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Reactor Chamber:
XRK 900

  • Reactor Chamber: XRK 900
  • Reactor Chamber: XRK 900
  • Reactor Chamber: XRK 900
  • Reactor Chamber: XRK 900
  • Reactor Chamber: XRK 900
  • Reactor Chamber: XRK 900
  • Reactor chamber for all common diffractometers
  • For solid state and solid state-gas reactions up to 900 °C and 10 bar
  • Sample holder options: chemically resistant materials, sample spinning, open holders for gas extraction through the sample
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The XRK 900 reactor chamber is the only heating chamber on the market specifically designed for X-ray diffraction experiments for studies of solid state and solid state-gas reactions up to 900 °C and 10 bar. It is a unique tool for in-situ X-ray diffraction investigations - unmatched in robustness and performance.

Key features

Optimal for solid state - gas reactions

  • Furnace heater for excellent temperature uniformity in the sample
  • Reliable measurement and control of the sample temperature
  • Homogeneous flushing and gas flow inside the chamber without dead volumes

Rugged design

  • High quality materials for a long working life
  • Housing temperature up to 150 °C to avoid condensation of reaction products
  • Fits on all common diffractometers

Choice of sample holders

  • Different materials, all chemically very resistant
  • Optional sample spinning for good diffraction data quality
  • Open sample holders for gas extraction through the sample
  • Easy exchange of samples

Technical specifications

Operating temperature 25 °C to 900 °C
Temperature measurement NiCr/NiAl thermocouple
Atmospheres Vacuum (1mbar), air, inert gas, reactive gas
Max. housing temperature 150 °C
Angle of incidence 0 to +165° 2Θ
Max. operating pressure 1 mbar to 10 bar
Sample holder material Stainless steel or glass ceramics
Sample diameter max. 14 mm
Measure geometry Reflection

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  • Qualified support in your local language
  • Protection for your investment throughout its lifecycle
  • 3-year warranty
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Compatible instruments

Consumables

Consumables

Not all items are purchasable online in specific countries.

To find out if you can purchase online from your location, check the online availability below.

SAMPLE HOLDER CLOSED MADE OF GLASS CERAMICS (MACOR)

Online price only | excl.incl. 0VAT
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 69977
Product details
Closed sample holder made of Macor (glass ceramics) Gas flow through the sample and extraction of gas through the sample holder is not possible.

SIEVE 0.2 mm MACOR FOR XRK SAMPLE HOLDER OPEN

Online price only | excl.incl. 0VAT
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 87070
Product details
Macor plate with Ø 0.2 mm holes for gas flow through the sample.

SAMPLE HOLDER CLOSED MADE OF STAINLESS STEEL

Online price only | excl.incl. 0VAT
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 69973
Product details
Closed stainless steel sample holder. Gas flow through the sample and extraction of gas through the sample holder is not possible. Maximum operating temperature 600 °C.

SAMPLE HOLDER OPEN STEEL WITH SIEVE

Online price only | excl.incl. 0VAT
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 101733
Product details
Stainless steel sample holder where the sample is placed on a sieve plate. Gas can flow through the sample and can be extracted at the bottom of the sample holder. Not feasible for vacuum operation of XRK 900. Maximum operating temperature 600 °C.

SAMPLE HOLDER OPEN MACOR WITH SIEVE

Online price only | excl.incl. 0VAT
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 101734
Product details
Sample holder made of Macor (glass ceramics) where the sample is placed on a sieve plate (69963). Gas can flow through the sample and can be extracted at the bottom of the sample holder. Not feasible for vacuum operation of XRK 900

SPARE PARTS PACKAGE XRK 900

Online price only | excl.incl. 0VAT
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 27489
Product details
Consists of:
- 2 Pcs. 17162 Set of Kapton foils (XRK with BE foil)
- 1 Pc. 13463 Pressure hose silicone (6.5 m)
- 1 Pc. 70175 Vacuum grease (20 g)
- 1 Pc. 10213 Set of O-Rings

Si (510) ZERO BACKGROUND INSERT XRK

Online price only | excl.incl. 0VAT
Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 110226
Product details
Si(510) plate of 0.5 mm thickness without X-ray scattering for X-ray transparent samples. Maximum temperature in oxidizing atmospheres: 500 °C Maximum temperature in non-reactive atmospheres: 900 °C.

NON-AMBIENT GUIDE

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Delivery time: %1$s – %2$s working days %1$s – %2$s weeks %1$s – %2$s months
Part number: 223464
Product details
The XRD-Guide gives an overview from instrumentation, analysis, and data interpretation to applications. It gives an introduction to non-ambient X-ray diffraction (NA-XRD) and aims to give a global overview on the main instrumentation and applications. The XRD-Guide is intended to help people new to the field of NA-XRD analysis.