per vuoto (VTHT / VTRB)

Tribometro pin-on-disk: TRB³

Ultra Nanoindentation Tester: UNHT³

Viscosimetro a sfera rotante Lovis 2000 M/ME

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Anton Paar Applicazioni

Better Sample Preparation of Polymers - Microwave-induced Oxygen Combustion (MIC)

Better Sample Preparation of Polymers - Microwave-induced Oxygen Combustion (MIC)

If you have any problems with digesting plastic & polymer samples for elemental analysis due to inhomogeneity or high residual carbon content think about the unique microwave-induced oxygen combustion from Anton Paar.

Improve Digestion Quality and Save Money – Microwave Digestion rules out Open Digestion

Improve Digestion Quality and Save Money – Microwave Digestion rules out Open Digestion

Reliable elemental analysis results need robust sample preparation to destroy sample matrices or to separate matrix from analytes. The sample preparation step is by far the most error-prone and critical step of the analytical procedure.

Mesoporous thin films - Investigating the structure of multi-layered films by GISAXS

Mesoporous thin films - Investigating the structure of multi-layered films by GISAXS

Single- and double-layered mesoporous thin films have been analyzed by GISAXS for their structural properties using the SAXSpoint system.

Characterization of the scratch resistance of ceramic tiles

Characterization of the scratch resistance of ceramic tiles

High temperature tribological behavior of advanced hard coatings for cutting tools

High temperature tribological behavior of advanced hard coatings for cutting tools

High temperature tribological behavior of advanced hard coatings for cutting tools

The influence of Surface Roughness on Instrumented Indentation Testing (IIT)

The influence of Surface Roughness on Instrumented Indentation Testing (IIT)

In-Situ observation of the scratch/indentation true contact area to provide analysis without being model-dependent

In-Situ observation of the scratch/indentation true contact area to provide analysis without being model-dependent

Nanoindentation and Nanoscratch of Oxide Coatings on Thin Film Polymer Substrates

Nanoindentation and Nanoscratch of Oxide Coatings on Thin Film Polymer Substrates

Nanotribological properties of Diamond like carbon thin flexible films on ACM rubber

Nanotribological properties of Diamond like carbon thin flexible films on ACM rubber

Physical characterization of coated surfaces - Part II : Scratch Test

Physical characterization of coated surfaces - Part II : Scratch Test

Review of Indenter Materials for High Temperature Nanoindentation

Review of Indenter Materials for High Temperature Nanoindentation

Spherical Nanoindentation of Polyacrylamide Hydrogels using the Bioindenter (BHT)

Spherical Nanoindentation of Polyacrylamide Hydrogels using the Bioindenter (BHT)

The Ultra Nanoindentation Tester: New generation of thermal drift free indentation

The Ultra Nanoindentation Tester: New generation of thermal drift free indentation

Gold nanoparticles: Size matters, and so does stability

Gold nanoparticles: Size matters, and so does stability

Gold nanoparticles are now used in many fields, from medicine to electronics, but each application has specific particle-size and stability requirements. Gold nanoparticles can be easily monitored with the Litesizer™ 500.

Applications of nanoindentation in biology and medicine

Applications of nanoindentation in biology and medicine

Nanoindentation for biological materials

Nanomaterials | Platinum-doped TiO2 Nanofibers and Nanowires

Nanomaterials | Platinum-doped TiO2 Nanofibers and Nanowires

Herein is summarized an easy large scale synthesis of TiO2 nanotubes which were doped with platinum and characterized towards their photocatalytic activity.

Identifying three different particle sizes in one sample with DLS

Identifying three different particle sizes in one sample with DLS

Particle suspensions often contain more than one size of particle. However, many particle analyzers cannot resolve particle mixtures, instead they detect an average of all sizes. The Litesizer™ 500 can detect three sizes in one sample.

Nanoparticles for Ceramics: Size, Stability & pH

Nanoparticles for Ceramics: Size, Stability & pH

In nanoparticle suspensions that will be used in ceramics, particle size and stability are of vital importance. Suspension stability is essential to ensure that the particles to stay in suspension, and maintain constant particle size.

Temperature-dependent GISAXS studies on thin films

Temperature-dependent GISAXS studies on thin films

The temperature-induced decomposition of a thin film structure has been studied using the SAXSpoint system with the new temperature-controlled GISAXS stage.

An insight into the Structure of Copolymer Surfactants

An insight into the Structure of Copolymer Surfactants

The structure of inhomogeneous (core-shell) nanoparticles was studied with the SAXSpoint system. The internal structure of Pluronic P123 micelles in water was determined by calculating the radial electron density profile.

Collagen - A Validation Sample for SAXS Systems

Collagen - A Validation Sample for SAXS Systems

The performance of the SAXSpoint 2.0 system is evaluated by measurements of tendon collagen. SAXSpoint 2.0 produces data with excellent resolution in the entire angular range and delivers true 2D SWAXS images.

Tuning of Solid Surface Properties by Self-Assembled Monolayers

Tuning of Solid Surface Properties by Self-Assembled Monolayers

The zeta potential measurement assists in tailoring the properties of technical and biomedical surfaces using self-assembled monolayers.

Nanomaterials | Microwave Synthesis Meets X-ray Diffraction

Nanomaterials | Microwave Synthesis Meets X-ray Diffraction

Herein a kinetic study is presented employing a high-energy X-ray synchotron beamline together with a customized microwave reactor.

SAXSpoint with MetalJet Source

SAXSpoint with MetalJet Source

SAXSpoint now integrates the high-brightness MetalJet X-ray source enabling ultra-fast SAXS measurements in the laboratory.

_Synthesis | Nanomaterials | TiO2 Thin Films

_Synthesis | Nanomaterials | TiO2 Thin Films

The fabrication of nano-sized films is an important research topic, as it allows diverse applications, e.g. for semiconductor devices, optoelectronics, energy storage, medicine, etc.

In-situ GISAXS heating experiments on self-assembled Gold nanoparticles

In-situ GISAXS heating experiments on self-assembled Gold nanoparticles

Thermal morphology changes of self-assembled Gold nanoparticles have been studied using the SAXSpoint system with the temperature controlled GISAXS stage.

Size and shape of gold nanoparticles in toluene via SAXS

Size and shape of gold nanoparticles in toluene via SAXS

A solution of colloidal gold nanoparticles was characterized for size and shape by the SAXSpace system.

Evaluating GISAXS data with SAXSanalysis using the BornAgain export

Evaluating GISAXS data with SAXSanalysis using the BornAgain export

A detailed GISAXS structure analysis of a monolayer of gold nanoparticles with SAXSanalysis and BornAgain.

Studying the Internal Structure of Carbon Nanotubes with SAXS

Studying the Internal Structure of Carbon Nanotubes with SAXS

A polymer/multi-walled carbon nanotubes composite was measured with the SAXSpace system. The internal structure of the nanotubes was determined by calculating the electron density profile of the nanotube’s cross-section.

Protein Shape Determination by Small Angle X-Ray Scattering

Protein Shape Determination by Small Angle X-Ray Scattering

The 3-dimensional shape of Glucose Isomerase in solution was studied with the SAXSpace system. The solution structure of this protein was compared with the crystal structure obtained by X-ray crystallography.

Protein Mass Determination using Small Angle X-Ray Scattering

Protein Mass Determination using Small Angle X-Ray Scattering

The molecular weight of Glucose Isomerase was determined with the SAXSpace small-angle X-ray scattering system. The results are in good agreement with theoretically calculated values from X-ray crystallography data.

Desmearing of Line-smeared Scattering Curves

Desmearing of Line-smeared Scattering Curves

Small Angle X-Ray Scattering instruments use two different beam geometries - point collimation and line collimation. Using a line shaped beam dramatically reduces the measurement time while maintaining the same data quality.

Quantum dots - Size determination by SAXS

Quantum dots - Size determination by SAXS

A dispersion of nanosized CdSe quantum dots was analyzed with the SAXSpace system. The particle size, which is a very crucial parameter for the properties of quantum dots, was determined within a very short time.

Fast SAXS Measurements of a Diluted Protein Solution

Fast SAXS Measurements of a Diluted Protein Solution

A 1% Lysozyme solution was measured with the SAXSpace system. Structural information can be obtained already after 1 minute due to the highly intense line-collimation mode and the compact design of the SAXSpace system.

Structural Characterization of a Mesoporous Material

Structural Characterization of a Mesoporous Material

A mesoporous material was studied with the SAXSpace system. Important structural parameters like pore size, degree of polydispersity, total volume fraction of the pores and arrangement of the pores were obtained.

Small Angle X-Ray Scattering with Microcrystalline Materials

Small Angle X-Ray Scattering with Microcrystalline Materials

SAXS is routinely used for the characterization of liquid crystalline phases. If the crystalline domains are large and the sample is very viscous the scattering is not averaged over all orientations. The RotorCell enables measuring such samples.

Quality control of pharmaceutical excipients during storage and processing

Quality control of pharmaceutical excipients during storage and processing

The structure of pharmaceutical excipients as a function of storage time and temperature was analyzed by small- and wide-angle X-ray scattering using the SAXSpace system.

Fast Structure Analysis of Pharmaceutical Excipients by SWAXS for Product Quality Control

Fast Structure Analysis of Pharmaceutical Excipients by SWAXS for Product Quality Control

The nanostructure of pharmaceutical excipients used as taste masking agents was rapidly determined for quick quality control with the SAXSpace system.

Coir fibers - SWAXS studies of structural changes induced by tensile stress

Coir fibers - SWAXS studies of structural changes induced by tensile stress

Microfibril angle in coir fibers during tensile straining was studied using the SAXSpace system operated in point collimation mode in combination with the integrated TS 600 tensile stage.

Structure Determination of Interacting Sample Systems

Structure Determination of Interacting Sample Systems

Evaluation of interacting (charged or concentrated) particles requires the knowledge of “form and structure factor”. The unique GIFT software allows to study samples in their original state and to determine the nanostructure of the particles.

Studying the Internal Structure of Lamellar Systems

Studying the Internal Structure of Lamellar Systems

The SAXSpace system was used to characterize nano-structured lamellae present in a surfactant sample. The internal structure (core-shell) of the lamellae could be precisely determined.

An Insight into the Structure of Surfactants

An Insight into the Structure of Surfactants

The structure of inhomogeneous (core-shell) nanoparticles was studied with the SAXSpace system. The internal structure of Sodium Dodecyl Sulfate micelles in water was determined by calculating the radial electron density profile.

Size and Size Distribution of Gold Nanoparticles by SAXS

Size and Size Distribution of Gold Nanoparticles by SAXS

Gold nanoparticle dispersions were measured with the SAXSpace system. SAXS proved to be a well-suited method for determining the size distribution of a binary mixture of two dispersions with very similar particle size.